data_50196 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; Backbone chemical shifts of E2A residues 1-100 ; _BMRB_accession_number 50196 _BMRB_flat_file_name bmr50196.str _Entry_type original _Submission_date 2020-02-13 _Accession_date 2020-02-13 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details 'The backbone chemical shifts of E2A residues 1-100' loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Langelaan David N. . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 1 spectral_peak_list 1 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 124 "13C chemical shifts" 295 "15N chemical shifts" 93 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2020-07-13 update BMRB 'update entry citation' 2020-02-24 original author 'original release' stop_ _Original_release_date 2020-02-18 save_ ############################# # Citation for this entry # ############################# save_citations_1 _Saveframe_category entry_citation _Citation_full . _Citation_title ; Structural insights into TAZ2 domain-mediated CBP/p300 recruitment by transactivation domain 1 of the lymphopoietic transcription factor E2A ; _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 32098872 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Lochhead Marina R. . 2 Brown Alexandra D. . 3 Kirlin Alyssa C. . 4 Chitayat Seth . . 5 Munro Kim . . 6 Findlay Jane E. . 7 Baillie George S. . 8 LeBrun David P. . 9 Langelaan David N. . 10 Smith Steven P. . stop_ _Journal_abbreviation 'J. Biol. Chem.' _Journal_name_full 'The Journal of biological chemistry' _Journal_volume 295 _Journal_issue 13 _Journal_ISSN 1083-351X _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 4303 _Page_last 4315 _Year 2020 _Details . loop_ _Keyword E2A Taz2 'solution NMR' 'transcription factor' stop_ save_ ################################## # Molecular system description # ################################## save_assembly_1 _Saveframe_category molecular_system _Mol_system_name 'E2A residues 1-100' _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label E2A:1-100 $entity_1 stop_ _System_molecular_weight 10486.3478 _System_physical_state 'intrinsically disordered' _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_entity_1 _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common entity_1 _Molecular_mass 10486.3478 _Mol_thiol_state 'not present' loop_ _Biological_function 'Transcription factor' stop_ _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 102 _Mol_residue_sequence ; GSMNQPQRMAPVGTDKELSD LLDFSMMFPLPVTNGKGRPA SLAGAQFGGSGLEDRPSSGS WGSGDQSSSSFDPSRTFSEG THFTESHSSLSSSTFLGPGL GG ; loop_ _Residue_seq_code _Residue_label 1 GLY 2 SER 3 MET 4 ASN 5 GLN 6 PRO 7 GLN 8 ARG 9 MET 10 ALA 11 PRO 12 VAL 13 GLY 14 THR 15 ASP 16 LYS 17 GLU 18 LEU 19 SER 20 ASP 21 LEU 22 LEU 23 ASP 24 PHE 25 SER 26 MET 27 MET 28 PHE 29 PRO 30 LEU 31 PRO 32 VAL 33 THR 34 ASN 35 GLY 36 LYS 37 GLY 38 ARG 39 PRO 40 ALA 41 SER 42 LEU 43 ALA 44 GLY 45 ALA 46 GLN 47 PHE 48 GLY 49 GLY 50 SER 51 GLY 52 LEU 53 GLU 54 ASP 55 ARG 56 PRO 57 SER 58 SER 59 GLY 60 SER 61 TRP 62 GLY 63 SER 64 GLY 65 ASP 66 GLN 67 SER 68 SER 69 SER 70 SER 71 PHE 72 ASP 73 PRO 74 SER 75 ARG 76 THR 77 PHE 78 SER 79 GLU 80 GLY 81 THR 82 HIS 83 PHE 84 THR 85 GLU 86 SER 87 HIS 88 SER 89 SER 90 LEU 91 SER 92 SER 93 SER 94 THR 95 PHE 96 LEU 97 GLY 98 PRO 99 GLY 100 LEU 101 GLY 102 GLY stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source_1 _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $entity_1 Human 9606 Eukaryota Metazoa Homo sapiens stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_type _Vector_name $entity_1 'recombinant technology' . Escherichia coli . plasmid 'pET 21' stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type solution _Details 'pH 6.0' loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $entity_1 1 mM '[U-13C; U-15N]' D2O 5 '% v/v' '[U-100% 2H]' 'sodium chloride' 50 mM 'natural abundance' MES 20 mM 'natural abundance' stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Saveframe_category software _Name 'CcpNmr Analysis' _Version 2.4 loop_ _Task collection 'data analysis' processing stop_ _Details 'The CCPN NMR assignment and data analysis application' save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 600 _Details . save_ ############################# # NMR applied experiments # ############################# save_2D_1H-15N_HSQC/HMQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC/HMQC' _Sample_label $sample_1 save_ save_3D_HNCO_2 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCO' _Sample_label $sample_1 save_ save_3D_CBCA(CO)NH_3 _Saveframe_category NMR_applied_experiment _Experiment_name '3D CBCA(CO)NH' _Sample_label $sample_1 save_ save_3D_HNCACB_4 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCACB' _Sample_label $sample_1 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 50 . mM pH 6 . pH pressure 1 . atm temperature 298 . K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Saveframe_category chemical_shift_reference _Details . loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio water C 13 protons ppm 4.782 internal indirect . . . 0.25144953 water H 1 protons ppm 4.782 internal direct . . . 1 water N 15 protons ppm 4.782 internal indirect . . . 0.101329118 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Saveframe_category assigned_chemical_shifts _Details . loop_ _Experiment_label '2D 1H-15N HSQC/HMQC' '3D HNCO' '3D CBCA(CO)NH' '3D HNCACB' stop_ loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Chem_shift_reference_set_label $chem_shift_reference_1 _Mol_system_component_name E2A:1-100 _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 2 2 SER C C 174.602 0.005 1 2 2 2 SER CA C 58.439 . 1 3 2 2 SER CB C 63.989 . 1 4 3 3 MET H H 8.585 0.0 1 5 3 3 MET C C 175.906 0.004 1 6 3 3 MET CA C 55.675 0.021 1 7 3 3 MET CB C 32.687 . 1 8 3 3 MET N N 122.017 0.003 1 9 4 4 ASN H H 8.460 0.001 1 10 4 4 ASN C C 174.651 0.004 1 11 4 4 ASN CA C 53.321 0.027 1 12 4 4 ASN CB C 38.882 0.042 1 13 4 4 ASN N N 119.720 0.002 1 14 5 5 GLN H H 8.253 0.0 1 15 5 5 GLN HE21 H 6.880 . 1 16 5 5 GLN HE22 H 7.517 . 1 17 5 5 GLN C C 173.855 . 1 18 5 5 GLN CA C 53.742 . 1 19 5 5 GLN CB C 29.120 . 1 20 5 5 GLN N N 121.303 0.005 1 21 5 5 GLN NE2 N 112.397 0.0 1 22 6 6 PRO C C 176.808 0.007 1 23 6 6 PRO CA C 63.280 0.012 1 24 6 6 PRO CB C 32.155 0.022 1 25 7 7 GLN H H 8.508 0.001 1 26 7 7 GLN HE21 H 7.544 . 1 27 7 7 GLN HE22 H 6.888 . 1 28 7 7 GLN C C 175.872 0.008 1 29 7 7 GLN CA C 55.872 0.055 1 30 7 7 GLN CB C 29.570 0.077 1 31 7 7 GLN N N 120.689 0.014 1 32 7 7 GLN NE2 N 112.640 0.001 1 33 8 8 ARG H H 8.377 0.0 1 34 8 8 ARG HA H 4.324 0.002 1 35 8 8 ARG HB2 H 1.751 0.006 2 36 8 8 ARG HB3 H 1.827 0.007 2 37 8 8 ARG HG2 H 1.608 0.0 1 38 8 8 ARG HD2 H 3.181 0.0 1 39 8 8 ARG C C 175.978 0.015 1 40 8 8 ARG CA C 56.063 0.031 1 41 8 8 ARG CB C 30.918 0.017 1 42 8 8 ARG CG C 27.170 0.01 1 43 8 8 ARG CD C 43.399 0.016 1 44 8 8 ARG N N 122.529 0.009 1 45 9 9 MET H H 8.428 0.002 1 46 9 9 MET C C 175.376 0.005 1 47 9 9 MET CA C 55.111 0.002 1 48 9 9 MET CB C 33.106 0.031 1 49 9 9 MET N N 122.181 0.01 1 50 10 10 ALA H H 8.290 0.001 1 51 10 10 ALA HA H 4.568 . 1 52 10 10 ALA HB H 1.351 . 1 53 10 10 ALA C C 175.340 . 1 54 10 10 ALA CA C 50.497 0.012 1 55 10 10 ALA CB C 18.297 0.028 1 56 10 10 ALA N N 126.649 0.007 1 57 11 11 PRO C C 176.869 0.004 1 58 11 11 PRO CA C 62.896 . 1 59 11 11 PRO CB C 32.000 . 1 60 12 12 VAL H H 8.276 0.0 1 61 12 12 VAL HA H 4.124 0.001 1 62 12 12 VAL HB H 2.074 0.001 1 63 12 12 VAL HG1 H 0.965 0.0 2 64 12 12 VAL HG2 H 0.966 0.0 2 65 12 12 VAL C C 176.752 0.014 1 66 12 12 VAL CA C 62.442 0.051 1 67 12 12 VAL CB C 32.941 0.023 1 68 12 12 VAL CG1 C 20.562 0.01 2 69 12 12 VAL CG2 C 21.215 0.003 2 70 12 12 VAL N N 120.350 0.004 1 71 13 13 GLY H H 8.534 0.002 1 72 13 13 GLY C C 174.422 0.004 1 73 13 13 GLY CA C 45.353 0.016 1 74 13 13 GLY N N 112.485 0.004 1 75 14 14 THR H H 8.094 0.0 1 76 14 14 THR C C 174.468 0.009 1 77 14 14 THR CA C 61.899 0.022 1 78 14 14 THR CB C 69.860 0.016 1 79 14 14 THR CG2 C 21.566 . 