data_51103 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 51103 _Entry.Title ; TIA-1 prion-like domain, relaxation data ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2021-09-26 _Entry.Accession_date 2021-09-26 _Entry.Last_release_date 2021-09-26 _Entry.Original_release_date 2021-09-26 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Naotaka Sekiyama . . . . 51103 2 Ken-ichi Akagi . . . . 51103 3 Takashi Kodama . S. . . 51103 4 Hidehito Tochio . . . . 51103 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID heteronucl_NOEs 1 51103 heteronucl_T1_relaxation 1 51103 heteronucl_T2_relaxation 1 51103 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID 'T1 relaxation values' 74 51103 'T2 relaxation values' 74 51103 'heteronuclear NOE values' 64 51103 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2022-09-23 2021-09-26 update BMRB 'update entry citation' 51103 1 . . 2022-08-17 2021-09-26 original author 'original release' 51103 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 51102 'TIA-1 prion-like domain, backbone chemical shifts' 51103 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 51103 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 36112647 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; ALS mutations in the TIA-1 prion-like domain trigger highly condensed pathogenic structures ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Proc. Natl. Acad. Sci. U. S. A.' _Citation.Journal_name_full 'Proceedings of the National Academy of Sciences of the United States of America' _Citation.Journal_volume 119 _Citation.Journal_issue 38 _Citation.Journal_ASTM . _Citation.Journal_ISSN 1091-6490 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first e2122523119 _Citation.Page_last e2122523119 _Citation.Year 2022 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Naotaka Sekiyama N. . . . 51103 1 2 Kiyofumi Takaba K. . . . 51103 1 3 Saori Maki-Yonekura S. . . . 51103 1 4 Ken-Ichi Akagi K. I. . . 51103 1 5 Yasuko Ohtani Y. . . . 51103 1 6 Kayo Imamura K. . . . 51103 1 7 Tsuyoshi Terakawa T. . . . 51103 1 8 Keitaro Yamashita K. . . . 51103 1 9 Daigo Inaoka D. . . . 51103 1 10 Koji Yonekura K. . . . 51103 1 11 Takashi Kodama T. S. . . 51103 1 12 Hidehito Tochio H. . . . 51103 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 51103 _Assembly.ID 1 _Assembly.Name 'TIA-1 prion-like domain' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'TIA-1 prion-like domain' 1 $entity_1 . . yes native no no . . . 51103 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 51103 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; MGSSHHHHHHHHHHHHSENL YFQGGQYVPNGWQVPAYGVY GQPWSQQGFNQTQSSAPWMG PNYSVPPPQGQNGSMLPSQP AGYRVAGYETQ ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq 'TIA-1 320-386' _Entity.Polymer_author_seq_details 'His-TEV-TIA1 320-386' _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites yes _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 91 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_biological_function.Biological_function _Entity_biological_function.Entry_ID _Entity_biological_function.Entity_ID 'RNA-binding protein' 51103 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 -10 MET . 51103 1 2 -9 GLY . 51103 1 3 -8 SER . 