BMRB Entry 15187
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15187
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Title: Backbone and side-chain methyl order parameters and effective correlation times for calmodulin in complex with Phosphodiesterase1A peptide PubMed: 17637663
Deposition date: 2007-03-19 Original release date: 2007-03-19
Authors: Marlow, Michael; Wand, A. Joshua
Citation: Frederick, Kendra; Marlow, Michael; Valentine, Kathy; Wand, A. Joshua. "Conformational entropy in molecular recognition by proteins" Nature 448, 325-329 (2007).
Assembly members:
calmodulin, polymer, 148 residues, Formula weight is not available
PDEs, polymer, 22 residues, Formula weight is not available
Natural source: Common Name: chicken Taxonomy ID: 9031 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Gallus gallus
Experimental source: Production method: recombinant technology Host organism: Escherichia coli Vector: pET
Entity Sequences (FASTA):
calmodulin: ADQLTEEQIAEFKEAFSLFD
KDGDGTITTKELGTVMRSLG
QNPTEAELQDMINEVDADGN
GTIDFPEFLTMMARKMKDTD
SEEEIREAFRVFDKDGNGYI
SAAELRHVMTNLGEKLTDEE
VDEMIREADIDGDGQVNYEE
FVQMMTAK
PDEs: GSQTEKMWQRLKGILRSLVK
QL
- order_parameters
Data type | Count |
order parameters | 185 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | calmodulin | 1 |
2 | PDEs | 2 |
Entities:
Entity 1, calmodulin 148 residues - Formula weight is not available
1 | ALA | ASP | GLN | LEU | THR | GLU | GLU | GLN | ILE | ALA | ||||
2 | GLU | PHE | LYS | GLU | ALA | PHE | SER | LEU | PHE | ASP | ||||
3 | LYS | ASP | GLY | ASP | GLY | THR | ILE | THR | THR | LYS | ||||
4 | GLU | LEU | GLY | THR | VAL | MET | ARG | SER | LEU | GLY | ||||
5 | GLN | ASN | PRO | THR | GLU | ALA | GLU | LEU | GLN | ASP | ||||
6 | MET | ILE | ASN | GLU | VAL | ASP | ALA | ASP | GLY | ASN | ||||
7 | GLY | THR | ILE | ASP | PHE | PRO | GLU | PHE | LEU | THR | ||||
8 | MET | MET | ALA | ARG | LYS | MET | LYS | ASP | THR | ASP | ||||
9 | SER | GLU | GLU | GLU | ILE | ARG | GLU | ALA | PHE | ARG | ||||
10 | VAL | PHE | ASP | LYS | ASP | GLY | ASN | GLY | TYR | ILE | ||||
11 | SER | ALA | ALA | GLU | LEU | ARG | HIS | VAL | MET | THR | ||||
12 | ASN | LEU | GLY | GLU | LYS | LEU | THR | ASP | GLU | GLU | ||||
13 | VAL | ASP | GLU | MET | ILE | ARG | GLU | ALA | ASP | ILE | ||||
14 | ASP | GLY | ASP | GLY | GLN | VAL | ASN | TYR | GLU | GLU | ||||
15 | PHE | VAL | GLN | MET | MET | THR | ALA | LYS |
Entity 2, PDEs 22 residues - Formula weight is not available
1 | GLY | SER | GLN | THR | GLU | LYS | MET | TRP | GLN | ARG | ||||
2 | LEU | LYS | GLY | ILE | LEU | ARG | SER | LEU | VAL | LYS | ||||
3 | GLN | LEU |
Samples:
sample_1: calmodulin, [U-100% 15N], 1.0 mM; PDEs 1.1-1.2 mM
sample_2: calmodulin, [U-100% 13C; U-100% 15N; 60% 2H], 1.0 mM; PDEs 1.1-1.2 mM
sample_conditions_1: ionic strength: 122 mM; pH: 6.5; pressure: 1 atm; temperature: 308 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-15N HSQC | sample_1 | isotropic | sample_conditions_1 |
2D 1H-15N HSQC | sample_1 | isotropic | sample_conditions_1 |
2D 1H-13C HSQC | sample_2 | isotropic | sample_conditions_1 |
2D 1H-13C HSQC | sample_2 | isotropic | sample_conditions_1 |
Software:
NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
NMRDraw, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - peak picking
NMR spectrometers:
- Varian INOVA 500 MHz
- Varian INOVA 600 MHz
Related Database Links:
BMRB | 15184 15185 15186 15188 15191 15470 15624 15650 15852 1634 16418 16465 1648 16764 17264 17360 17771 17807 18027 18028 18556 19036 19238 19586 19604 25253 25257 26503 26626 26627 4056 4270 4284 4310 |
PDB | |
DBJ | BAA08302 BAA11896 BAA19786 BAA19787 BAA19788 |
EMBL | CAA10601 CAA32050 CAA32062 CAA32119 CAA32120 |
GB | AAA35635 AAA35641 AAA37365 AAA40862 AAA40863 |
PIR | JC1305 MCON |
PRF | 0409298A 0608335A |
REF | NP_001008160 NP_001009759 NP_001027633 NP_001039714 NP_001040234 |
SP | O02367 O16305 O96081 P02594 P05932 |
TPG | DAA13808 DAA18029 DAA19590 DAA24777 DAA24988 |
AlphaFold | O02367 O16305 O96081 P02594 P05932 |