1 80 14 14 THR N N 113.091 0.004 1 81 15 15 ASP H H 8.461 0.002 1 82 15 15 ASP C C 176.468 0.006 1 83 15 15 ASP CA C 54.788 0.011 1 84 15 15 ASP CB C 40.931 0.037 1 85 15 15 ASP N N 122.308 0.004 1 86 16 16 LYS H H 8.188 0.0 1 87 16 16 LYS C C 176.686 0.006 1 88 16 16 LYS CA C 56.726 0.004 1 89 16 16 LYS CB C 33.025 0.03 1 90 16 16 LYS N N 121.452 0.004 1 91 17 17 GLU H H 8.378 0.001 1 92 17 17 GLU C C 176.956 0.007 1 93 17 17 GLU CA C 57.047 0.006 1 94 17 17 GLU CB C 29.991 0.019 1 95 17 17 GLU N N 121.014 0.006 1 96 18 18 LEU H H 8.196 0.001 1 97 18 18 LEU C C 177.743 0.003 1 98 18 18 LEU CA C 55.644 0.02 1 99 18 18 LEU CB C 42.180 0.066 1 100 18 18 LEU N N 122.213 0.006 1 101 19 19 SER H H 8.195 0.001 1 102 19 19 SER C C 174.704 0.009 1 103 19 19 SER CA C 59.009 0.017 1 104 19 19 SER CB C 63.792 0.013 1 105 19 19 SER N N 115.678 0.006 1 106 20 20 ASP H H 8.307 0.0 1 107 20 20 ASP C C 176.371 0.004 1 108 20 20 ASP CA C 54.865 0.011 1 109 20 20 ASP CB C 40.950 0.016 1 110 20 20 ASP N N 122.024 0.006 1 111 21 21 LEU H H 7.971 0.0 1 112 21 21 LEU C C 177.483 0.005 1 113 21 21 LEU CA C 55.630 0.005 1 114 21 21 LEU CB C 42.267 0.019 1 115 21 21 LEU N N 121.208 0.004 1 116 22 22 LEU H H 8.011 0.0 1 117 22 22 LEU C C 176.857 0.002 1 118 22 22 LEU CA C 55.387 0.025 1 119 22 22 LEU CB C 42.337 0.009 1 120 22 22 LEU N N 121.799 0.003 1 121 23 23 ASP H H 8.063 0.001 1 122 23 23 ASP C C 176.545 0.001 1 123 23 23 ASP CA C 54.142 0.003 1 124 23 23 ASP CB C 41.215 0.015 1 125 23 23 ASP N N 120.258 0.004 1 126 24 24 PHE H H 8.280 0.001 1 127 24 24 PHE C C 176.558 . 1 128 24 24 PHE CA C 58.781 0.007 1 129 24 24 PHE CB C 39.259 . 1 130 24 24 PHE N N 121.988 0.002 1 131 25 25 SER H H 8.314 0.001 1 132 25 25 SER C C 174.881 0.006 1 133 25 25 SER CA C 59.847 0.029 1 134 25 25 SER CB C 63.545 0.007 1 135 25 25 SER N N 116.138 0.009 1 136 26 26 MET H H 7.984 0.002 1 137 26 26 MET C C 176.057 0.004 1 138 26 26 MET CA C 55.651 0.029 1 139 26 26 MET CB C 32.435 . 1 140 26 26 MET N N 120.452 0.001 1 141 27 27 MET H H 7.894 0.0 1 142 27 27 MET C C 175.352 0.005 1 143 27 27 MET CA C 55.836 0.016 1 144 27 27 MET CB C 33.074 0.029 1 145 27 27 MET N N 119.558 0.002 1 146 28 28 PHE H H 7.969 0.001 1 147 28 28 PHE C C 173.349 . 1 148 28 28 PHE CA C 55.317 . 1 149 28 28 PHE CB C 39.242 . 1 150 28 28 PHE N N 120.381 0.005 1 151 29 29 PRO C C 176.607 0.002 1 152 29 29 PRO CA C 62.999 0.009 1 153 29 29 PRO CB C 31.966 . 1 154 30 30 LEU H H 8.215 0.001 1 155 30 30 LEU C C 175.494 . 1 156 30 30 LEU CA C 53.108 . 1 157 30 30 LEU CB C 41.911 . 1 158 30 30 LEU N N 123.457 0.009 1 159 31 31 PRO C C 176.905 0.009 1 160 31 31 PRO CA C 63.024 . 1 161 31 31 PRO CB C 31.958 . 1 162 32 32 VAL H H 8.237 0.001 1 163 32 32 VAL HA H 4.174 0.0 1 164 32 32 VAL HB H 2.087 0.004 1 165 32 32 VAL HG1 H 0.945 0.0 2 166 32 32 VAL HG2 H 0.943 0.001 2 167 32 32 VAL C C 176.616 0.003 1 168 32 32 VAL CA C 62.353 0.018 1 169 32 32 VAL CB C 32.783 0.02 1 170 32 32 VAL CG1 C 20.498 0.018 2 171 32 32 VAL CG2 C 21.295 0.01 2 172 32 32 VAL N N 120.209 0.016 1 173 33 33 THR H H 8.228 0.001 1 174 33 33 THR C C 174.336 0.015 1 175 33 33 THR CA C 61.610 0.021 1 176 33 33 THR CB C 69.881 0.011 1 177 33 33 THR CG2 C 21.538 . 1 178 33 33 THR N N 117.225 0.024 1 179 34 34 ASN H H 8.449 0.001 1 180 34 34 ASN C C 175.686 0.006 1 181 34 34 ASN CA C 53.384 0.014 1 182 34 34 ASN CB C 38.941 0.023 1 183 34 34 ASN N N 121.028 0.019 1 184 35 35 GLY H H 8.411 0.0 1 185 35 35 GLY C C 174.224 0.007 1 186 35 35 GLY CA C 45.568 0.005 1 187 35 35 GLY N N 109.168 0.011 1 188 36 36 LYS H H 8.168 0.001 1 189 36 36 LYS C C 177.051 0.019 1 190 36 36 LYS CA C 56.303 0.014 1 191 36 36 LYS CB C 32.926 0.05 1 192 36 36 LYS N N 120.484 0.004 1 193 37 37 GLY H H 8.410 0.003 1 194 37 37 GLY C C 173.607 0.004 1 195 37 37 GLY CA C 45.120 0.029 1 196 37 37 GLY N N 109.645 0.02 1 197 38 38 ARG H H 8.151 0.001 1 198 38 38 ARG C C 174.247 . 1 199 38 38 ARG CA C 53.994 . 1 200 38 38 ARG CB C 30.344 . 1 201 38 38 ARG N N 121.464 0.003 1 202 39 39 PRO C C 176.738 0.004 1 203 39 39 PRO CA C 63.143 0.002 1 204 39 39 PRO CB C 32.104 0.001 1 205 40 40 ALA H H 8.473 0.0 1 206 40 40 ALA HA H 4.260 . 1 207 40 40 ALA HB H 1.388 0.001 1 208 40 40 ALA C C 177.963 0.012 1 209 40 40 ALA CA C 52.896 0.01 1 210 40 40 ALA CB C 19.185 0.037 1 211 40 40 ALA N N 124.498 0.005 1 212 41 41 SER H H 8.214 0.001 1 213 41 41 SER C C 174.634 0.002 1 214 41 41 SER CA C 58.198 0.013 1 215 41 41 SER CB C 63.790 0.011 1 216 41 41 SER N N 114.147 0.012 1 217 42 42 LEU H H 8.215 0.002 1 218 42 42 LEU C C 177.136 0.007 1 219 42 42 LEU CA C 55.193 0.021 1 220 42 42 LEU CB C 42.305 0.031 1 221 42 42 LEU N N 124.152 0.021 1 222 43 43 ALA H H 8.202 0.004 1 223 43 43 ALA HA H 4.269 0.006 1 224 43 43 ALA HB H 1.374 0.0 1 225 43 43 ALA C C 178.196 0.004 1 226 43 43 ALA CA C 52.905 0.025 1 227 43 43 ALA CB C 19.170 0.033 1 228 43 43 ALA N N 124.300 0.036 1 229 44 44 GLY H H 8.294 0.001 1 230 44 44 GLY C C 174.102 0.006 1 231 44 44 GLY CA C 45.331 0.019 1 232 44 44 GLY N N 107.973 0.003 1 233 45 45 ALA H H 8.078 0.0 1 234 45 45 ALA HA H 4.264 0.002 1 235 45 45 ALA HB H 1.341 0.004 1 236 45 45 ALA C C 177.754 0.004 1 237 45 45 ALA CA C 52.686 0.005 1 238 45 45 ALA CB C 19.333 0.024 1 239 45 45 ALA N N 123.573 0.002 1 240 46 46 GLN H H 8.346 0.001 1 241 46 46 GLN HE21 H 7.416 . 1 242 46 46 GLN HE22 H 6.824 . 1 243 46 46 GLN C C 175.744 0.005 1 244 46 46 GLN CA C 55.962 0.009 1 245 46 46 GLN CB C 29.386 0.021 1 246 46 46 GLN N N 119.040 0.002 1 247 46 46 GLN NE2 N 112.392 0.0 1 248 47 47 PHE H H 8.238 0.001 1 249 47 47 PHE C C 176.252 0.005 1 250 47 47 PHE CA C 57.756 0.025 1 251 47 47 PHE CB C 39.598 0.021 1 252 47 47 PHE N N 120.900 0.001 1 253 48 48 GLY H H 8.340 0.001 1 254 48 48 GLY C C 174.549 0.004 1 255 48 48 GLY CA C 45.445 0.026 1 256 48 48 GLY N N 110.729 0.004 1 257 49 49 GLY H H 8.031 0.001 1 258 49 49 GLY C C 174.288 0.002 1 259 49 49 GLY CA C 45.307 0.026 1 260 49 49 GLY N N 108.518 0.003 1 261 50 50 SER H H 8.411 0.001 1 262 50 50 SER C C 175.177 0.004 1 263 50 50 SER CA C 58.575 0.02 1 264 50 50 SER CB C 64.060 0.021 1 265 50 50 SER N N 115.742 0.004 1 266 51 51 GLY H H 8.595 0.0 1 267 51 51 GLY C C 174.258 0.016 1 268 51 51 GLY CA C 45.439 0.056 1 269 51 51 GLY N N 111.121 0.002 1 270 52 52 LEU H H 8.109 0.001 1 271 52 52 LEU C C 177.553 . 1 272 52 52 LEU CA C 55.283 0.037 1 273 52 52 LEU CB C 42.437 0.031 1 274 52 52 LEU N N 121.387 0.033 1 275 53 53 GLU H H 8.491 0.0 1 276 53 53 GLU C C 176.061 . 1 277 53 53 GLU CA C 56.731 0.02 1 278 53 53 GLU CB C 30.162 0.005 1 279 53 53 GLU N N 120.680 0.001 1 280 54 54 ASP H H 8.286 0.0 1 281 54 54 ASP C C 175.666 0.004 1 282 54 54 ASP CA C 54.271 0.007 1 283 54 54 ASP CB C 41.092 0.044 1 284 54 54 ASP N N 121.233 0.004 1 285 55 55 ARG H H 8.104 0.001 1 286 55 55 ARG C C 174.033 . 1 287 55 55 ARG CA C 53.966 . 1 288 55 55 ARG CB C 30.410 . 