Content for NMR-STAR saveframe, "assigned_chem_shift_list_1"
save_assigned_chem_shift_list_1
_Assigned_chem_shift_list.Sf_category assigned_chemical_shifts
_Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1
_Assigned_chem_shift_list.Entry_ID 25116
_Assigned_chem_shift_list.ID 1
_Assigned_chem_shift_list.Sample_condition_list_ID 1
_Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1
_Assigned_chem_shift_list.Chem_shift_reference_ID 1
_Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1
_Assigned_chem_shift_list.Chem_shift_1H_err .
_Assigned_chem_shift_list.Chem_shift_13C_err .
_Assigned_chem_shift_list.Chem_shift_15N_err .
_Assigned_chem_shift_list.Chem_shift_31P_err .
_Assigned_chem_shift_list.Chem_shift_2H_err .
_Assigned_chem_shift_list.Chem_shift_19F_err .
_Assigned_chem_shift_list.Error_derivation_method .
_Assigned_chem_shift_list.Details
;
K-RAS isoleucine C -methyl resonances were first tentatively assigned based on
assignments of T35S H-RAS-GMPPNP (BMRB code: 17610), and then remaining
ambiguous assignments were resolved by mutagenesis of isoleucines 21, 36, 100,
139, and 163 to leucine residues.
The A-RAFRBD isoleucine C -methyl resonance assignments were transferred from BMRB entry: 11265.
;
_Assigned_chem_shift_list.Text_data_format .
_Assigned_chem_shift_list.Text_data .
loop_
_Chem_shift_experiment.Experiment_ID
_Chem_shift_experiment.Experiment_name
_Chem_shift_experiment.Sample_ID
_Chem_shift_experiment.Sample_label
_Chem_shift_experiment.Sample_state
_Chem_shift_experiment.Entry_ID
_Chem_shift_experiment.Assigned_chem_shift_list_ID
1 '2D 1H-13C HMQC' . . . 25116 1
2 '2D 1H-13C HMQC' . . . 25116 1
stop_
loop_
_Atom_chem_shift.ID
_Atom_chem_shift.Assembly_atom_ID
_Atom_chem_shift.Entity_assembly_ID
_Atom_chem_shift.Entity_ID
_Atom_chem_shift.Comp_index_ID
_Atom_chem_shift.Seq_ID
_Atom_chem_shift.Comp_ID
_Atom_chem_shift.Atom_ID
_Atom_chem_shift.Atom_type
_Atom_chem_shift.Atom_isotope_number
_Atom_chem_shift.Val
_Atom_chem_shift.Val_err
_Atom_chem_shift.Assign_fig_of_merit
_Atom_chem_shift.Ambiguity_code
_Atom_chem_shift.Occupancy
_Atom_chem_shift.Resonance_ID
_Atom_chem_shift.Auth_entity_assembly_ID
_Atom_chem_shift.Auth_asym_ID
_Atom_chem_shift.Auth_seq_ID
_Atom_chem_shift.Auth_comp_ID
_Atom_chem_shift.Auth_atom_ID
_Atom_chem_shift.Details
_Atom_chem_shift.Entry_ID
_Atom_chem_shift.Assigned_chem_shift_list_ID
1 . 1 1 23 23 ILE HD11 H 1 0.565 . . 1 . . . B 21 ILE HD . 25116 1
2 . 1 1 23 23 ILE HD12 H 1 0.565 . . 1 . . . B 21 ILE HD . 25116 1
3 . 1 1 23 23 ILE HD13 H 1 0.565 . . 1 . . . B 21 ILE HD . 25116 1
4 . 1 1 23 23 ILE CD1 C 13 10.043 . . 1 . . . B 21 ILE CD1 . 25116 1
5 . 1 1 26 26 ILE HD11 H 1 0.379 . . 1 . . . B 24 ILE HD . 25116 1
6 . 1 1 26 26 ILE HD12 H 1 0.379 . . 1 . . . B 24 ILE HD . 25116 1
7 . 1 1 26 26 ILE HD13 H 1 0.379 . . 1 . . . B 24 ILE HD . 25116 1
8 . 1 1 26 26 ILE CD1 C 13 8.757 . . 1 . . . B 24 ILE CD1 . 25116 1
9 . 1 1 38 38 ILE HD11 H 1 0.550 . . 1 . . . B 36 ILE HD . 25116 1
