# 1 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" ;cosydfesgpph ;avance-version (02/03/07) ;2D homonuclear shift correlation ;with double quantum filter ;phase sensitive ;water suppression using excitation sculpting with gradients ;allowing for presaturation during relaxation delay in cases ; of radiation damping ; ;phasecycle: A. Derome & M. Williamson, J. Magn. Reson. 88, ; 177 - 185 (1990) ;T.-L. Hwang & A.J. Shaka, J. Magn. Reson., ; Series A 112 275-279 (1995) prosol relations= # 1 "/u/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance2.incl ; for 1 ; ;avance-version (03/02/17) ;$Id: pulseprogram,v 1.1 2021/02/11 15:59:21 bmrbsvc Exp $ # 19 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" 2 # 1 "/u/exp/stan/nmr/lists/pp/Grad.incl" 1 ;Grad2.incl - include file for Gradient Spectroscopy ; for 1 ; ;avance-version (02/05/31) define list EA= ;$Id: pulseprogram,v 1.1 2021/02/11 15:59:21 bmrbsvc Exp $ # 20 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" 2 "p2=p1*2" "d11=30m" "d12=20u" "d13=4u" "d0=in0/2-p1*4/3.1416" # 1 "mc_line 36 file /u/exp/stan/nmr/lists/pp/cosydfesgpph expanding definition part of mc command before ze" define delay MCWRK define delay MCREST define loopcounter ST1CNT "ST1CNT = td1 / (2)" "MCWRK = 0.333333*d11" "MCREST = d11 - d11" # 36 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" 1 ze # 1 "mc_line 36 file /u/exp/stan/nmr/lists/pp/cosydfesgpph expanding definition of mc command after ze" # 37 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" # 1 "mc_line 37 file /u/exp/stan/nmr/lists/pp/cosydfesgpph expanding start label for mc command" 2 MCWRK * 2 LBLSTS1, MCWRK LBLF1, MCREST # 38 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" 3 d12 pl9:f1 d1 cw:f1 ph29 d13 do:f1 d12 pl1:f1 p1 ph1 d0 p1 ph2 d13 p1 ph3 50u setnmr3|0 setnmr0|34|32|33 p16:gp1 d16 pl0:f1 (p12:sp1 ph4:r):f1 4u d12 pl1:f1 p2 ph5 4u p16:gp1 d16 50u p16:gp2 d16 pl0:f1 (p12:sp1 ph6:r):f1 4u d12 pl1:f1 p2 ph7 4u p16:gp2 d16 4u setnmr3^0 setnmr0^34^32^33 go=2 ph31 # 1 "mc_line 75 file /u/exp/stan/nmr/lists/pp/cosydfesgpph expanding mc command in line" MCWRK wr #0 if #0 zd ip1 MCWRK ip29 lo to LBLSTS1 times 2 MCWRK id0 lo to LBLF1 times ST1CNT # 76 "/u/exp/stan/nmr/lists/pp/cosydfesgpph" exit ph1=1 1 1 1 1 1 1 1 0 0 0 0 0 0 0 0 ph2=0 0 0 0 0 0 0 0 1 1 1 1 1 1 1 1 ph3=1 2 3 0 1 2 3 0 2 3 0 1 2 3 0 1 ph4=0 0 0 0 1 1 1 1 1 1 1 1 2 2 2 2 ph5=2 2 2 2 3 3 3 3 3 3 3 3 0 0 0 0 ph6=0 0 0 0 0 0 0 0 1 1 1 1 1 1 1 1 ph7=2 2 2 2 2 2 2 2 3 3 3 3 3 3 3 3 ph29=0 0 0 0 0 0 0 0 1 1 1 1 1 1 1 1 ph31=0 3 2 1 2 1 0 3 3 2 1 0 1 0 3 2 ;pl0 : 120dB ;pl1 : f1 channel - power level for pulse (default) ;pl9 : f1 channel - power level for presaturation ;sp1 : f1 channel - shaped pulse 180 degree ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p12: f1 channel - 180 degree shaped pulse (Squa100.1000) [2 msec] ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) ;d1 : relaxation delay; 1-5 * T1 ;d11: delay for disk I/O [30 msec] ;d12: delay for power switching [20 usec] ;d13: short delay [4 usec] ;d16: delay for homospoil/gradient recovery ;in0: 1/(1 * SW) = 2 * DW ;nd0: 1 ;NS: 16 * n ;DS: 16 ;td1: number of experiments ;FnMODE: States-TPPI, TPPI, States or QSEC ;use gradient ratio: gp 1 : gp 2 ; 31 : 11 ;for z-only gradients: ;gpz1: 31% ;gpz2: 11% ;use gradient files: ;gpnam1: SINE.100 ;gpnam2: SINE.100 ;set pl9 to 120dB when presaturation is not required ; use 75 - 80dB to reduce radiation damping ;Processing ;PHC0(F1): 90 ;PHC1(F1): -180 ;FCOR(F1): 1 ;$Id: pulseprogram,v 1.1 2021/02/11 15:59:21 bmrbsvc Exp $