1 289 55 55 ARG N N 121.660 0.004 1 290 56 56 PRO C C 177.180 0.003 1 291 56 56 PRO CA C 63.138 0.049 1 292 56 56 PRO CB C 32.149 0.025 1 293 57 57 SER H H 8.508 0.001 1 294 57 57 SER C C 174.870 0.008 1 295 57 57 SER CA C 58.538 0.031 1 296 57 57 SER CB C 63.821 0.005 1 297 57 57 SER N N 116.345 0.004 1 298 58 58 SER H H 8.305 0.003 1 299 58 58 SER C C 174.918 0.029 1 300 58 58 SER CA C 58.518 0.013 1 301 58 58 SER CB C 63.868 0.031 1 302 58 58 SER N N 117.333 0.083 1 303 59 59 GLY H H 8.300 0.001 1 304 59 59 GLY C C 174.017 0.006 1 305 59 59 GLY CA C 45.352 0.015 1 306 59 59 GLY N N 110.374 0.01 1 307 60 60 SER H H 8.089 0.0 1 308 60 60 SER C C 174.298 0.006 1 309 60 60 SER CA C 58.193 0.004 1 310 60 60 SER CB C 63.800 0.026 1 311 60 60 SER N N 115.451 0.006 1 312 61 61 TRP H H 8.195 0.002 1 313 61 61 TRP C C 176.728 0.003 1 314 61 61 TRP CA C 57.587 0.067 1 315 61 61 TRP CB C 29.687 0.021 1 316 61 61 TRP N N 122.978 0.024 1 317 62 62 GLY H H 8.267 0.0 1 318 62 62 GLY C C 174.123 0.004 1 319 62 62 GLY CA C 45.398 0.016 1 320 62 62 GLY N N 110.729 0.003 1 321 63 63 SER H H 8.181 0.001 1 322 63 63 SER C C 175.162 0.008 1 323 63 63 SER CA C 58.506 0.01 1 324 63 63 SER CB C 63.945 0.003 1 325 63 63 SER N N 115.525 0.004 1 326 64 64 GLY H H 8.462 0.0 1 327 64 64 GLY C C 173.974 0.004 1 328 64 64 GLY CA C 45.447 0.013 1 329 64 64 GLY N N 110.796 0.003 1 330 65 65 ASP H H 8.221 0.001 1 331 65 65 ASP C C 176.585 0.009 1 332 65 65 ASP CA C 54.419 0.06 1 333 65 65 ASP CB C 41.214 0.032 1 334 65 65 ASP N N 120.451 0.006 1 335 66 66 GLN H H 8.424 0.0 1 336 66 66 GLN HE21 H 6.792 . 1 337 66 66 GLN HE22 H 7.449 . 1 338 66 66 GLN C C 176.319 0.008 1 339 66 66 GLN CA C 56.120 0.017 1 340 66 66 GLN CB C 29.141 0.034 1 341 66 66 GLN N N 120.887 0.006 1 342 66 66 GLN NE2 N 112.456 0.001 1 343 67 67 SER H H 8.376 0.0 1 344 67 67 SER C C 174.920 . 1 345 67 67 SER CA C 58.902 . 1 346 67 67 SER CB C 63.813 . 1 347 67 67 SER N N 116.545 0.008 1 348 69 69 SER C C 174.578 . 1 349 69 69 SER CA C 58.480 . 1 350 69 69 SER CB C 63.818 . 1 351 70 70 SER H H 8.200 0.0 1 352 70 70 SER C C 173.870 0.011 1 353 70 70 SER CA C 58.459 . 1 354 70 70 SER CB C 63.790 0.024 1 355 70 70 SER N N 117.356 0.002 1 356 71 71 PHE H H 8.102 0.0 1 357 71 71 PHE C C 174.538 0.006 1 358 71 71 PHE CA C 57.705 0.005 1 359 71 71 PHE CB C 39.786 0.017 1 360 71 71 PHE N N 122.087 0.005 1 361 72 72 ASP H H 8.088 0.001 1 362 72 72 ASP C C 174.760 . 1 363 72 72 ASP CA C 51.211 . 1 364 72 72 ASP CB C 41.746 . 1 365 72 72 ASP N N 124.159 0.003 1 366 73 73 PRO C C 177.321 0.001 1 367 73 73 PRO CA C 63.810 . 1 368 73 73 PRO CB C 32.131 0.009 1 369 74 74 SER H H 8.375 0.0 1 370 74 74 SER C C 174.847 0.007 1 371 74 74 SER CA C 59.534 0.018 1 372 74 74 SER CB C 63.593 0.034 1 373 74 74 SER N N 114.858 0.003 1 374 75 75 ARG H H 7.759 0.0 1 375 75 75 ARG HA H 4.331 0.002 1 376 75 75 ARG HB2 H 1.836 0.004 2 377 75 75 ARG HB3 H 1.711 0.003 2 378 75 75 ARG HG2 H 1.510 0.0 2 379 75 75 ARG HG3 H 1.552 0.0 2 380 75 75 ARG HD2 H 3.127 0.001 1 381 75 75 ARG C C 176.179 0.004 1 382 75 75 ARG CA C 56.183 0.013 1 383 75 75 ARG CB C 30.686 0.026 1 384 75 75 ARG CG C 27.085 0.005 1 385 75 75 ARG CD C 43.317 0.003 1 386 75 75 ARG N N 122.029 0.004 1 387 76 76 THR H H 7.948 0.002 1 388 76 76 THR C C 174.306 0.008 1 389 76 76 THR CA C 62.163 0.028 1 390 76 76 THR CB C 69.824 0.005 1 391 76 76 THR CG2 C 21.560 . 1 392 76 76 THR N N 114.666 0.005 1 393 77 77 PHE H H 8.251 0.002 1 394 77 77 PHE C C 175.787 0.005 1 395 77 77 PHE CA C 57.773 0.034 1 396 77 77 PHE CB C 39.624 0.01 1 397 77 77 PHE N N 122.308 0.004 1 398 78 78 SER H H 8.197 0.001 1 399 78 78 SER C C 174.397 0.005 1 400 78 78 SER CA C 58.335 0.033 1 401 78 78 SER CB C 63.907 0.043 1 402 78 78 SER N N 117.323 0.012 1 403 79 79 GLU H H 8.423 0.0 1 404 79 79 GLU C C 176.965 0.006 1 405 79 79 GLU CA C 56.976 0.016 1 406 79 79 GLU CB C 30.223 0.037 1 407 79 79 GLU N N 122.924 0.003 1 408 80 80 GLY H H 8.385 0.001 1 409 80 80 GLY C C 174.308 0.005 1 410 80 80 GLY CA C 45.373 0.011 1 411 80 80 GLY N N 109.513 0.016 1 412 81 81 THR H H 7.965 0.001 1 413 81 81 THR C C 174.360 . 1 414 81 81 THR CA C 61.995 0.008 1 415 81 81 THR CB C 69.766 0.001 1 416 81 81 THR N N 113.375 0.01 1 417 82 82 HIS H H 8.435 0.002 1 418 82 82 HIS C C 174.169 0.003 1 419 82 82 HIS CA C 55.351 0.005 1 420 82 82 HIS CB C 29.250 . 1 421 82 82 HIS N N 120.852 0.0 1 422 83 83 PHE H H 8.301 0.001 1 423 83 83 PHE C C 175.854 0.004 1 424 83 83 PHE CA C 58.081 0.028 1 425 83 83 PHE CB C 39.675 0.029 1 426 83 83 PHE N N 122.029 0.003 1 427 84 84 THR H H 8.128 0.0 1 428 84 84 THR C C 174.169 0.008 1 429 84 84 THR CA C 61.839 . 1 430 84 84 THR CB C 69.900 0.019 1 431 84 84 THR CG2 C 21.601 . 1 432 84 84 THR N N 116.194 0.004 1 433 85 85 GLU H H 8.382 0.001 1 434 85 85 GLU C C 176.363 0.005 1 435 85 85 GLU CA C 56.696 0.031 1 436 85 85 GLU CB C 30.346 0.035 1 437 85 85 GLU N N 123.382 0.005 1 438 86 86 SER H H 8.335 0.0 1 439 86 86 SER C C 174.508 . 1 440 86 86 SER CA C 58.415 0.001 1 441 86 86 SER CB C 63.783 0.072 1 442 86 86 SER N N 116.746 0.014 1 443 87 87 HIS H H 8.514 0.001 1 444 87 87 HIS N N 120.755 0.032 1 445 88 88 SER C C 174.642 . 1 446 88 88 SER CA C 58.455 . 1 447 88 88 SER CB C 63.901 . 1 448 89 89 SER H H 8.469 0.0 1 449 89 89 SER C C 174.619 0.008 1 450 89 89 SER CA C 58.508 0.028 1 451 89 89 SER CB C 63.746 0.035 1 452 89 89 SER N N 118.172 0.006 1 453 90 90 LEU H H 8.266 0.0 1 454 90 90 LEU C C 177.610 0.004 1 455 90 90 LEU CA C 55.448 0.009 1 456 90 90 LEU CB C 42.344 0.034 1 457 90 90 LEU N N 123.778 0.006 1 458 91 91 SER H H 8.274 0.001 1 459 91 91 SER C C 174.713 0.01 1 460 91 91 SER CA C 58.421 . 1 461 91 91 SER CB C 63.758 0.001 1 462 91 91 SER N N 116.197 0.004 1 463 92 92 SER H H 8.308 0.0 1 464 92 92 SER C C 174.757 . 1 465 92 92 SER CA C 58.601 . 1 466 92 92 SER CB C 63.848 . 1 467 92 92 SER N N 117.598 0.001 1 468 93 93 SER H H 8.335 0.002 1 469 93 93 SER C C 174.677 0.006 1 470 93 93 SER CA C 58.616 0.026 1 471 93 93 SER CB C 63.825 0.047 1 472 93 93 SER N N 117.607 0.004 1 473 94 94 THR H H 8.062 0.001 1 474 94 94 THR C C 174.086 0.007 1 475 94 94 THR CA C 62.141 0.031 1 476 94 94 THR CB C 69.682 0.011 1 477 94 94 THR CG2 C 21.538 . 1 478 94 94 THR N N 115.777 0.009 1 479 95 95 PHE H H 8.179 0.002 1 480 95 95 PHE C C 175.282 0.007 1 481 95 95 PHE CA C 57.793 0.034 1 482 95 95 PHE CB C 39.564 0.021 1 483 95 95 PHE N N 122.809 0.004 1 484 96 96 LEU H H 8.149 0.0 1 485 96 96 LEU C C 176.945 0.004 1 486 96 96 LEU CA C 54.846 0.002 1 487 96 96 LEU CB C 42.754 0.038 1 488 96 96 LEU N N 124.662 0.006 1 489 97 97 GLY H H 7.660 0.0 1 490 97 97 GLY C C 171.580 . 1 491 97 97 GLY CA C 44.626 . 1 492 97 97 GLY N N 108.917 0.003 1 493 98 98 PRO C C 177.767 0.006 1 494 98 98 PRO CA C 63.463 0.006 1 495 98 98 PRO CB C 32.113 . 1 496 99 99 GLY H H 8.510 0.001 1 497 99 99 GLY C C 174.315 0.0 1 498 99 99 GLY CA C 45.385 0.0 1 499 99 99 GLY N N 109.511 0.003 1 500 100 100 LEU H H 8.108 0.001 1 501 100 100 LEU C C 177.864 0.005 1 502 100 100 LEU CA C 55.259 . 1 503 100 100 LEU CB C 42.450 . 1 504 100 100 LEU N N 121.453 0.027 1 505 101 101 GLY H H 8.453 0.0 1 506 101 101 GLY C C 173.696 0.005 1 507 101 101 GLY CA C 45.342 0.014 1 508 101 101 GLY N N 109.759 0.005 1 509 102 102 GLY H H 7.888 0.0 1 510 102 102 GLY C C 179.065 . 1 511 102 102 GLY CA C 45.984 . 1 512 102 102 GLY N N 115.142 0.003 1 stop_ save_ save_spectral_peak_list_1 _Saveframe_category spectral_peak_list _Details 'Default list' loop_ _Software_label $software_1 stop_ _Experiment_label '2D 1H-15N HSQC/HMQC' _Number_of_spectral_dimensions 2 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 1 H 1H 2 N 15N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_1 >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_1 >> _Spectral_peak_list.Entry_ID 50196 >> _Spectral_peak_list.ID 1 >> _Spectral_peak_list.Name 'peak list' >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Chem_shift_reference_ID 1 >> _Spectral_peak_list.Chem_shift_reference_label $chem_shift_reference_1 >> _Spectral_peak_list.Experiment_ID 1 >> _Spectral_peak_list.Experiment_name '2D 1H-15N HSQC/HMQC' >> _Spectral_peak_list.Experiment_class . >> _Spectral_peak_list.Experiment_type . >> _Spectral_peak_list.Number_of_spectral_dimensions 2 >> _Spectral_peak_list.Chemical_shift_list . >> _Spectral_peak_list.Assigned_chem_shift_list_ID 1 >> _Spectral_peak_list.Assigned_chem_shift_list_label $assigned_chemical_shifts_1 >> _Spectral_peak_list.Details 'Default list' >> _Spectral_peak_list.Text_data_format . >> _Spectral_peak_list.Text_data . >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Axis_code >> _Spectral_dim.Spectrometer_frequency >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Under_sampling_type >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Value_first_point >> _Spectral_dim.Absolute_peak_positions >> _Spectral_dim.Acquisition >> _Spectral_dim.Center_frequency_offset >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_reduced_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 1 . . H 1 1H . aliased 5995.20019531 Hz . . . . . . 