# 1 "/xwin3.5/exp/stan/nmr/lists/pp/SD_noesyprst.DS" ;SD_noesyprst ;avance-version ;2D homonuclear correlation via dipolar coupling ;dipolar coupling may be due to noe or chemical exchange. ;phase sensitive using States-TPPI method ;with presaturation during relaxation delay ; Added frequency list to center spectrum for RNA - 1/23/97 - ELW ;Allows you to center spectrum anywhere. ;Uses a frequency list: ; 1) set the first value to water ; 2) set the second value to the desired center of spectrum in f1 + f2 ; 3) Set o1 to the desired center of spectrum in f2 (needed for DQD) ; changed 3/21/97 - td based on ELW's pp ; changed presat to 'vladi-trick' 03-24-96, td # 1 "/xwin3.5/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance.incl ; ;avance-version (03/02/17) ;$Id: pulseprogram,v 1.1 2021/02/11 15:58:06 bmrbsvc Exp $ # 20 "/xwin3.5/exp/stan/nmr/lists/pp/SD_noesyprst.DS" 2 # 1 "/xwin3.5/exp/stan/nmr/lists/pp/Grad.incl" 1 ;Grad.incl - include file for Gradient Spectroscopy ; ;avance-version (02/05/31) define list EA= ;$Id: pulseprogram,v 1.1 2021/02/11 15:58:06 bmrbsvc Exp $ # 21 "/xwin3.5/exp/stan/nmr/lists/pp/SD_noesyprst.DS" 2 "d11=30m" "d12=20u" "d13=5u" "d16=200u" "l3=(td1/2)" "d0=((in0/2)-(p1*4/3.14159))" "d8=d9-p16-d16" 1 ze 2 d11 3 d11 4 d12 pl9:f1 setnmr2^0 p18*0.8 ph29 d13 p18*0.2 ph30 setnmr2|0 d12 pl1:f1 ;d12 ph1:f1 p1 ph1 d0 p1 ph2 d8 p16:gp1 ;800us d16 p1 ph3 go=2 ph31 d11 wr #0 if #0 ip1 zd lo to 3 times 2 d11 id0 lo to 4 times l3 setnmr2^0 exit ph1 =0 2 ph2 =0 0 0 0 0 0 0 0 2 2 2 2 2 2 2 2 ph3 =0 0 2 2 1 1 3 3 ph29=0 ph30=1 ph31=0 2 2 0 1 3 3 1 2 0 0 2 3 1 1 3 ;pl1 : f1 channel - power level for pulse (default) ;pl9 : f1 channel - power level for presaturation ;p1 : f1 channel - 90 degree high power pulse ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d9 : mixing time ;d11: delay for disk I/O [30 msec] ;d12: delay for power switching [20 usec] ;d13: short delay [3 usec] ;L3: loop for phase sensitive 2D using States-TPPI method: l3 = td1/2 ;in0: 1/(1 * SW) = 2 * DW ;nd0: 1 ;NS: 8 * n ;DS: 16 ;td1: number of experiments ;MC2: States-TPPI ;gpz1 35% sine.100