BMRB Entry 5489
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR5489
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Title: Backbone and 1H assignments for Tachyplesin I, alanine mutant
Deposition date: 2002-08-02 Original release date: 2002-11-04
Authors: Laederach, Alain; Andreotti, Amy; Fulton, Donald
Assembly members:
Tachyplesin I, alanine mutant, polymer, 17 residues, Formula weight is not available
Natural source: Common Name: Horseshoe crab Taxonomy ID: 6853 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Tachypleus tridentatus
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
Tachyplesin I, alanine mutant: KWAFRVAYRGIAYRRAR
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 51 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Tachyplesin I, alanine mutant | 1 |
Entities:
Entity 1, Tachyplesin I, alanine mutant 17 residues - Formula weight is not available
| 1 | LYS | TRP | ALA | PHE | ARG | VAL | ALA | TYR | ARG | GLY | ||||
| 2 | ILE | ALA | TYR | ARG | ARG | ALA | ARG |
Samples:
water_sample: Tachyplesin I, alanine mutant0.5 – 1.0 mM; TFA 0.15%
condition_Water_4C: pH: 3.0; temperature: 277 K; ionic strength: 0.0015 %
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | not available | not available | not available |
| 2D 1H-1H TOCSY | not available | not available | not available |
| 2D 1H-1H ROESY | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Bruker DRX 500 MHz