50196 1 >> 2 . . N 15 15N . aliased 1519.56396484 Hz . . . . . . 50196 1 >> >> stop_ >> >> loop_ >> _Spectral_peak_software.Software_ID >> _Spectral_peak_software.Software_label >> _Spectral_peak_software.Method_ID >> _Spectral_peak_software.Method_label >> _Spectral_peak_software.Entry_ID >> _Spectral_peak_software.Spectral_peak_list_ID >> >> 1 $software_1 . . 50196 1 >> >> stop_ >> >> loop_ >> _Peak.ID >> _Peak.Figure_of_merit >> _Peak.Restraint >> _Peak.Details >> _Peak.Entry_ID >> _Peak.Spectral_peak_list_ID >> >> 1 1.0 . . 50196 1 >> 2 1.0 . . 50196 1 >> 3 1.0 . . 50196 1 >> 4 1.0 . . 50196 1 >> 5 1.0 . . 50196 1 >> 6 1.0 . . 50196 1 >> 7 1.0 . . 50196 1 >> 8 1.0 . . 50196 1 >> 9 1.0 . . 50196 1 >> 10 1.0 . . 50196 1 >> 11 1.0 . . 50196 1 >> 12 1.0 . . 50196 1 >> 13 1.0 . . 50196 1 >> 14 1.0 . . 50196 1 >> 15 1.0 . . 50196 1 >> 16 1.0 . . 50196 1 >> 17 1.0 . . 50196 1 >> 18 1.0 . . 50196 1 >> 19 1.0 . . 50196 1 >> 20 1.0 . . 50196 1 >> 21 1.0 . . 50196 1 >> 22 1.0 . . 50196 1 >> 23 1.0 . . 50196 1 >> 24 1.0 . . 50196 1 >> 25 1.0 . . 50196 1 >> 26 1.0 . . 50196 1 >> 27 1.0 . . 50196 1 >> 28 1.0 . . 50196 1 >> 29 1.0 . . 50196 1 >> 30 1.0 . . 50196 1 >> 31 1.0 . . 50196 1 >> 32 1.0 . . 50196 1 >> 33 1.0 . . 50196 1 >> 34 1.0 . . 50196 1 >> 35 1.0 . . 50196 1 >> 36 1.0 . . 50196 1 >> 37 1.0 . . 50196 1 >> 38 1.0 . . 50196 1 >> 39 1.0 . . 50196 1 >> 40 1.0 . . 50196 1 >> 41 1.0 . . 50196 1 >> 42 1.0 . . 50196 1 >> 43 1.0 . . 50196 1 >> 44 1.0 . . 50196 1 >> 45 1.0 . . 50196 1 >> 46 1.0 . . 50196 1 >> 47 1.0 . . 50196 1 >> 48 1.0 . . 50196 1 >> 49 1.0 . . 50196 1 >> 50 1.0 . . 50196 1 >> 51 1.0 . . 50196 1 >> 52 1.0 . . 50196 1 >> 53 1.0 . . 50196 1 >> 54 1.0 . . 50196 1 >> 55 1.0 . . 50196 1 >> 56 1.0 . . 50196 1 >> 57 1.0 . . 50196 1 >> 58 1.0 . . 50196 1 >> 59 1.0 . . 50196 1 >> 60 1.0 . . 50196 1 >> 61 1.0 . . 50196 1 >> 62 1.0 . . 50196 1 >> 63 1.0 . . 50196 1 >> 64 1.0 . . 50196 1 >> 65 1.0 . . 50196 1 >> 66 1.0 . . 50196 1 >> 67 1.0 . . 50196 1 >> 68 1.0 . . 50196 1 >> 69 1.0 . . 50196 1 >> 70 1.0 . . 50196 1 >> 71 1.0 . . 50196 1 >> 72 1.0 . . 50196 1 >> 73 1.0 . . 50196 1 >> 74 1.0 . . 50196 1 >> 75 1.0 . . 50196 1 >> 76 1.0 . . 50196 1 >> 77 1.0 . . 50196 1 >> 78 1.0 . . 50196 1 >> 79 1.0 . . 50196 1 >> 80 1.0 . . 50196 1 >> 81 1.0 . . 50196 1 >> 82 1.0 . . 50196 1 >> 83 1.0 . . 50196 1 >> 84 1.0 . . 50196 1 >> 85 1.0 . . 50196 1 >> 86 1.0 . . 50196 1 >> 87 1.0 . . 50196 1 >> 88 1.0 . . 50196 1 >> 89 1.0 . . 50196 1 >> 90 1.0 . . 50196 1 >> 91 1.0 . . 50196 1 >> 92 1.0 . . 50196 1 >> 93 1.0 . . 50196 1 >> 94 1.0 . . 50196 1 >> 95 1.0 . . 50196 1 >> 96 1.0 . . 50196 1 >> 97 1.0 . . 50196 1 >> >> stop_ >> >> loop_ >> _Peak_general_char.Peak_ID >> _Peak_general_char.Intensity_val >> _Peak_general_char.Intensity_val_err >> _Peak_general_char.Measurement_method >> _Peak_general_char.Entry_ID >> _Peak_general_char.Spectral_peak_list_ID >> >> 1 1266973.50000 . height 50196 1 >> 1 5853966.34375 . volume 50196 1 >> 2 1029083.56250 . height 50196 1 >> 2 5077950.06250 . volume 50196 1 >> 3 1228950.75000 . height 50196 1 >> 3 6779606.03125 . volume 50196 1 >> 4 1457278.00000 . height 50196 1 >> 4 7340293.50000 . volume 50196 1 >> 5 993896.87500 . height 50196 1 >> 5 5312047.29688 . volume 50196 1 >> 6 1252321.50000 . height 50196 1 >> 6 6296912.28125 . volume 50196 1 >> 7 1574830.75000 . height 50196 1 >> 7 7992246.12500 . volume 50196 1 >> 8 1108688.00000 . height 50196 1 >> 8 6226551.93750 . volume 50196 1 >> 9 1229639.50000 . height 50196 1 >> 9 6512004.06250 . volume 50196 1 >> 10 1077946.87500 . height 50196 1 >> 10 5474436.68750 . volume 50196 1 >> 11 1575206.00000 . height 50196 1 >> 11 7873383.03125 . volume 50196 1 >> 12 814612.00000 . height 50196 1 >> 12 4574688.87500 . volume 50196 1 >> 13 1349214.50000 . height 50196 1 >> 13 7015497.00000 . volume 50196 1 >> 14 1446240.37500 . height 50196 1 >> 14 7379150.68750 . volume 50196 1 >> 15 1161437.75000 . height 50196 1 >> 15 6229338.03125 . volume 50196 1 >> 16 1041076.87500 . height 50196 1 >> 16 5366948.40625 . volume 50196 1 >> 17 1233424.50000 . height 50196 1 >> 17 6744213.25000 . volume 50196 1 >> 18 1595442.00000 . height 50196 1 >> 18 8462872.62500 . volume 50196 1 >> 19 1020656.93750 . height 50196 1 >> 19 5695109.85938 . volume 50196 1 >> 20 624048.18750 . height 50196 1 >> 20 3697725.07812 . volume 50196 1 >> 21 2155206.00000 . height 50196 1 >> 21 12024795.00000 . volume 50196 1 >> 22 1551474.50000 . height 50196 1 >> 22 7803763.43750 . volume 50196 1 >> 23 545980.00000 . height 50196 1 >> 23 3358991.87500 . volume 50196 1 >> 24 1329536.00000 . height 50196 1 >> 24 7327446.71875 . volume 50196 1 >> 25 2230577.00000 . height 50196 1 >> 25 12982115.43750 . volume 50196 1 >> 26 1112533.50000 . height 50196 1 >> 26 6091233.21875 . volume 50196 1 >> 27 1399709.00000 . height 50196 1 >> 27 7553677.21875 . volume 50196 1 >> 28 1418724.75000 . height 50196 1 >> 28 7264563.25000 . volume 50196 1 >> 29 1086493.25000 . height 50196 1 >> 29 5879021.37500 . volume 50196 1 >> 30 1252862.62500 . height 50196 1 >> 30 7051948.21875 . volume 50196 1 >> 31 1500600.50000 . height 50196 1 >> 31 7747892.56250 . volume 50196 1 >> 32 1532165.37500 . height 50196 1 >> 32 8229151.75000 . volume 50196 1 >> 33 1015108.37500 . height 50196 1 >> 33 5757725.68750 . volume 50196 1 >> 34 1273651.25000 . height 50196 1 >> 34 7406074.68750 . volume 50196 1 >> 35 1413525.12500 . height 50196 1 >> 35 7722736.06250 . volume 50196 1 >> 36 1631481.75000 . height 50196 1 >> 36 8869071.00000 . volume 50196 1 >> 37 1234150.87500 . height 50196 1 >> 37 7206280.90625 . volume 50196 1 >> 38 1369115.12500 . height 50196 1 >> 38 7366135.96875 . volume 50196 1 >> 39 917520.25000 . height 50196 1 >> 39 4989346.62500 . volume 50196 1 >> 40 1609042.25000 . height 50196 1 >> 40 8247282.34375 . volume 50196 1 >> 41 1633730.25000 . height 50196 1 >> 41 8420805.00000 . volume 50196 1 >> 42 757498.93750 . height 50196 1 >> 42 4075484.71875 . volume 50196 1 >> 43 1116933.00000 . height 50196 1 >> 43 6853368.43750 . volume 50196 1 >> 44 1358754.50000 . height 50196 1 >> 44 7305680.12500 . volume 50196 1 >> 45 748322.00000 . height 50196 1 >> 45 4354132.17188 . volume 50196 1 >> 46 985040.68750 . height 50196 1 >> 46 5448154.65625 . volume 50196 1 >> 47 1500370.37500 . height 50196 1 >> 47 7610500.43750 . volume 50196 1 >> 48 461381.18750 . height 50196 1 >> 48 2744441.18750 . volume 50196 1 >> 49 973918.62500 . height 50196 1 >> 49 5414110.18750 . volume 50196 1 >> 50 1899392.75000 . height 50196 1 >> 50 11397630.25000 . volume 50196 1 >> 51 689515.00000 . height 50196 1 >> 51 4083777.43750 . volume 50196 1 >> 52 1287357.75000 . height 50196 1 >> 52 6624021.28125 . volume 50196 1 >> 53 1092088.25000 . height 50196 1 >> 53 5713657.03125 . volume 50196 1 >> 54 974454.50000 . height 50196 1 >> 54 5365445.03125 . volume 50196 1 >> 55 905999.93750 . height 50196 1 >> 55 5331430.03125 . volume 50196 1 >> 56 1135520.25000 . height 50196 1 >> 56 6287917.06250 . volume 50196 1 >> 57 912310.75000 . height 50196 1 >> 57 