51103 1 4 -7 SER . 51103 1 5 -6 HIS . 51103 1 6 -5 HIS . 51103 1 7 -4 HIS . 51103 1 8 -3 HIS . 51103 1 9 -2 HIS . 51103 1 10 -1 HIS . 51103 1 11 0 HIS . 51103 1 12 1 HIS . 51103 1 13 2 HIS . 51103 1 14 3 HIS . 51103 1 15 4 HIS . 51103 1 16 5 HIS . 51103 1 17 6 SER . 51103 1 18 7 GLU . 51103 1 19 8 ASN . 51103 1 20 9 LEU . 51103 1 21 10 TYR . 51103 1 22 11 PHE . 51103 1 23 12 GLN . 51103 1 24 13 GLY . 51103 1 25 14 GLY . 51103 1 26 15 GLN . 51103 1 27 16 TYR . 51103 1 28 17 VAL . 51103 1 29 18 PRO . 51103 1 30 19 ASN . 51103 1 31 20 GLY . 51103 1 32 21 TRP . 51103 1 33 22 GLN . 51103 1 34 23 VAL . 51103 1 35 24 PRO . 51103 1 36 25 ALA . 51103 1 37 26 TYR . 51103 1 38 27 GLY . 51103 1 39 28 VAL . 51103 1 40 29 TYR . 51103 1 41 30 GLY . 51103 1 42 31 GLN . 51103 1 43 32 PRO . 51103 1 44 33 TRP . 51103 1 45 34 SER . 51103 1 46 35 GLN . 51103 1 47 36 GLN . 51103 1 48 37 GLY . 51103 1 49 38 PHE . 51103 1 50 39 ASN . 51103 1 51 40 GLN . 51103 1 52 41 THR . 51103 1 53 42 GLN . 51103 1 54 43 SER . 51103 1 55 44 SER . 51103 1 56 45 ALA . 51103 1 57 46 PRO . 51103 1 58 47 TRP . 51103 1 59 48 MET . 51103 1 60 49 GLY . 51103 1 61 50 PRO . 51103 1 62 51 ASN . 51103 1 63 52 TYR . 51103 1 64 53 SER . 51103 1 65 54 VAL . 51103 1 66 55 PRO . 51103 1 67 56 PRO . 51103 1 68 57 PRO . 51103 1 69 58 GLN . 51103 1 70 59 GLY . 51103 1 71 60 GLN . 51103 1 72 61 ASN . 51103 1 73 62 GLY . 51103 1 74 63 SER . 51103 1 75 64 MET . 51103 1 76 65 LEU . 51103 1 77 66 PRO . 51103 1 78 67 SER . 51103 1 79 68 GLN . 51103 1 80 69 PRO . 51103 1 81 70 ALA . 51103 1 82 71 GLY . 51103 1 83 72 TYR . 51103 1 84 73 ARG . 51103 1 85 74 VAL . 51103 1 86 75 ALA . 51103 1 87 76 GLY . 51103 1 88 77 TYR . 51103 1 89 78 GLU . 51103 1 90 79 THR . 51103 1 91 80 GLN . 51103 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . MET 1 1 51103 1 . GLY 2 2 51103 1 . SER 3 3 51103 1 . SER 4 4 51103 1 . HIS 5 5 51103 1 . HIS 6 6 51103 1 . HIS 7 7 51103 1 . HIS 8 8 51103 1 . HIS 9 9 51103 1 . HIS 10 10 51103 1 . HIS 11 11 51103 1 . HIS 12 12 51103 1 . HIS 13 13 51103 1 . HIS 14 14 51103 1 . HIS 15 15 51103 1 . HIS 16 16 51103 1 . SER 17 17 51103 1 . GLU 18 18 51103 1 . ASN 19 19 51103 1 . LEU 20 20 51103 1 . TYR 21 21 51103 1 . PHE 22 22 51103 1 . GLN 23 23 51103 1 . GLY 24 24 51103 1 . GLY 25 25 51103 1 . GLN 26 26 51103 1 . TYR 27 27 51103 1 . VAL 28 28 51103 1 . PRO 29 29 51103 1 . ASN 30 30 51103 1 . GLY 31 31 51103 1 . TRP 32 32 51103 1 . GLN 33 33 51103 1 . VAL 34 34 51103 1 . PRO 35 35 51103 1 . ALA 36 36 51103 1 . TYR 37 37 51103 1 . GLY 38 38 51103 1 . VAL 39 39 51103 1 . TYR 40 40 51103 1 . GLY 41 41 51103 1 . GLN 42 42 51103 1 . PRO 43 43 51103 1 . TRP 44 44 51103 1 . SER 45 45 51103 1 . GLN 46 46 51103 1 . GLN 47 47 51103 1 . GLY 48 48 51103 1 . PHE 49 49 51103 1 . ASN 50 50 51103 1 . GLN 51 51 51103 1 . THR 52 52 51103 1 . GLN 53 53 51103 1 . SER 54 54 51103 1 . SER 55 55 51103 1 . ALA 56 56 51103 1 . PRO 57 57 51103 1 . TRP 58 58 51103 1 . MET 59 59 51103 1 . GLY 60 60 51103 1 . PRO 61 61 51103 1 . ASN 62 62 51103 1 . TYR 63 63 51103 1 . SER 64 64 51103 1 . VAL 65 65 51103 1 . PRO 66 66 51103 1 . PRO 67 67 51103 1 . PRO 68 68 51103 1 . GLN 69 69 51103 1 . GLY 70 70 51103 1 . GLN 71 71 51103 1 . ASN 72 72 51103 1 . GLY 73 73 51103 