# 1 "/u/exp/stan/nmr/lists/pp/SD_noe11ezg_SB" ;SD_noe11ezg ;2D NOE with 11echo and gradients ;phase sensitive using States-TPPI ;with presaturation during relaxation delay and mixing time ;the shortest mixing time ~50 ms!!!! otherwise problems with radiation ;damping ;added decoupling, 9/15/94; thorsten ;changed for DRX, 05/01/96; thorsten ;Allows you to center spectrum anywhere. ;Uses a frequency list: ; 1) set the first value to the desired center of spectrum in f1 ; 2) set the second value to water ; 3) set the third value to the desired center of spectrum in f2 ; 4) Set o1 to the desired center of spectrum in f2 (needed for DQD) ;changed 1/21/97 - ELW ;d2 calculation added 3-22-97, td # 1 "/u/exp/stan/nmr/lists/pp//Avance.incl" ;Avance.incl ; ;version 99/08/02 # 21 "/u/exp/stan/nmr/lists/pp/SD_noe11ezg_SB" # 1 "/u/exp/stan/nmr/lists/pp//Grad.incl" ;Grad.incl - include file for Gradient Spectroscopy ;avance-version ;version 99/02/19 define list EA= # 22 "/u/exp/stan/nmr/lists/pp/SD_noe11ezg_SB" "d11=30m" "d16=200u" "l3=td1/2" "d0=(in0/2)-(p1*4/3.14159)" "d8=d9-p16-d16" "d2=1s/(cnst2*4)-(p1*0.667)" 1 ze d11 2 d11 3 d11 pl1:f1 4 d11 setnmr2^0 d1 fq1:f1 ;Center setnmr2|0 p1 ph1 d0 p1 ph2 d8 p16:gp1 ;800us d16 fq1:f1 ;Water 200us p1 ph3 d2 p1 ph6 p16:gp2 d16 p1 ph7 d2 d2 p1 ph8 p16:gp2 d16 fq1:f1 ;Center go=2 ph31 d11 wr #0 if #0 ip1 zd lo to 3 times 2 d11 id0 lo to 4 times l3 setnmr2^0 exit ph1= 0 2 0 2 1 3 1 3 2 0 2 0 3 1 3 1 2 0 2 0 3 1 3 1 0 2 0 2 1 3 1 3 ph2= 0 0 2 2 1 1 3 3 2 2 0 0 3 3 1 1 2 2 0 0 3 3 1 1 0 0 2 2 1 1 3 3 ph3= 0 0 0 0 1 1 1 1 2 2 2 2 3 3 3 3 ph6= 2 2 2 2 3 3 3 3 0 0 0 0 1 1 1 1 ph7= 0 0 0 0 1 1 1 1 2 2 2 2 3 3 3 3 ph8= 2 2 2 2 3 3 3 3 0 0 0 0 1 1 1 1 ph20=0 0 0 0 0 0 0 0 2 2 2 2 2 2 2 2 ph31=0 2 2 0 1 3 3 1 2 0 0 2 3 1 1 3 ;pl1: Proton power level ;p1 : 90 degree proton pulse ;d9 : the mixing time ;d0 : incremented delay (2D) = in0/2-(4/pi*p1) ;d2 : delay for exitation maximum, calculated based ; on cnst2 = offset of first max in Hz ;d11: delay for disk I/O [30 msec] ;gp1: Homospoil during mixing time ;gp2: Watergate gradient ;in0: 1/(SW) ;nd0: 1 ;NS: 2,4 8,16 or 32 * n ;DS: 4 ;td1: number of experiments ;MC2: States-TPPI ; gpz1 35% sine.100 ;gpz2 25% sine.100