4970416.37500 . volume 50196 1 >> 58 901250.56250 . height 50196 1 >> 58 4894443.43750 . volume 50196 1 >> 59 1382943.75000 . height 50196 1 >> 59 7828001.25000 . volume 50196 1 >> 60 1335459.00000 . height 50196 1 >> 60 7068010.96875 . volume 50196 1 >> 61 1124404.75000 . height 50196 1 >> 61 6084883.71875 . volume 50196 1 >> 62 1190788.87500 . height 50196 1 >> 62 6393750.87500 . volume 50196 1 >> 63 1041571.06250 . height 50196 1 >> 63 5735110.96875 . volume 50196 1 >> 64 987782.00000 . height 50196 1 >> 64 5568032.81250 . volume 50196 1 >> 65 1070788.62500 . height 50196 1 >> 65 5576908.06250 . volume 50196 1 >> 66 1311758.00000 . height 50196 1 >> 66 7405342.50000 . volume 50196 1 >> 67 1284453.25000 . height 50196 1 >> 67 6740877.03125 . volume 50196 1 >> 68 1241458.75000 . height 50196 1 >> 68 6442068.40625 . volume 50196 1 >> 69 1106055.62500 . height 50196 1 >> 69 6100626.39062 . volume 50196 1 >> 70 1162322.87500 . height 50196 1 >> 70 6302334.03125 . volume 50196 1 >> 71 1276368.00000 . height 50196 1 >> 71 6742811.31250 . volume 50196 1 >> 72 976817.18750 . height 50196 1 >> 72 5392163.04688 . volume 50196 1 >> 73 1120630.75000 . height 50196 1 >> 73 5524521.56250 . volume 50196 1 >> 74 803278.00000 . height 50196 1 >> 74 4616944.43750 . volume 50196 1 >> 75 985196.68750 . height 50196 1 >> 75 4887444.78125 . volume 50196 1 >> 76 915220.00000 . height 50196 1 >> 76 5359887.96875 . volume 50196 1 >> 77 663574.50000 . height 50196 1 >> 77 3847319.51562 . volume 50196 1 >> 78 1128508.25000 . height 50196 1 >> 78 6334210.92188 . volume 50196 1 >> 79 1400053.12500 . height 50196 1 >> 79 5548113.90625 . volume 50196 1 >> 80 1191367.00000 . height 50196 1 >> 80 5158739.81250 . volume 50196 1 >> 81 1310170.37500 . height 50196 1 >> 81 6538159.28125 . volume 50196 1 >> 82 1123975.75000 . height 50196 1 >> 82 5448975.20312 . volume 50196 1 >> 83 1061615.75000 . height 50196 1 >> 83 6881480.12500 . volume 50196 1 >> 84 2155206.00000 . height 50196 1 >> 84 12024795.00000 . volume 50196 1 >> 85 2000676.25000 . height 50196 1 >> 85 11682824.56250 . volume 50196 1 >> 86 1025729.62500 . height 50196 1 >> 86 7176432.68750 . volume 50196 1 >> 87 1498274.87500 . height 50196 1 >> 87 9814100.12500 . volume 50196 1 >> 88 1572801.00000 . height 50196 1 >> 88 8525858.50000 . volume 50196 1 >> 89 1005642.50000 . height 50196 1 >> 89 5676603.62500 . volume 50196 1 >> 90 408855.18750 . height 50196 1 >> 90 3986754.60938 . volume 50196 1 >> 91 1454469.37500 . height 50196 1 >> 91 9547022.56250 . volume 50196 1 >> 92 270152.37500 . height 50196 1 >> 92 3569086.71875 . volume 50196 1 >> 93 1382784.50000 . height 50196 1 >> 93 6227718.31250 . volume 50196 1 >> 94 1368835.75000 . height 50196 1 >> 94 5609050.70312 . volume 50196 1 >> 95 1385713.50000 . height 50196 1 >> 95 5446716.79688 . volume 50196 1 >> 96 1282717.75000 . height 50196 1 >> 96 5842374.53125 . volume 50196 1 >> 97 1013824.00000 . height 50196 1 >> 97 6876740.56250 . volume 50196 1 >> >> stop_ >> >> loop_ >> _Peak_char.Peak_ID >> _Peak_char.Spectral_dim_ID >> _Peak_char.Chem_shift_val >> _Peak_char.Chem_shift_val_err >> _Peak_char.Line_width_val >> _Peak_char.Line_width_val_err >> _Peak_char.Phase_val >> _Peak_char.Phase_val_err >> _Peak_char.Decay_rate_val >> _Peak_char.Decay_rate_val_err >> _Peak_char.Coupling_pattern >> _Peak_char.Bounding_box_upper_val >> _Peak_char.Bounding_box_lower_val >> _Peak_char.Bounding_box_range_val >> _Peak_char.Details >> _Peak_char.Derivation_method_ID >> _Peak_char.Entry_ID >> _Peak_char.Spectral_peak_list_ID >> >> 1 1 7.887 . 15.93887266590 . . . . . . . . . . . 50196 1 >> 1 2 115.135 . 5.89386140610 . . . . . . . . . . . 50196 1 >> 2 1 7.660 . 15.89313291830 . . . . . . . . . . . 50196 1 >> 2 2 108.913 . 6.39518335043 . . . . . . . . . . . 50196 1 >> 3 1 8.030 . 16.84687812380 . . . . . . . . . . . 50196 1 >> 3 2 108.513 . 7.15273651073 . . . . . . . . . . . 50196 1 >> 4 1 8.289 . 15.38320620110 . . . . . . . . . . . 50196 1 >> 4 2 126.645 . 6.82012955318 . . . . . . . . . . . 50196 1 >> 5 1 8.149 . 16.51383558670 . . . . . . . . . . . 50196 1 >> 5 2 124.677 . 6.91029504470 . . . . . . . . . . . 50196 1 >> 6 1 8.473 . 15.42680189800 . . . . . . . . . . . 50196 1 >> 6 2 124.497 . 7.04312045236 . . . . . . . . . . . 50196 1 >> 7 1 8.201 . 15.44109556910 . . . . . . . . . . . 50196 1 >> 7 2 124.307 . 6.87503947708 . . . . . . . . . . . 50196 1 >> 8 1 8.216 . 17.36716775250 . . . . . . . . . . . 50196 1 >> 8 2 124.141 . 7.25449535526 . . . . . . . . . . . 50196 1 >> 9 1 8.087 . 17.61587763000 . . . . . . . . . . . 50196 1 >> 9 2 124.154 . 6.64063637104 . . . . . . . . . . . 50196 1 >> 10 1 8.266 . 16.22474608830 . . . . . . . . . . . 50196 1 >> 10 2 123.768 . 6.83681764139 . . . . . . . . . . . 50196 1 >> 11 1 8.078 . 15.27993442720 . . . . . . . . . . . 50196 1 >> 11 2 123.568 . 6.61287572498 . . . . . . . . . . . 50196 1 >> 12 1 8.215 . 16.67821280450 . . . . . . . . . . . 50196 1 >> 12 2 123.466 . 7.66977288276 . . . . . . . . . . . 50196 1 >> 13 1 8.381 . 15.90421051340 . . . . . . . . . . . 50196 1 >> 13 2 123.376 . 7.14041857317 . . . . . . . . . . . 50196 1 >> 14 1 8.195 . 16.15577912510 . . . . . . . . . . . 50196 1 >> 14 2 122.981 . 6.61889883416 . . . . . . . . . . . 50196 1 >> 15 1 8.423 . 16.00891165440 . . . . . . . . . . . 50196 1 >> 15 2 122.928 . 7.46118310177 . . . . . . . . . . . 50196 1 >> 16 1 8.179 . 16.11182608640 . . . . . . . . . . . 50196 1 >> 16 2 122.803 . 6.89070861824 . . . . . . . . . . . 50196 1 >> 17 1 8.376 . 16.49525381420 . . . . . . . . . . . 50196 1 >> 17 2 122.535 . 7.29357763511 . . . . . . . . . . . 50196 1 >> 18 1 8.459 . 16.49846989020 . . . . . . . . . . . 50196 1 >> 18 2 122.315 . 6.93798776096 . . . . . . . . . . . 50196 1 >> 19 1 8.425 . 17.15240534390 . . . . . . . . . . . 50196 1 >> 19 2 122.173 . 7.41539841471 . . . . . . . . . . . 50196 1 >> 20 1 8.584 . 18.43454764340 . . . . . . . . . . . 50196 1 >> 20 2 122.016 . 8.25505606328 . . . . . . . . . . . 50196 1 >> 21 1 8.301 . 25.07467256220 . . . . . . . . . . . 50196 1 >> 21 2 122.029 . 7.23819220260 . . . . . . . . . . . 50196 1 >> 22 1 8.285 . 16.44987140840 . . . . . . . . . . . 50196 1 >> 22 2 121.227 . 6.60644503699 . . . . . . . . . . . 50196 1 >> 23 1 8.448 . 21.38654807150 . . . . . . . . . . . 50196 1 >> 23 2 121.046 . 8.83771262477 . . . . . . . . . . . 50196 1 >> 24 1 8.377 . 16.11647152950 . . . . . . . . . . . 50196 1 >> 24 2 121.001 . 7.43930970528 . . . . . . . . . . . 50196 1 >> 25 1 8.509 . 21.42799971770 . . . . . . . . . . . 50196 1 >> 25 2 120.684 . 6.96076688815 . . . . . . . . . . . 50196 1 >> 26 1 8.248 . 16.84044597180 . . . . . . . . . . . 50196 1 >> 26 2 122.315 . 7.40421264053 . . . . . . . . . . . 50196 1 >> 27 1 8.196 . 16.55886065070 . . . . . . . . . . . 50196 1 >> 27 2 122.200 . 7.31843994292 . . . . . . . . . . . 50196 1 >> 28 1 8.101 . 16.14970431490 . . . . . . . . . . . 50196 1 >> 28 2 122.097 . 6.78473812595 . . . . . . . . . . . 50196 1 >> 29 1 7.757 . 16.76576154020 . . . . . . . . . . . 50196 1 >> 29 2 122.019 . 7.32989743631 . . . . . . . . . . . 50196 1 >> 30 1 8.010 . 16.52098242220 . . . . . . . . . . . 50196 1 >> 30 2 121.793 . 7.44243447621 . . . . . . . . . . . 50196 1 >> 31 1 8.103 . 16.39841419240 . . . . . . . . . . . 50196 1 >> 31 2 121.662 . 6.89419568145 . . . . . . . . . . . 50196 1 >> 32 1 8.188 . 18.12544700540 . . . . . . . . . . . 50196 1 >> 32 2 121.457 . 7.23461456632 . . . . . . . . . . . 50196 1 >> 33 1 8.152 . 41.49595662840 . . . . . . . . . . . 50196 1 >> 33 2 121.462 . 7.40933001900 . . . . . . . . . . . 50196 1 >> 34 1 8.107 . 16.95300863180 . . . . . . . . . . . 50196 1 >> 34 2 121.471 . 16.08523385360 . . . . . . . . . . . 50196 1 >> 35 1 8.253 . 17.01161268340 . . . . . . . . . . . 