1 . SER 74 74 51103 1 . MET 75 75 51103 1 . LEU 76 76 51103 1 . PRO 77 77 51103 1 . SER 78 78 51103 1 . GLN 79 79 51103 1 . PRO 80 80 51103 1 . ALA 81 81 51103 1 . GLY 82 82 51103 1 . TYR 83 83 51103 1 . ARG 84 84 51103 1 . VAL 85 85 51103 1 . ALA 86 86 51103 1 . GLY 87 87 51103 1 . TYR 88 88 51103 1 . GLU 89 89 51103 1 . THR 90 90 51103 1 . GLN 91 91 51103 1 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 51103 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 10090 organism . 'Mus musculus' Mouse . . Eukaryota Metazoa Mus musculus . . . . . . . . . . . . . 51103 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 51103 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli BL21(DE3) . . plasmid . . pET28b . . . 51103 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 51103 _Sample.ID 1 _Sample.Name 'TIA-1 prion-like domain' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'TIA-1 prion-like domain' '[U-99% 13C; U-99% 15N]' . . 1 $entity_1 . . 500 . . uM . . . . 51103 1 2 MES 'natural abundance' . . . . . . 50 . . mM . . . . 51103 1 3 'sodium chloride' 'natural abundance' . . . . . . 150 . . mM . . . . 51103 1 4 DTT 'natural abundance' . . . . . . 1 . . mM . . . . 51103 1 5 1,6-hexanediol 'natural abundance' . . . . . . 10 . . % . . . . 51103 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 51103 _Sample_condition_list.ID 1 _Sample_condition_list.Name sample_condition_1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 0.15 . M 51103 1 pH 6.5 . pH 51103 1 pressure 1 . atm 51103 1 temperature 310 . K 51103 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 51103 _Software.ID 1 _Software.Type . _Software.Name TOPSPIN _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID collection . 51103 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 51103 _Software.ID 2 _Software.Type . _Software.Name NMRPipe _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID processing . 51103 2 stop_ save_ save_software_3 _Software.Sf_category software _Software.Sf_framecode software_3 _Software.Entry_ID 51103 _Software.ID 3 _Software.Type . _Software.Name NMRFAM-SPARKY _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'data analysis' . 51103 3 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 51103 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name 'Bruker AVANCE II 800 MHz spectrometer' _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'AVANCE II' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 800 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 51103 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 'T1/R1 relaxation' no no . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51103 1 2 'T2/R2 relaxation' no no . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51103 1 3 '1H-15N heteronoe' no no . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51103 1 stop_ save_ ############################## # Heteronuclear NOE values # ############################## save_heteronucl_NOEs_1 _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode heteronucl_NOEs_1 _Heteronucl_NOE_list.Entry_ID 51103 _Heteronucl_NOE_list.ID 1 _Heteronucl_NOE_list.Name 'TIA-1 prion-like domain, heteronuclear NOE' _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 800.20376094 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val 1 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '1H-15N heteronoe' . . . 