10 . 1 1 38 38 ILE HD12 H 1 0.550 . . 1 . . . B 36 ILE HD . 25116 1
11 . 1 1 38 38 ILE HD13 H 1 0.550 . . 1 . . . B 36 ILE HD . 25116 1
12 . 1 1 38 38 ILE CD1 C 13 11.108 . . 1 . . . B 36 ILE CD1 . 25116 1
13 . 1 1 48 48 ILE HD11 H 1 0.381 . . 1 . . . B 46 ILE HD . 25116 1
14 . 1 1 48 48 ILE HD12 H 1 0.381 . . 1 . . . B 46 ILE HD . 25116 1
15 . 1 1 48 48 ILE HD13 H 1 0.381 . . 1 . . . B 46 ILE HD . 25116 1
16 . 1 1 48 48 ILE CD1 C 13 12.585 . . 1 . . . B 46 ILE CD1 . 25116 1
17 . 1 1 57 57 ILE HD11 H 1 0.472 . . 1 . . . B 55 ILE HD . 25116 1
18 . 1 1 57 57 ILE HD12 H 1 0.472 . . 1 . . . B 55 ILE HD . 25116 1
19 . 1 1 57 57 ILE HD13 H 1 0.472 . . 1 . . . B 55 ILE HD . 25116 1
20 . 1 1 57 57 ILE CD1 C 13 12.518 . . 1 . . . B 55 ILE CD1 . 25116 1
21 . 1 1 86 86 ILE HD11 H 1 0.705 . . 1 . . . B 84 ILE HD . 25116 1
22 . 1 1 86 86 ILE HD12 H 1 0.705 . . 1 . . . B 84 ILE HD . 25116 1
23 . 1 1 86 86 ILE HD13 H 1 0.705 . . 1 . . . B 84 ILE HD . 25116 1
24 . 1 1 86 86 ILE CD1 C 13 12.648 . . 1 . . . B 84 ILE CD1 . 25116 1
25 . 1 1 95 95 ILE HD11 H 1 0.728 . . 1 . . . B 93 ILE HD . 25116 1
26 . 1 1 95 95 ILE HD12 H 1 0.728 . . 1 . . . B 93 ILE HD . 25116 1
27 . 1 1 95 95 ILE HD13 H 1 0.728 . . 1 . . . B 93 ILE HD . 25116 1
28 . 1 1 95 95 ILE CD1 C 13 6.618 . . 1 . . . B 93 ILE CD1 . 25116 1
29 . 1 1 102 102 ILE HD11 H 1 0.245 . . 1 . . . B 100 ILE HD . 25116 1
30 . 1 1 102 102 ILE HD12 H 1 0.245 . . 1 . . . B 100 ILE HD . 25116 1
31 . 1 1 102 102 ILE HD13 H 1 0.245 . . 1 . . . B 100 ILE HD . 25116 1
32 . 1 1 102 102 ILE CD1 C 13 12.710 . . 1 . . . B 100 ILE CD1 . 25116 1
33 . 1 1 141 141 ILE HD11 H 1 0.835 . . 1 . . . B 139 ILE HD . 25116 1
34 . 1 1 141 141 ILE HD12 H 1 0.835 . . 1 . . . B 139 ILE HD . 25116 1
35 . 1 1 141 141 ILE HD13 H 1 0.835 . . 1 . . . B 139 ILE HD . 25116 1
36 . 1 1 141 141 ILE CD1 C 13 12.698 . . 1 . . . B 139 ILE CD1 . 25116 1
37 . 1 1 144 144 ILE HD11 H 1 0.619 . . 1 . . . B 142 ILE HD . 25116 1
38 . 1 1 144 144 ILE HD12 H 1 0.619 . . 1 . . . B 142 ILE HD . 25116 1
39 . 1 1 144 144 ILE HD13 H 1 0.619 . . 1 . . . B 142 ILE HD . 25116 1
40 . 1 1 144 144 ILE CD1 C 13 11.108 . . 1 . . . B 142 ILE CD1 . 25116 1
41 . 3 3 47 47 ILE HD11 H 1 0.766 . . 1 . . . . 854 ILE HD . 25116 1
42 . 3 3 47 47 ILE HD12 H 1 0.766 . . 1 . . . . 854 ILE HD . 25116 1
43 . 3 3 47 47 ILE HD13 H 1 0.766 . . 1 . . . . 854 ILE HD . 25116 1
44 . 3 3 47 47 ILE CD1 C 13 10.039 . . 1 . . . . 854 ILE CD . 25116 1
45 . 3 3 60 60 ILE HD11 H 1 0.708 . . 1 . . . . 867 ILE HD . 25116 1
46 . 3 3 60 60 ILE HD12 H 1 0.708 . . 1 . . . . 867 ILE HD . 25116 1
47 . 3 3 60 60 ILE HD13 H 1 0.708 . . 1 . . . . 867 ILE HD . 25116 1
48 . 3 3 60 60 ILE CD1 C 13 11.862 . . 1 . . . . 867 ILE CD . 25116 1
49 . 3 3 69 69 ILE HD11 H 1 0.671 . . 1 . . . . 876 ILE HD . 25116 1
50 . 3 3 69 69 ILE HD12 H 1 0.671 . . 1 . . . . 876 ILE HD . 25116 1
51 . 3 3 69 69 ILE HD13 H 1 0.671 . . 1 . . . . 876 ILE HD . 25116 1
52 . 3 3 69 69 ILE CD1 C 13 12.027 . . 1 . . . . 876 ILE CD . 25116 1
stop_
save_