50196 1 >> 35 2 121.316 . 6.84315775632 . . . . . . . . . . . 50196 1 >> 36 1 8.108 . 16.82400825000 . . . . . . . . . . . 50196 1 >> 36 2 121.339 . 14.57904898040 . . . . . . . . . . . 50196 1 >> 37 1 7.970 . 16.94514711270 . . . . . . . . . . . 50196 1 >> 37 2 121.205 . 7.54849554157 . . . . . . . . . . . 50196 1 >> 38 1 8.237 . 16.79256217350 . . . . . . . . . . . 50196 1 >> 38 2 120.903 . 7.03639540188 . . . . . . . . . . . 50196 1 >> 39 1 8.167 . 17.31142243520 . . . . . . . . . . . 50196 1 >> 39 2 120.488 . 7.16442043681 . . . . . . . . . . . 50196 1 >> 40 1 8.220 . 16.41413723060 . . . . . . . . . . . 50196 1 >> 40 2 120.444 . 6.78555328358 . . . . . . . . . . . 50196 1 >> 41 1 8.276 . 16.73788888150 . . . . . . . . . . . 50196 1 >> 41 2 120.356 . 6.81299692389 . . . . . . . . . . . 50196 1 >> 42 1 8.236 . 18.75079511690 . . . . . . . . . . . 50196 1 >> 42 2 120.194 . 6.85176219800 . . . . . . . . . . . 50196 1 >> 43 1 7.986 . 18.72792524310 . . . . . . . . . . . 50196 1 >> 43 2 120.452 . 8.83087435795 . . . . . . . . . . . 50196 1 >> 44 1 8.062 . 18.35986321180 . . . . . . . . . . . 50196 1 >> 44 2 120.249 . 6.92847758858 . . . . . . . . . . . 50196 1 >> 45 1 7.893 . 17.81920510170 . . . . . . . . . . . 50196 1 >> 45 2 119.562 . 8.01961136694 . . . . . . . . . . . 50196 1 >> 46 1 8.459 . 17.96750193960 . . . . . . . . . . . 50196 1 >> 46 2 119.722 . 7.19612101142 . . . . . . . . . . . 50196 1 >> 47 1 8.346 . 16.21474051850 . . . . . . . . . . . 50196 1 >> 47 2 119.037 . 6.66975561315 . . . . . . . . . . . 50196 1 >> 48 1 8.469 . 18.40774701010 . . . . . . . . . . . 50196 1 >> 48 2 118.184 . 7.97808361419 . . . . . . . . . . . 50196 1 >> 49 1 8.306 . 16.92656534030 . . . . . . . . . . . 50196 1 >> 49 2 117.260 . 7.47925242930 . . . . . . . . . . . 50196 1 >> 50 1 8.196 . 17.27676028270 . . . . . . . . . . . 50196 1 >> 50 2 117.317 . 8.92760639708 . . . . . . . . . . . 50196 1 >> 51 1 8.226 . 33.66373953820 . . . . . . . . . . . 50196 1 >> 51 2 117.224 . 7.91490889763 . . . . . . . . . . . 50196 1 >> 52 1 8.375 . 15.90957064010 . . . . . . . . . . . 50196 1 >> 52 2 116.533 . 6.91724652785 . . . . . . . . . . . 50196 1 >> 53 1 8.507 . 16.27799001320 . . . . . . . . . . . 50196 1 >> 53 2 116.340 . 6.89541841790 . . . . . . . . . . . 50196 1 >> 54 1 8.274 . 17.48008775440 . . . . . . . . . . . 50196 1 >> 54 2 116.198 . 7.40009156583 . . . . . . . . . . . 50196 1 >> 55 1 8.314 . 19.51121842050 . . . . . . . . . . . 50196 1 >> 55 2 116.126 . 7.93447268082 . . . . . . . . . . . 50196 1 >> 56 1 8.411 . 16.29371305140 . . . . . . . . . . . 50196 1 >> 56 2 115.736 . 7.30843161864 . . . . . . . . . . . 50196 1 >> 57 1 8.127 . 17.39682712010 . . . . . . . . . . . 50196 1 >> 57 2 116.194 . 7.13588991965 . . . . . . . . . . . 50196 1 >> 58 1 8.061 . 17.22601775020 . . . . . . . . . . . 50196 1 >> 58 2 115.771 . 7.08236123508 . . . . . . . . . . . 50196 1 >> 59 1 8.193 . 16.42164140790 . . . . . . . . . . . 50196 1 >> 59 2 115.679 . 7.46068494988 . . . . . . . . . . . 50196 1 >> 60 1 8.181 . 16.37804571100 . . . . . . . . . . . 50196 1 >> 60 2 115.523 . 7.46983282999 . . . . . . . . . . . 50196 1 >> 61 1 8.089 . 17.10630825460 . . . . . . . . . . . 50196 1 >> 61 2 115.458 . 7.07674570472 . . . . . . . . . . . 50196 1 >> 62 1 8.374 . 16.29728646920 . . . . . . . . . . . 50196 1 >> 62 2 114.865 . 7.15491026442 . . . . . . . . . . . 50196 1 >> 63 1 7.945 . 16.92477863140 . . . . . . . . . . . 50196 1 >> 63 2 114.672 . 7.13507476202 . . . . . . . . . . . 50196 1 >> 64 1 8.213 . 17.11559914080 . . . . . . . . . . . 50196 1 >> 64 2 114.153 . 7.60560186242 . . . . . . . . . . . 50196 1 >> 65 1 7.965 . 16.81114394600 . . . . . . . . . . . 50196 1 >> 65 2 113.367 . 6.92005429303 . . . . . . . . . . . 50196 1 >> 66 1 8.093 . 16.99660432870 . . . . . . . . . . . 50196 1 >> 66 2 113.099 . 7.28651293562 . . . . . . . . . . . 50196 1 >> 67 1 8.531 . 16.87117736470 . . . . . . . . . . . 50196 1 >> 67 2 112.486 . 7.03598782307 . . . . . . . . . . . 50196 1 >> 68 1 8.594 . 17.11131103950 . . . . . . . . . . . 50196 1 >> 68 2 111.123 . 6.57714464873 . . . . . . . . . . . 50196 1 >> 69 1 8.461 . 16.79006078110 . . . . . . . . . . . 50196 1 >> 69 2 110.803 . 7.24620791932 . . . . . . . . . . . 50196 1 >> 70 1 8.339 . 17.56656446470 . . . . . . . . . . . 50196 1 >> 70 2 110.732 . 7.01597117452 . . . . . . . . . . . 50196 1 >> 71 1 8.266 . 16.92156255540 . . . . . . . . . . . 50196 1 >> 71 2 110.733 . 7.19883820353 . . . . . . . . . . . 50196 1 >> 72 1 8.299 . 17.40719003170 . . . . . . . . . . . 50196 1 >> 72 2 110.375 . 7.14132430387 . . . . . . . . . . . 50196 1 >> 73 1 8.453 . 16.60602976540 . . . . . . . . . . . 50196 1 >> 73 2 109.762 . 6.24383574989 . . . . . . . . . . . 50196 1 >> 74 1 8.410 . 20.95344983650 . . . . . . . . . . . 50196 1 >> 74 2 109.660 . 7.67244478833 . . . . . . . . . . . 50196 1 >> 75 1 8.510 . 16.44308191460 . . . . . . . . . . . 50196 1 >> 75 2 109.506 . 6.41157707616 . . . . . . . . . . . 50196 1 >> 76 1 8.384 . 17.53904914770 . . . . . . . . . . . 50196 1 >> 76 2 109.491 . 7.72706034975 . . . . . . . . . . . 50196 1 >> 77 1 8.410 . 18.34592688250 . . . . . . . . . . . 50196 1 >> 77 2 109.163 . 8.02658549335 . . . . . . . . . . . 50196 1 >> 78 1 8.292 . 17.04198673450 . . . . . . . . . . . 50196 1 >> 78 2 107.968 . 7.31259797988 . . . . . . . . . . . 50196 1 >> 79 1 7.544 . 11.78227310420 . . . . . . . . . . . 50196 1 >> 79 2 112.641 . 5.86696120421 . . . . . . . . . . . 50196 1 >> 80 1 7.449 . 12.43334982370 . . . . . . . . . . . 50196 1 >> 80 2 112.456 . 6.37118148679 . . . . . . . . . . . 50196 1 >> 81 1 6.888 . 16.16685672020 . . . . . . . . . . . 50196 1 >> 81 2 112.639 . 6.21793185177 . . . . . . . . . . . 50196 1 >> 82 1 6.792 . 16.75468394500 . . . . . . . . . . . 50196 1 >> 82 2 112.457 . 6.28432191233 . . . . . . . . . . . 50196 1 >> 83 1 8.279 . 34.41808803150 . . . . . . . . . . . 50196 1 >> 83 2 121.987 . 7.53980052682 . . . . . . . . . . . 50196 1 >> 84 1 8.307 . 25.07467256220 . . . . . . . . . . . 50196 1 >> 84 2 122.018 . 7.23819220260 . . . . . . . . . . . 50196 1 >> 85 1 8.490 . 23.04032582000 . . . . . . . . . . . 50196 1 >> 85 2 120.679 . 6.84601080803 . . . . . . . . . . . 50196 1 >> 86 1 7.969 . 21.76818909040 . . . . . . . . . . . 50196 1 >> 86 2 120.385 . 10.24947507210 . . . . . . . . . . . 50196 1 >> 87 1 8.200 . 17.54762535040 . . . . . . . . . . . 50196 1 >> 87 2 117.358 . 10.35014703980 . . . . . . . . . . . 50196 1 >> 88 1 8.423 . 16.67785546280 . . . . . . . . . . . 50196 1 >> 88 2 120.887 . 7.75998366081 . . . . . . . . . . . 50196 1 >> 89 1 8.334 . 17.23816737070 . . . . . . . . . . . 50196 1 >> 89 2 116.739 . 8.27747289819 . . . . . . . . . . . 50196 1 >> 90 1 8.436 . 19.91358526250 . . . . . . . . . . . 50196 1 >> 90 2 120.852 . 18.09296710380 . . . . . . . . . . . 50196 1 >> 91 1 8.308 . 30.26577657120 . . . . . . . . . . . 50196 1 >> 91 2 117.599 . 8.66204615484 . . . . . . . . . . . 50196 1 >> 92 1 8.513 . 25.62247750790 . . . . . . . . . . . 50196 1 >> 92 2 120.770 . 16.76534703880 . . . . . . . . . . . 50196 1 >> 93 1 6.880 . 15.01192809370 . . . . . . . . . . . 50196 1 >> 93 2 112.397 . 5.94231799874 . . . . . . . . . . . 50196 1 >> 94 1 7.517 . 12.55055792690 . . . . . . . . . . . 50196 1 >> 94 2 112.397 . 5.85917192016 . . . . . . . . . . . 50196 1 >> 95 1 7.416 . 12.07422133680 . . . . . . . . . . . 50196 1 >> 95 2 112.392 . 5.58256176335 . . . . . . . . . . . 50196 1 >> 96 1 6.824 . 15.04087277780 . . . . . . . . . . . 50196 1 >> 96 2 112.392 . 5.67331597983 . . . . . . . . . . . 50196 1 >> 97 1 8.334 . 36.17299350330 . . . . . . . . . . . 50196 1 >> 97 2 117.601 . 7.52272750306 . . . . . . . . . . . 