51103 1 stop_ loop_ _Heteronucl_NOE_software.Software_ID _Heteronucl_NOE_software.Software_label _Heteronucl_NOE_software.Method_ID _Heteronucl_NOE_software.Method_label _Heteronucl_NOE_software.Entry_ID _Heteronucl_NOE_software.Heteronucl_NOE_list_ID 1 $software_1 . . 51103 1 2 $software_2 . . 51103 1 3 $software_3 . . 51103 1 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.4647 0.0089 . . . . . . . . . . 51103 1 2 . 1 1 19 19 ASN N N 15 . 1 1 19 19 ASN H H 1 0.4812 0.0363 . . . . . . . . . . 51103 1 3 . 1 1 20 20 LEU N N 15 . 1 1 20 20 LEU H H 1 0.5843 0.0767 . . . . . . . . . . 51103 1 4 . 1 1 21 21 TYR N N 15 . 1 1 21 21 TYR H H 1 0.6080 0.0347 . . . . . . . . . . 51103 1 5 . 1 1 22 22 PHE N N 15 . 1 1 22 22 PHE H H 1 0.5982 0.0468 . . . . . . . . . . 51103 1 6 . 1 1 23 23 GLN N N 15 . 1 1 23 23 GLN H H 1 0.5807 0.0788 . . . . . . . . . . 51103 1 7 . 1 1 24 24 GLY N N 15 . 1 1 24 24 GLY H H 1 0.4722 0.0393 . . . . . . . . . . 51103 1 8 . 1 1 25 25 GLY N N 15 . 1 1 25 25 GLY H H 1 0.4557 0.0152 . . . . . . . . . . 51103 1 9 . 1 1 26 26 GLN N N 15 . 1 1 26 26 GLN H H 1 0.4027 0.0472 . . . . . . . . . . 51103 1 10 . 1 1 27 27 TYR N N 15 . 1 1 27 27 TYR H H 1 0.5721 0.0572 . . . . . . . . . . 51103 1 11 . 1 1 28 28 VAL N N 15 . 1 1 28 28 VAL H H 1 0.4287 0.0012 . . . . . . . . . . 51103 1 12 . 1 1 30 30 ASN N N 15 . 1 1 30 30 ASN H H 1 0.5760 0.0489 . . . . . . . . . . 51103 1 13 . 1 1 31 31 GLY N N 15 . 1 1 31 31 GLY H H 1 0.5119 0.0562 . . . . . . . . . . 51103 1 14 . 1 1 32 32 TRP N N 15 . 1 1 32 32 TRP H H 1 0.4770 0.0010 . . . . . . . . . . 51103 1 15 . 1 1 33 33 GLN N N 15 . 1 1 33 33 GLN H H 1 0.5459 0.0484 . . . . . . . . . . 51103 1 16 . 1 1 34 34 VAL N N 15 . 1 1 34 34 VAL H H 1 0.4354 0.0127 . . . . . . . . . . 51103 1 17 . 1 1 36 36 ALA N N 15 . 1 1 36 36 ALA H H 1 0.4273 0.0000 . . . . . . . . . . 51103 1 18 . 1 1 37 37 TYR N N 15 . 1 1 37 37 TYR H H 1 0.4549 0.0063 . . . . . . . . . . 51103 1 19 . 1 1 38 38 GLY N N 15 . 1 1 38 38 GLY H H 1 0.5099 0.0015 . . . . . . . . . . 51103 1 20 . 1 1 39 39 VAL N N 15 . 1 1 39 39 VAL H H 1 0.5766 0.0362 . . . . . . . . . . 51103 1 21 . 1 1 40 40 TYR N N 15 . 1 1 40 40 TYR H H 1 0.5048 0.0173 . . . . . . . . . . 51103 1 22 . 1 1 41 41 GLY N N 15 . 1 1 41 41 GLY H H 1 0.4244 0.0099 . . . . . . . . . . 51103 1 23 . 1 1 42 42 GLN N N 15 . 1 1 42 42 GLN H H 1 0.5821 0.0160 . . . . . . . . . . 51103 1 24 . 1 1 44 44 TRP N N 15 . 1 1 44 44 TRP H H 1 0.6324 0.0482 . . . . . . . . . . 51103 1 25 . 1 1 45 45 SER N N 15 . 1 1 45 45 SER H H 1 0.5613 0.0421 . . . . . . . . . . 51103 1 26 . 1 1 46 46 GLN N N 15 . 1 1 46 46 GLN H H 1 0.4430 0.0030 . . . . . . . . . . 51103 1 27 . 1 1 47 47 GLN N N 15 . 1 1 47 47 GLN H H 1 0.5346 0.0516 . . . . . . . . . . 51103 1 28 . 1 1 48 48 GLY N N 15 . 1 1 48 48 GLY H H 1 0.4537 0.0662 . . . . . . . . . . 51103 1 29 . 1 1 49 49 PHE N N 15 . 1 1 49 49 PHE H H 1 0.5137 0.0613 . . . . . . . . . . 51103 1 30 . 1 1 50 50 ASN N N 15 . 1 1 50 50 ASN H H 1 0.3799 0.0090 . . . . . . . . . . 51103 1 31 . 1 1 51 51 GLN N N 15 . 1 1 51 51 GLN H H 1 0.4986 0.0862 . . . . . . . . . . 51103 1 32 . 1 1 52 52 THR N N 15 . 1 1 52 52 THR H H 1 0.3513 0.0248 . . . . . . . . . . 51103 1 33 . 1 1 53 53 GLN N N 15 . 1 1 53 53 GLN H H 1 0.3741 0.0800 . . . . . . . . . . 51103 1 34 . 1 1 54 54 SER N N 15 . 1 1 54 54 SER H H 1 0.3717 0.0491 . . . . . . . . . . 51103 1 35 . 1 1 55 55 SER N N 15 . 1 1 55 55 SER H H 1 0.3747 0.0502 . . . . . . . . . . 51103 1 36 . 1 1 56 56 ALA N N 15 . 1 1 56 56 ALA H H 1 0.3770 0.0586 . . . . . . . . . . 51103 1 37 . 1 1 58 58 TRP N N 15 . 1 1 58 58 TRP H H 1 0.3998 0.0055 . . . . . . . . . . 51103 1 38 . 1 1 59 59 MET N N 15 . 1 1 59 59 MET H H 1 0.5645 0.0386 . . . . . . . . . . 51103 1 39 . 1 1 60 60 GLY N N 15 . 1 1 60 60 GLY H H 1 0.4380 0.0723 . . . . . . . . . . 51103 1 40 . 1 1 62 62 ASN N N 15 . 1 1 62 62 ASN H H 1 0.3659 0.0120 . . . . . . . . . . 51103 1 41 . 1 1 63 63 TYR N N 15 . 1 1 63 63 TYR H H 1 0.4770 0.0010 . . . . . . . . . . 51103 1 42 . 1 1 64 64 SER N N 15 . 1 1 64 64 SER H H 1 0.4863 0.0517 . . . . . . . . . . 51103 1 43 . 1 1 65 65 VAL N N 15 . 1 1 65 65 VAL H H 1 0.3493 0.0108 . . . . . . . . . . 51103 1 44 . 1 1 69 69 GLN N N 15 . 1 1 69 69 GLN H H 1 0.2783 0.0129 . . . . . . . . . . 51103 1 45 . 1 1 70 70 GLY N N 15 . 1 1 70 70 GLY H H 1 0.1455 0.0052 . . . . . . . . . . 51103 1 46 . 1 1 71 71 GLN N N 15 . 1 1 71 71 GLN H H 1 0.2414 0.0785 . . . . . . . . . . 51103 1 47 . 1 1 72 72 ASN N N 15 . 1 1 72 72 ASN H H 1 0.1377 0.0224 . . . . . . . . . . 51103 1 48 . 1 1 73 73 GLY N N 15 . 1 1 73 73 GLY H H 1 0.0749 0.0054 . . . . . . . . . . 51103 1 49 . 1 1 74 74 SER N N 15 . 1 1 74 74 SER H H 1 0.1505 0.0260 . . . . . . . . . . 51103 1 50 . 1 1 75 75 MET N N 15 . 1 1 75 75 MET H H 1 0.2249 0.0428 . . . . . . . . . . 51103 1 51 . 1 1 76 76 LEU N N 15 . 1 1 76 76 LEU H H 1 0.0881 0.0264 . . . . . . . . . . 51103 1 52 . 1 1 78 78 SER N N 15 . 1 1 78 78 SER H H 1 0.2981 0.0616 . . . . . . . . . . 51103 1 53 . 1 1 79 79 GLN N N 15 . 1 1 79 79 GLN H H 1 0.3602 0.0385 . . . . . . . . . . 51103 1 54 . 1 1 81 81 ALA N N 15 . 1 1 81 81 ALA H H 1 0.1011 0.0194 . . . . . . . . . . 51103 1 55 . 1 1 82 82 GLY N N 15 . 1 1 82 82 GLY H H 1 0.2744 0.0640 . . . . . . . . . . 51103 1 56 . 1 1 83 83 TYR N N 15 . 1 1 83 83 TYR H H 1 0.2834 0.0111 . . . . . . . . . . 51103 1 57 . 1 1 84 84 ARG N N 15 . 1 1 84 84 ARG H H 1 0.2241 0.0264 . . . . . . . . . . 51103 1 58 . 1 1 85 85 VAL N N 15 . 1 1 85 85 VAL H H 1 0.2506 0.0528 . . . . . . . . . . 51103 1 59 . 1 1 86 86 ALA N N 15 . 1 1 86 86 ALA H H 1 0.2037 0.0241 . . . . . . . . . . 51103 1 60 . 1 1 87 87 GLY N N 15 . 1 1 87 87 GLY H H 1 0.1408 0.0301 . . . . . . . . . . 51103 1 61 . 1 1 88 88 TYR N N 15 . 1 1 88 88 TYR H H 1 0.3201 0.0056 . . . . . . . . . . 51103 1 62 . 1 1 89 89 GLU N N 15 . 1 1 89 89 GLU H H 1 0.1743 0.0887 . . . . . . . . . . 51103 1 63 . 1 1 90 90 THR N N 15 . 1 1 90 90 THR H H 1 -0.5401 0.1209 . . . . . . . . . . 51103 1 64 . 1 1 91 91 GLN N N 15 . 1 1 91 91 GLN H H 1 -0.7071 0.0700 . . . . . . . . . . 51103 1 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_heteronucl_T1_relaxation_1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_1 _Heteronucl_T1_list.Entry_ID 51103 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Name 'TIA-1 prion-like domain, T1' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 800.20376094 _Heteronucl_T1_list.T1_coherence_type Iz _Heteronucl_T1_list.T1_val_units s _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 'T1/R1 relaxation' . . . 