50196 1 >> >> stop_ >> >> loop_ >> _Assigned_peak_chem_shift.Peak_ID >> _Assigned_peak_chem_shift.Spectral_dim_ID >> _Assigned_peak_chem_shift.Set_ID >> _Assigned_peak_chem_shift.Magnetization_linkage_ID >> _Assigned_peak_chem_shift.Assembly_atom_ID >> _Assigned_peak_chem_shift.Val >> _Assigned_peak_chem_shift.Contribution_fractional_val >> _Assigned_peak_chem_shift.Figure_of_merit >> _Assigned_peak_chem_shift.Assigned_chem_shift_list_ID >> _Assigned_peak_chem_shift.Atom_chem_shift_ID >> _Assigned_peak_chem_shift.Entity_assembly_ID >> _Assigned_peak_chem_shift.Entity_ID >> _Assigned_peak_chem_shift.Comp_index_ID >> _Assigned_peak_chem_shift.Comp_ID >> _Assigned_peak_chem_shift.Atom_ID >> _Assigned_peak_chem_shift.Ambiguity_code >> _Assigned_peak_chem_shift.Ambiguity_set_ID >> _Assigned_peak_chem_shift.Auth_atom_peak_num >> _Assigned_peak_chem_shift.Auth_entity_ID >> _Assigned_peak_chem_shift.Auth_seq_ID >> _Assigned_peak_chem_shift.Auth_comp_ID >> _Assigned_peak_chem_shift.Auth_atom_ID >> _Assigned_peak_chem_shift.Auth_ambiguity_code >> _Assigned_peak_chem_shift.Auth_ambiguity_set_ID >> _Assigned_peak_chem_shift.Auth_amb_atom_grp_ID >> _Assigned_peak_chem_shift.Resonance_ID >> _Assigned_peak_chem_shift.Details >> _Assigned_peak_chem_shift.Entry_ID >> _Assigned_peak_chem_shift.Spectral_peak_list_ID >> >> 1 1 1 . . 7.887 . . 1 1 1 102 GLY H . . . . . . . . . . 13 . 50196 1 >> 1 2 1 . . 115.135 . . 1 1 1 102 GLY N . . . . . . . . . . 14 . 50196 1 >> 2 1 1 . . 7.660 . . 1 1 1 97 GLY H . . . . . . . . . . 83 . 50196 1 >> 2 2 1 . . 108.913 . . 1 1 1 97 GLY N . . . . . . . . . . 84 . 50196 1 >> 3 1 1 . . 8.030 . . 1 1 1 49 GLY H . . . . . . . . . . 123 . 50196 1 >> 3 2 1 . . 108.513 . . 1 1 1 49 GLY N . . . . . . . . . . 124 . 50196 1 >> 4 1 1 . . 8.289 . . 1 1 1 10 ALA H . . . . . . . . . . 97 . 50196 1 >> 4 2 1 . . 126.645 . . 1 1 1 10 ALA N . . . . . . . . . . 98 . 50196 1 >> 5 1 1 . . 8.149 . . 1 1 1 96 LEU H . . . . . . . . . . 51 . 50196 1 >> 5 2 1 . . 124.677 . . 1 1 1 96 LEU N . . . . . . . . . . 52 . 50196 1 >> 6 1 1 . . 8.473 . . 1 1 1 40 ALA H . . . . . . . . . . 27 . 50196 1 >> 6 2 1 . . 124.497 . . 1 1 1 40 ALA N . . . . . . . . . . 28 . 50196 1 >> 7 1 1 . . 8.201 . . 1 1 1 43 ALA H . . . . . . . . . . 117 . 50196 1 >> 7 2 1 . . 124.307 . . 1 1 1 43 ALA N . . . . . . . . . . 118 . 50196 1 >> 8 1 1 . . 8.216 . . 1 1 1 42 LEU H . . . . . . . . . . 121 . 50196 1 >> 8 2 1 . . 124.141 . . 1 1 1 42 LEU N . . . . . . . . . . 122 . 50196 1 >> 9 1 1 . . 8.087 . . 1 1 1 72 ASP H . . . . . . . . . . 85 . 50196 1 >> 9 2 1 . . 124.154 . . 1 1 1 72 ASP N . . . . . . . . . . 86 . 50196 1 >> 10 1 1 . . 8.266 . . 1 1 1 90 LEU H . . . . . . . . . . 47 . 50196 1 >> 10 2 1 . . 123.768 . . 1 1 1 90 LEU N . . . . . . . . . . 48 . 50196 1 >> 11 1 1 . . 8.078 . . 1 1 1 45 ALA H . . . . . . . . . . 21 . 50196 1 >> 11 2 1 . . 123.568 . . 1 1 1 45 ALA N . . . . . . . . . . 22 . 50196 1 >> 12 1 1 . . 8.215 . . 1 1 1 30 LEU H . . . . . . . . . . 137 . 50196 1 >> 12 2 1 . . 123.466 . . 1 1 1 30 LEU N . . . . . . . . . . 138 . 50196 1 >> 13 1 1 . . 8.381 . . 1 1 1 85 GLU H . . . . . . . . . . 101 . 50196 1 >> 13 2 1 . . 123.376 . . 1 1 1 85 GLU N . . . . . . . . . . 102 . 50196 1 >> 14 1 1 . . 8.195 . . 1 1 1 61 TRP H . . . . . . . . . . 61 . 50196 1 >> 14 2 1 . . 122.981 . . 1 1 1 61 TRP N . . . . . . . . . . 62 . 50196 1 >> 15 1 1 . . 8.423 . . 1 1 1 79 GLU H . . . . . . . . . . 151 . 50196 1 >> 15 2 1 . . 122.928 . . 1 1 1 79 GLU N . . . . . . . . . . 152 . 50196 1 >> 16 1 1 . . 8.179 . . 1 1 1 95 PHE H . . . . . . . . . . 19 . 50196 1 >> 16 2 1 . . 122.803 . . 1 1 1 95 PHE N . . . . . . . . . . 20 . 50196 1 >> 17 1 1 . . 8.376 . . 1 1 1 8 ARG H . . . . . . . . . . 65 . 50196 1 >> 17 2 1 . . 122.535 . . 1 1 1 8 ARG N . . . . . . . . . . 66 . 50196 1 >> 18 1 1 . . 8.459 . . 1 1 1 15 ASP H . . . . . . . . . . 5 . 50196 1 >> 18 2 1 . . 122.315 . . 1 1 1 15 ASP N . . . . . . . . . . 6 . 50196 1 >> 19 1 1 . . 8.425 . . 1 1 1 9 MET H . . . . . . . . . . 115 . 50196 1 >> 19 2 1 . . 122.173 . . 1 1 1 9 MET N . . . . . . . . . . 116 . 50196 1 >> 20 1 1 . . 8.584 . . 1 1 1 3 MET H . . . . . . . . . . 53 . 50196 1 >> 20 2 1 . . 122.016 . . 1 1 1 3 MET N . . . . . . . . . . 54 . 50196 1 >> 21 1 1 . . 8.301 . . 1 1 1 83 PHE H . . . . . . . . . . 7 . 50196 1 >> 21 2 1 . . 122.029 . . 1 1 1 83 PHE N . . . . . . . . . . 8 . 50196 1 >> 22 1 1 . . 8.285 . . 1 1 1 54 ASP H . . . . . . . . . . 119 . 50196 1 >> 22 2 1 . . 121.227 . . 1 1 1 54 ASP N . . . . . . . . . . 120 . 50196 1 >> 23 1 1 . . 8.448 . . 1 1 1 34 ASN H . . . . . . . . . . 488 . 50196 1 >> 23 2 1 . . 121.046 . . 1 1 1 34 ASN N . . . . . . . . . . 489 . 50196 1 >> 24 1 1 . . 8.377 . . 1 1 1 17 GLU H . . . . . . . . . . 45 . 50196 1 >> 24 2 1 . . 121.001 . . 1 1 1 17 GLU N . . . . . . . . . . 46 . 50196 1 >> 25 1 1 . . 8.509 . . 1 1 1 7 GLN H . . . . . . . . . . 135 . 50196 1 >> 25 2 1 . . 120.684 . . 1 1 1 7 GLN N . . . . . . . . . . 136 . 50196 1 >> 26 1 1 . . 8.248 . . 1 1 1 77 PHE H . . . . . . . . . . 33 . 50196 1 >> 26 2 1 . . 122.315 . . 1 1 1 77 PHE N . . . . . . . . . . 34 . 50196 1 >> 27 1 1 . . 8.196 . . 1 1 1 18 LEU H . . . . . . . . . . 59 . 50196 1 >> 27 2 1 . . 122.200 . . 1 1 1 18 LEU N . . . . . . . . . . 60 . 50196 1 >> 28 1 1 . . 8.101 . . 1 1 1 71 PHE H . . . . . . . . . . 109 . 50196 1 >> 28 2 1 . . 122.097 . . 1 1 1 71 PHE N . . . . . . . . . . 110 . 50196 1 >> 29 1 1 . . 7.757 . . 1 1 1 75 ARG H . . . . . . . . . . 107 . 50196 1 >> 29 2 1 . . 122.019 . . 1 1 1 75 ARG N . . . . . . . . . . 108 . 50196 1 >> 30 1 1 . . 8.010 . . 1 1 1 22 LEU H . . . . . . . . . . 3 . 50196 1 >> 30 2 1 . . 121.793 . . 1 1 1 22 LEU N . . . . . . . . . . 4 . 50196 1 >> 31 1 1 . . 8.103 . . 1 1 1 55 ARG H . . . . . . . . . . 89 . 50196 1 >> 31 2 1 . . 121.662 . . 1 1 1 55 ARG N . . . . . . . . . . 90 . 50196 1 >> 32 1 1 . . 8.188 . . 1 1 1 16 LYS H . . . . . . . . . . 79 . 50196 1 >> 32 2 1 . . 121.457 . . 1 1 1 16 LYS N . . . . . . . . . . 80 . 50196 1 >> 33 1 1 . . 8.152 . . 1 1 1 38 ARG H . . . . . . . . . . 41 . 50196 1 >> 33 2 1 . . 121.462 . . 1 1 1 38 ARG N . . . . . . . . . . 42 . 50196 1 >> 34 1 1 . . 8.107 . . 1 1 1 100 LEU H . . . . . . . . . . 15 . 50196 1 >> 34 2 1 . . 121.471 . . 1 1 1 100 LEU N . . . . . . . . . . 16 . 50196 1 >> 35 1 1 . . 8.253 . . 1 1 1 5 GLN H . . . . . . . . . . 131 . 50196 1 >> 35 2 1 . . 121.316 . . 1 1 1 5 GLN N . . . . . . . . . . 132 . 50196 1 >> 36 1 1 . . 8.108 . . 1 1 1 52 LEU H . . . . . . . . . . 91 . 50196 1 >> 36 2 1 . . 121.339 . . 1 1 1 52 LEU N . . . . . . . . . . 92 . 50196 1 >> 37 1 1 . . 7.970 . . 1 1 1 21 LEU H . . . . . . . . . . 105 . 50196 1 >> 37 2 1 . . 121.205 . . 1 1 1 21 LEU N . . . . . . . . . . 106 . 50196 1 >> 38 1 1 . . 8.237 . . 1 1 1 47 PHE H . . . . . . . . . . 143 . 50196 1 >> 38 2 1 . . 120.903 . . 1 1 1 47 PHE N . . . . . . . . . . 144 . 50196 1 >> 39 1 1 . . 8.167 . . 1 1 1 36 LYS H . . . . . . . . . . 147 . 50196 1 >> 39 2 1 . . 120.488 . . 1 1 1 36 LYS N . . . . . . . . . . 148 . 50196 1 >> 40 1 1 . . 8.220 . . 1 1 1 65 ASP H . . . . . . . . . . 35 . 50196 1 >> 40 2 1 . . 120.444 . . 1 1 1 65 ASP N . . . . . . . . . . 36 . 50196 1 >> 41 1 1 . . 8.276 . . 1 1 1 12 VAL H . . . . . . . . . . 67 . 50196 1 >> 41 2 1 . . 120.356 . . 1 1 1 12 VAL N . . . . . . . . . . 68 . 50196 1 >> 42 1 1 . . 8.236 . . 1 1 1 32 VAL H . . . . . . . . . . 99 . 50196 1 >> 42 2 1 . . 120.194 . . 1 1 1 32 VAL N . . . . . . . . . . 100 . 50196 1 >> 43 1 1 . . 7.986 . . 1 1 1 26 MET H . . . . . . . . . . 159 . 50196 1 >> 43 2 1 . . 120.452 . . 1 1 1 26 MET N . . . . . . . . . . 160 . 50196 1 >> 44 1 1 . . 8.062 . . 1 1 1 23 ASP H . . . . . . . . . . 9 . 50196 1 >> 44 2 1 . . 120.249 . . 1 1 1 23 ASP N . . . . . . . . . . 10 . 50196 1 >> 45 1 1 . . 7.893 . . 1 1 1 27 MET H . . . . . . . . . . 43 . 50196 1 >> 45 2 1 . . 