51103 1 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 51103 1 2 $software_2 . . 51103 1 3 $software_3 . . 51103 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 18 18 GLU N N 15 0.643 0.003 . . . . . 51103 1 2 . 1 1 19 19 ASN N N 15 0.647 0.001 . . . . . 51103 1 3 . 1 1 20 20 LEU N N 15 0.628 0.006 . . . . . 51103 1 4 . 1 1 21 21 TYR N N 15 0.619 0.005 . . . . . 51103 1 5 . 1 1 22 22 PHE N N 15 0.607 0.001 . . . . . 51103 1 6 . 1 1 23 23 GLN N N 15 0.629 0.001 . . . . . 51103 1 7 . 1 1 24 24 GLY N N 15 0.676 0.013 . . . . . 51103 1 8 . 1 1 25 25 GLY N N 15 0.654 0.001 . . . . . 51103 1 9 . 1 1 26 26 GLN N N 15 0.661 0.001 . . . . . 51103 1 10 . 1 1 27 27 TYR N N 15 0.632 0.000 . . . . . 51103 1 11 . 1 1 28 28 VAL N N 15 0.647 0.006 . . . . . 51103 1 12 . 1 1 29 29 PRO N N 15 0.000 0.000 . . . . . 51103 1 13 . 1 1 30 30 ASN N N 15 0.669 0.001 . . . . . 51103 1 14 . 1 1 31 31 GLY N N 15 0.675 0.007 . . . . . 51103 1 15 . 1 1 32 32 TRP N N 15 0.642 0.002 . . . . . 51103 1 16 . 1 1 33 33 GLN N N 15 0.627 0.003 . . . . . 51103 1 17 . 1 1 34 34 VAL N N 15 0.652 0.001 . . . . . 51103 1 18 . 1 1 35 35 PRO N N 15 0.000 0.000 . . . . . 51103 1 19 . 1 1 36 36 ALA N N 15 0.663 0.001 . . . . . 51103 1 20 . 1 1 37 37 TYR N N 15 0.676 0.001 . . . . . 51103 1 21 . 1 1 38 38 GLY N N 15 0.639 0.000 . . . . . 51103 1 22 . 1 1 39 39 VAL N N 15 0.639 0.003 . . . . . 51103 1 23 . 1 1 40 40 TYR N N 15 0.618 0.003 . . . . . 51103 1 24 . 1 1 41 41 GLY N N 15 0.643 0.000 . . . . . 51103 1 25 . 1 1 42 42 GLN N N 15 0.646 0.008 . . . . . 51103 1 26 . 1 1 43 43 PRO N N 15 0.000 0.000 . . . . . 51103 1 27 . 1 1 44 44 TRP N N 15 0.621 0.006 . . . . . 51103 1 28 . 1 1 45 45 SER N N 15 0.617 0.004 . . . . . 51103 1 29 . 1 1 46 46 GLN N N 15 0.625 0.001 . . . . . 51103 1 30 . 1 1 47 47 GLN N N 15 0.645 0.003 . . . . . 51103 1 31 . 1 1 48 48 GLY N N 15 0.669 0.002 . . . . . 51103 1 32 . 1 1 49 49 PHE N N 15 0.644 0.002 . . . . . 51103 1 33 . 1 1 50 50 ASN N N 15 0.654 0.003 . . . . . 51103 1 34 . 1 1 51 51 GLN N N 15 0.667 0.002 . . . . . 51103 1 35 . 1 1 52 52 THR N N 15 0.656 0.002 . . . . . 51103 1 36 . 1 1 53 53 GLN N N 15 0.659 0.006 . . . . . 51103 1 37 . 1 1 54 54 SER N N 15 0.725 0.006 . . . . . 51103 1 38 . 1 1 55 55 SER N N 15 0.728 0.001 . . . . . 51103 1 39 . 1 1 56 56 ALA N N 15 0.693 0.003 . . . . . 51103 1 40 . 1 1 57 57 PRO N N 15 0.000 0.000 . . . . . 51103 1 41 . 1 1 58 58 TRP N N 15 0.644 0.001 . . . . . 51103 1 42 . 1 1 59 59 MET N N 15 0.624 0.003 . . . . . 51103 1 43 . 1 1 60 60 GLY N N 15 0.702 0.003 . . . . . 51103 1 44 . 1 1 61 61 PRO N N 15 0.000 0.000 . . . . . 51103 1 45 . 1 1 62 62 ASN N N 15 0.687 0.001 . . . . . 51103 1 46 . 1 1 63 63 TYR N N 15 0.642 0.002 . . . . . 51103 1 47 . 1 1 64 64 SER N N 15 0.681 0.007 . . . . . 51103 1 48 . 1 1 65 65 VAL N N 15 0.686 0.003 . . . . . 51103 1 49 . 1 1 66 66 PRO N N 15 0.000 0.000 . . . . . 51103 1 50 . 1 1 67 67 PRO N N 15 0.000 0.000 . . . . . 51103 1 51 . 1 1 68 68 PRO N N 15 0.000 0.000 . . . . . 51103 1 52 . 1 1 69 69 GLN N N 15 0.697 0.000 . . . . . 51103 1 53 . 1 1 70 70 GLY N N 15 0.733 0.001 . . . . . 51103 1 54 . 1 1 71 71 GLN N N 15 0.736 0.002 . . . . . 51103 1 55 . 1 1 72 72 ASN N N 15 0.755 0.004 . . . . . 51103 1 56 . 1 1 73 73 GLY N N 15 0.767 0.007 . . . . . 51103 1 57 . 1 1 74 74 SER N N 15 0.723 0.003 . . . . . 51103 1 58 . 1 1 75 75 MET N N 15 0.715 0.001 . . . . . 51103 1 59 . 1 1 76 76 LEU N N 15 0.711 0.005 . . . . . 51103 1 60 . 1 1 77 77 PRO N N 15 0.000 0.000 . . . . . 51103 1 61 . 1 1 78 78 SER N N 15 0.722 0.000 . . . . . 51103 1 62 . 1 1 79 79 GLN N N 15 0.717 0.010 . . . . . 51103 1 63 . 1 1 80 80 PRO N N 15 0.000 0.000 . . . . . 51103 1 64 . 1 1 81 81 ALA N N 15 0.706 0.001 . . . . . 51103 1 65 . 1 1 82 82 GLY N N 15 0.728 0.004 . . . . . 51103 1 66 . 1 1 83 83 TYR N N 15 0.647 0.003 . . . . . 51103 1 67 . 1 1 84 84 ARG N N 15 0.651 0.003 . . . . . 51103 1 68 . 1 1 85 85 VAL N N 15 0.663 0.002 . . . . . 51103 1 69 . 1 1 86 86 ALA N N 15 0.667 0.002 . . . . . 51103 1 70 . 1 1 87 87 GLY N N 15 0.745 0.007 . . . . . 51103 1 71 . 1 1 88 88 TYR N N 15 0.677 0.001 . . . . . 51103 1 72 . 1 1 89 89 GLU N N 15 0.706 0.002 . . . . . 51103 1 73 . 1 1 90 90 THR N N 15 0.796 0.005 . . . . . 51103 1 74 . 1 1 91 91 GLN N N 15 0.967 0.001 . . . . . 51103 1 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Entry_ID 51103 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Name 'TIA-1 prion-like domain, T2' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method 'no calibration applied' _Heteronucl_T2_list.Temp_control_method 'no temperature control applied' _Heteronucl_T2_list.Spectrometer_frequency_1H 800.20376094 _Heteronucl_T2_list.T2_coherence_type I(+,-) _Heteronucl_T2_list.T2_val_units s _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 2 'T2/R2 relaxation' . . . 51103 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 51103 1 2 $software_2 . . 51103 1 3 $software_3 . . 51103 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 18 18 GLU N N 15 0.236 0.005 0 0 . . . . . 51103 1 2 . 1 1 19 19 ASN N N 15 0.202 0.003 0 0 . . . . . 51103 1 3 . 1 1 20 20 LEU N N 15 0.228 0.002 0 0 . . . . . 51103 1 4 . 1 1 21 21 TYR N N 15 0.189 0.000 0 0 . . . . . 51103 1 5 . 1 1 22 22 PHE N N 15 0.211 0.001 0 0 . . . . . 51103 1 6 . 1 1 23 23 GLN N N 15 0.228 0.003 0 0 . . . . . 51103 1 7 . 1 1 24 24 GLY N N 15 0.223 0.001 0 0 . . . . . 51103 1 8 . 1 1 25 25 GLY N N 15 0.233 0.000 0 0 . . . . . 51103 1 9 . 1 1 26 26 GLN N N 15 0.217 0.002 0 0 . . . . . 51103 1 10 . 1 1 27 27 TYR N N 15 0.218 0.002 0 0 . . . . . 51103 1 11 . 1 1 28 28 VAL N N 15 0.210 0.003 0 0 . . . . . 51103 1 12 . 1 1 29 29 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 13 . 1 1 30 30 ASN N N 15 0.181 0.001 0 0 . . . . . 51103 1 14 . 1 1 31 31 GLY N N 15 0.205 0.002 0 0 . . . . . 51103 1 15 . 1 1 32 32 TRP N N 15 0.216 0.000 0 0 . . . . . 51103 1 16 . 1 1 33 33 GLN N N 15 0.208 0.001 0 0 . . . . . 51103 1 17 . 1 1 34 34 VAL N N 15 0.209 0.001 0 0 . . . . . 51103 1 18 . 1 1 35 35 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 19 . 1 1 36 36 ALA N N 15 0.224 0.002 0 0 . . . . . 51103 1 20 . 1 1 37 37 TYR N N 15 0.183 0.001 0 0 . . . . . 51103 1 21 . 1 1 38 38 GLY N N 15 0.204 0.003 0 0 . . . . . 51103 1 22 . 