119.562 . . 1 1 1 27 MET N . . . . . . . . . . 44 . 50196 1 >> 46 1 1 . . 8.459 . . 1 1 1 4 ASN H . . . . . . . . . . 17 . 50196 1 >> 46 2 1 . . 119.722 . . 1 1 1 4 ASN N . . . . . . . . . . 18 . 50196 1 >> 47 1 1 . . 8.346 . . 1 1 1 46 GLN H . . . . . . . . . . 133 . 50196 1 >> 47 2 1 . . 119.037 . . 1 1 1 46 GLN N . . . . . . . . . . 134 . 50196 1 >> 48 1 1 . . 8.469 . . 1 1 1 89 SER H . . . . . . . . . . 93 . 50196 1 >> 48 2 1 . . 118.184 . . 1 1 1 89 SER N . . . . . . . . . . 94 . 50196 1 >> 49 1 1 . . 8.306 . . 1 1 1 58 SER H . . . . . . . . . . 145 . 50196 1 >> 49 2 1 . . 117.260 . . 1 1 1 58 SER N . . . . . . . . . . 146 . 50196 1 >> 50 1 1 . . 8.196 . . 1 1 1 78 SER H . . . . . . . . . . 157 . 50196 1 >> 50 2 1 . . 117.317 . . 1 1 1 78 SER N . . . . . . . . . . 158 . 50196 1 >> 51 1 1 . . 8.226 . . 1 1 1 33 THR H . . . . . . . . . . 69 . 50196 1 >> 51 2 1 . . 117.224 . . 1 1 1 33 THR N . . . . . . . . . . 70 . 50196 1 >> 52 1 1 . . 8.375 . . 1 1 1 67 SER H . . . . . . . . . . 31 . 50196 1 >> 52 2 1 . . 116.533 . . 1 1 1 67 SER N . . . . . . . . . . 32 . 50196 1 >> 53 1 1 . . 8.507 . . 1 1 1 57 SER H . . . . . . . . . . 149 . 50196 1 >> 53 2 1 . . 116.340 . . 1 1 1 57 SER N . . . . . . . . . . 150 . 50196 1 >> 54 1 1 . . 8.274 . . 1 1 1 91 SER H . . . . . . . . . . 81 . 50196 1 >> 54 2 1 . . 116.198 . . 1 1 1 91 SER N . . . . . . . . . . 82 . 50196 1 >> 55 1 1 . . 8.314 . . 1 1 1 25 SER H . . . . . . . . . . 63 . 50196 1 >> 55 2 1 . . 116.126 . . 1 1 1 25 SER N . . . . . . . . . . 64 . 50196 1 >> 56 1 1 . . 8.411 . . 1 1 1 50 SER H . . . . . . . . . . 49 . 50196 1 >> 56 2 1 . . 115.736 . . 1 1 1 50 SER N . . . . . . . . . . 50 . 50196 1 >> 57 1 1 . . 8.127 . . 1 1 1 84 THR H . . . . . . . . . . 25 . 50196 1 >> 57 2 1 . . 116.194 . . 1 1 1 84 THR N . . . . . . . . . . 26 . 50196 1 >> 58 1 1 . . 8.061 . . 1 1 1 94 THR H . . . . . . . . . . 95 . 50196 1 >> 58 2 1 . . 115.771 . . 1 1 1 94 THR N . . . . . . . . . . 96 . 50196 1 >> 59 1 1 . . 8.193 . . 1 1 1 19 SER H . . . . . . . . . . 55 . 50196 1 >> 59 2 1 . . 115.679 . . 1 1 1 19 SER N . . . . . . . . . . 56 . 50196 1 >> 60 1 1 . . 8.181 . . 1 1 1 63 SER H . . . . . . . . . . 29 . 50196 1 >> 60 2 1 . . 115.523 . . 1 1 1 63 SER N . . . . . . . . . . 30 . 50196 1 >> 61 1 1 . . 8.089 . . 1 1 1 60 SER H . . . . . . . . . . 75 . 50196 1 >> 61 2 1 . . 115.458 . . 1 1 1 60 SER N . . . . . . . . . . 76 . 50196 1 >> 62 1 1 . . 8.374 . . 1 1 1 74 SER H . . . . . . . . . . 155 . 50196 1 >> 62 2 1 . . 114.865 . . 1 1 1 74 SER N . . . . . . . . . . 156 . 50196 1 >> 63 1 1 . . 7.945 . . 1 1 1 76 THR H . . . . . . . . . . 111 . 50196 1 >> 63 2 1 . . 114.672 . . 1 1 1 76 THR N . . . . . . . . . . 112 . 50196 1 >> 64 1 1 . . 8.213 . . 1 1 1 41 SER H . . . . . . . . . . 71 . 50196 1 >> 64 2 1 . . 114.153 . . 1 1 1 41 SER N . . . . . . . . . . 72 . 50196 1 >> 65 1 1 . . 7.965 . . 1 1 1 81 THR H . . . . . . . . . . 141 . 50196 1 >> 65 2 1 . . 113.367 . . 1 1 1 81 THR N . . . . . . . . . . 142 . 50196 1 >> 66 1 1 . . 8.093 . . 1 1 1 14 THR H . . . . . . . . . . 11 . 50196 1 >> 66 2 1 . . 113.099 . . 1 1 1 14 THR N . . . . . . . . . . 12 . 50196 1 >> 67 1 1 . . 8.531 . . 1 1 1 13 GLY H . . . . . . . . . . 125 . 50196 1 >> 67 2 1 . . 112.486 . . 1 1 1 13 GLY N . . . . . . . . . . 126 . 50196 1 >> 68 1 1 . . 8.594 . . 1 1 1 51 GLY H . . . . . . . . . . 87 . 50196 1 >> 68 2 1 . . 111.123 . . 1 1 1 51 GLY N . . . . . . . . . . 88 . 50196 1 >> 69 1 1 . . 8.461 . . 1 1 1 64 GLY H . . . . . . . . . . 39 . 50196 1 >> 69 2 1 . . 110.803 . . 1 1 1 64 GLY N . . . . . . . . . . 40 . 50196 1 >> 70 1 1 . . 8.339 . . 1 1 1 48 GLY H . . . . . . . . . . 23 . 50196 1 >> 70 2 1 . . 110.732 . . 1 1 1 48 GLY N . . . . . . . . . . 24 . 50196 1 >> 71 1 1 . . 8.266 . . 1 1 1 62 GLY H . . . . . . . . . . 139 . 50196 1 >> 71 2 1 . . 110.733 . . 1 1 1 62 GLY N . . . . . . . . . . 140 . 50196 1 >> 72 1 1 . . 8.299 . . 1 1 1 59 GLY H . . . . . . . . . . 103 . 50196 1 >> 72 2 1 . . 110.375 . . 1 1 1 59 GLY N . . . . . . . . . . 104 . 50196 1 >> 73 1 1 . . 8.453 . . 1 1 1 101 GLY H . . . . . . . . . . 57 . 50196 1 >> 73 2 1 . . 109.762 . . 1 1 1 101 GLY N . . . . . . . . . . 58 . 50196 1 >> 74 1 1 . . 8.410 . . 1 1 1 37 GLY H . . . . . . . . . . 153 . 50196 1 >> 74 2 1 . . 109.660 . . 1 1 1 37 GLY N . . . . . . . . . . 154 . 50196 1 >> 75 1 1 . . 8.510 . . 1 1 1 99 GLY H . . . . . . . . . . 37 . 50196 1 >> 75 2 1 . . 109.506 . . 1 1 1 99 GLY N . . . . . . . . . . 38 . 50196 1 >> 76 1 1 . . 8.384 . . 1 1 1 80 GLY H . . . . . . . . . . 1 . 50196 1 >> 76 2 1 . . 109.491 . . 1 1 1 80 GLY N . . . . . . . . . . 2 . 50196 1 >> 77 1 1 . . 8.410 . . 1 1 1 35 GLY H . . . . . . . . . . 113 . 50196 1 >> 77 2 1 . . 109.163 . . 1 1 1 35 GLY N . . . . . . . . . . 114 . 50196 1 >> 78 1 1 . . 8.292 . . 1 1 1 44 GLY H . . . . . . . . . . 77 . 50196 1 >> 78 2 1 . . 107.968 . . 1 1 1 44 GLY N . . . . . . . . . . 78 . 50196 1 >> 79 1 1 . . 7.544 . . 1 1 1 7 GLN HE21 . . . . . . . . . . 73 . 50196 1 >> 79 2 1 . . 112.641 . . 1 1 1 7 GLN NE2 . . . . . . . . . . 74 . 50196 1 >> 80 1 1 . . 7.449 . . 1 1 1 66 GLN HE22 . . . . . . . . . . 130 . 50196 1 >> 80 2 1 . . 112.456 . . 1 1 1 66 GLN NE2 . . . . . . . . . . 129 . 50196 1 >> 81 1 1 . . 6.888 . . 1 1 1 7 GLN HE22 . . . . . . . . . . 127 . 50196 1 >> 81 2 1 . . 112.639 . . 1 1 1 7 GLN NE2 . . . . . . . . . . 74 . 50196 1 >> 82 1 1 . . 6.792 . . 1 1 1 66 GLN HE21 . . . . . . . . . . 128 . 50196 1 >> 82 2 1 . . 112.457 . . 1 1 1 66 GLN NE2 . . . . . . . . . . 129 . 50196 1 >> 83 1 1 . . 8.279 . . 1 1 1 24 PHE H . . . . . . . . . . 162 . 50196 1 >> 83 2 1 . . 121.987 . . 1 1 1 24 PHE N . . . . . . . . . . 161 . 50196 1 >> 84 1 1 . . 8.307 . . 1 1 1 20 ASP H . . . . . . . . . . 170 . 50196 1 >> 84 2 1 . . 122.018 . . 1 1 1 20 ASP N . . . . . . . . . . 171 . 50196 1 >> 85 1 1 . . 8.490 . . 1 1 1 53 GLU H . . . . . . . . . . 176 . 50196 1 >> 85 2 1 . . 120.679 . . 1 1 1 53 GLU N . . . . . . . . . . 177 . 50196 1 >> 86 1 1 . . 7.969 . . 1 1 1 28 PHE H . . . . . . . . . . 178 . 50196 1 >> 86 2 1 . . 120.385 . . 1 1 1 28 PHE N . . . . . . . . . . 179 . 50196 1 >> 87 1 1 . . 8.200 . . 1 1 1 70 SER H . . . . . . . . . . 256 . 50196 1 >> 87 2 1 . . 117.358 . . 1 1 1 70 SER N . . . . . . . . . . 257 . 50196 1 >> 88 1 1 . . 8.423 . . 1 1 1 66 GLN H . . . . . . . . . . 433 . 50196 1 >> 88 2 1 . . 120.887 . . 1 1 1 66 GLN N . . . . . . . . . . 434 . 50196 1 >> 89 1 1 . . 8.334 . . 1 1 1 86 SER H . . . . . . . . . . 438 . 50196 1 >> 89 2 1 . . 116.739 . . 1 1 1 86 SER N . . . . . . . . . . 439 . 50196 1 >> 90 1 1 . . 8.436 . . 1 1 1 82 HIS H . . . . . . . . . . 491 . 50196 1 >> 90 2 1 . . 120.852 . . 1 1 1 82 HIS N . . . . . . . . . . 492 . 50196 1 >> 91 1 1 . . 8.308 . . 1 1 1 92 SER H . . . . . . . . . . 495 . 50196 1 >> 91 2 1 . . 117.599 . . 1 1 1 92 SER N . . . . . . . . . . 496 . 50196 1 >> 92 1 1 . . 8.513 . . 1 1 1 87 HIS H . . . . . . . . . . 493 . 50196 1 >> 92 2 1 . . 120.770 . . 1 1 1 87 HIS N . . . . . . . . . . 494 . 50196 1 >> 93 1 1 . . 6.880 . . 1 1 1 5 GLN HE21 . . . . . . . . . . 502 . 50196 1 >> 93 2 1 . . 112.397 . . 1 1 1 5 GLN NE2 . . . . . . . . . . 503 . 50196 1 >> 94 1 1 . . 7.517 . . 1 1 1 5 GLN HE22 . . . . . . . . . . 504 . 50196 1 >> 94 2 1 . . 112.397 . . 1 1 1 5 GLN NE2 . . . . . . . . . . 503 . 50196 1 >> 95 1 1 . . 7.416 . . 1 1 1 46 GLN HE21 . . . . . . . . . . 505 . 50196 1 >> 95 2 1 . . 112.392 . . 1 1 1 46 GLN NE2 . . . . . . . . . . 506 . 50196 1 >> 96 1 1 . . 6.824 . . 1 1 1 46 GLN HE22 . . . . . . . . . . 507 . 50196 1 >> 96 2 1 . . 112.392 . . 1 1 1 46 GLN NE2 . . . . . . . . . . 506 . 50196 1 >> 97 1 1 . . 8.334 . . 1 1 1 93 SER H . . . . . . . . . . 508 . 50196 1 >> 97 2 1 . . 117.601 . . 1 1 1 93 SER N . . . . . . . . . . 509 . 50196 1 >> >> stop_ >> >>save_ >> ; save_