1 1 39 39 VAL N N 15 0.195 0.000 0 0 . . . . . 51103 1 23 . 1 1 40 40 TYR N N 15 0.212 0.001 0 0 . . . . . 51103 1 24 . 1 1 41 41 GLY N N 15 0.206 0.001 0 0 . . . . . 51103 1 25 . 1 1 42 42 GLN N N 15 0.207 0.000 0 0 . . . . . 51103 1 26 . 1 1 43 43 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 27 . 1 1 44 44 TRP N N 15 0.181 0.001 0 0 . . . . . 51103 1 28 . 1 1 45 45 SER N N 15 0.192 0.000 0 0 . . . . . 51103 1 29 . 1 1 46 46 GLN N N 15 0.232 0.003 0 0 . . . . . 51103 1 30 . 1 1 47 47 GLN N N 15 0.239 0.002 0 0 . . . . . 51103 1 31 . 1 1 48 48 GLY N N 15 0.260 0.001 0 0 . . . . . 51103 1 32 . 1 1 49 49 PHE N N 15 0.251 0.002 0 0 . . . . . 51103 1 33 . 1 1 50 50 ASN N N 15 0.261 0.000 0 0 . . . . . 51103 1 34 . 1 1 51 51 GLN N N 15 0.268 0.002 0 0 . . . . . 51103 1 35 . 1 1 52 52 THR N N 15 0.287 0.004 0 0 . . . . . 51103 1 36 . 1 1 53 53 GLN N N 15 0.281 0.001 0 0 . . . . . 51103 1 37 . 1 1 54 54 SER N N 15 0.260 0.002 0 0 . . . . . 51103 1 38 . 1 1 55 55 SER N N 15 0.244 0.001 0 0 . . . . . 51103 1 39 . 1 1 56 56 ALA N N 15 0.256 0.001 0 0 . . . . . 51103 1 40 . 1 1 57 57 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 41 . 1 1 58 58 TRP N N 15 0.184 0.001 0 0 . . . . . 51103 1 42 . 1 1 59 59 MET N N 15 0.231 0.007 0 0 . . . . . 51103 1 43 . 1 1 60 60 GLY N N 15 0.256 0.003 0 0 . . . . . 51103 1 44 . 1 1 61 61 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 45 . 1 1 62 62 ASN N N 15 0.209 0.001 0 0 . . . . . 51103 1 46 . 1 1 63 63 TYR N N 15 0.216 0.000 0 0 . . . . . 51103 1 47 . 1 1 64 64 SER N N 15 0.216 0.003 0 0 . . . . . 51103 1 48 . 1 1 65 65 VAL N N 15 0.284 0.003 0 0 . . . . . 51103 1 49 . 1 1 66 66 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 50 . 1 1 67 67 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 51 . 1 1 68 68 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 52 . 1 1 69 69 GLN N N 15 0.278 0.000 0 0 . . . . . 51103 1 53 . 1 1 70 70 GLY N N 15 0.320 0.000 0 0 . . . . . 51103 1 54 . 1 1 71 71 GLN N N 15 0.315 0.008 0 0 . . . . . 51103 1 55 . 1 1 72 72 ASN N N 15 0.321 0.004 0 0 . . . . . 51103 1 56 . 1 1 73 73 GLY N N 15 0.341 0.004 0 0 . . . . . 51103 1 57 . 1 1 74 74 SER N N 15 0.324 0.004 0 0 . . . . . 51103 1 58 . 1 1 75 75 MET N N 15 0.355 0.000 0 0 . . . . . 51103 1 59 . 1 1 76 76 LEU N N 15 0.315 0.003 0 0 . . . . . 51103 1 60 . 1 1 77 77 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 61 . 1 1 78 78 SER N N 15 0.318 0.001 0 0 . . . . . 51103 1 62 . 1 1 79 79 GLN N N 15 0.325 0.002 0 0 . . . . . 51103 1 63 . 1 1 80 80 PRO N N 15 0.000 0.000 0 0 . . . . . 51103 1 64 . 1 1 81 81 ALA N N 15 0.312 0.000 0 0 . . . . . 51103 1 65 . 1 1 82 82 GLY N N 15 0.311 0.000 0 0 . . . . . 51103 1 66 . 1 1 83 83 TYR N N 15 0.288 0.001 0 0 . . . . . 51103 1 67 . 1 1 84 84 ARG N N 15 0.316 0.001 0 0 . . . . . 51103 1 68 . 1 1 85 85 VAL N N 15 0.331 0.001 0 0 . . . . . 51103 1 69 . 1 1 86 86 ALA N N 15 0.302 0.004 0 0 . . . . . 51103 1 70 . 1 1 87 87 GLY N N 15 0.379 0.002 0 0 . . . . . 51103 1 71 . 1 1 88 88 TYR N N 15 0.319 0.003 0 0 . . . . . 51103 1 72 . 1 1 89 89 GLU N N 15 0.416 0.005 0 0 . . . . . 51103 1 73 . 1 1 90 90 THR N N 15 0.459 0.006 0 0 . . . . . 51103 1 74 . 1 1 91 91 GLN N N 15 0.673 0.003 0 0 . . . . . 51103 1 stop_ save_