data_51140 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 51140 _Entry.Title ; H3 tail in 193-bp nucleosome ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2021-10-14 _Entry.Accession_date 2021-10-14 _Entry.Last_release_date 2021-10-14 _Entry.Original_release_date 2021-10-14 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID 1 _Entry.Generated_software_label $software_1 _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Hideaki Ohtomo . . . . 51140 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 8 51140 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '15N chemical shifts' 145 51140 '1H chemical shifts' 145 51140 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2023-03-10 . original BMRB . 51140 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 51141 'H3 tail in 145-bp nucleosome' 51140 BMRB 51142 'H3 tail in 145-bp nucleosome with ubiquitin' 51140 BMRB 51143 'H3 tail in 193-bp nucleosome with ubiquitin' 51140 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 51140 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 36610636 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; H2A Ubiquitination Alters H3-tail Dynamics on Linker-DNA to Enhance H3K27 Methylation ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Mol. Biol.' _Citation.Journal_name_full 'Journal of molecular biology' _Citation.Journal_volume 435 _Citation.Journal_issue 4 _Citation.Journal_ASTM . _Citation.Journal_ISSN 1089-8638 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 167936 _Citation.Page_last 167936 _Citation.Year 2023 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Hideaki Ohtomo H. . . . 51140 1 2 Shinsuke Ito S. . . . 51140 1 3 Nicholas McKenzie N. J. . . 51140 1 4 Michael Uckelmann M. . . . 51140 1 5 Masatoshi Wakamori M. . . . 51140 1 6 Haruhiko Ehara H. . . . 51140 1 7 Ayako Furukawa A. . . . 51140 1 8 Yasuo Tsunaka Y. . . . 51140 1 9 Marika Shibata M. . . . 51140 1 10 Shun-Ichi Sekine S. I. . . 51140 1 11 Takashi Umehara T. . . . 51140 1 12 Chen Davidovich C. . . . 51140 1 13 Haruhiko Koseki H. . . . 51140 1 14 Yoshifumi Nishimura Y. . . . 51140 1 stop_ loop_ _Citation_keyword.Keyword _Citation_keyword.Entry_ID _Citation_keyword.Citation_ID H2AK119ub 51140 1 H3 51140 1 NCP 51140 1 histone 51140 1 'linker DNA' 51140 1 nucleosome 51140 1 ubiquitination 51140 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 51140 _Assembly.ID 1 _Assembly.Name nucleosome _Assembly.BMRB_code . _Assembly.Number_of_components 5 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'nucleosome, H3' 1 $entity_1 . . yes native no no . . . 51140 1 2 'nucleosome, H2A' 2 $entity_2 . . no native no no . . . 51140 1 3 'nucleosome, H2B' 3 $entity_3 . . no native no no . . . 51140 1 4 'nucleosome, H4' 4 $entity_4 . . no native no no . . . 51140 1 5 DNA 5 $entity_5 . . no native no no . . . 51140 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 51140 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; ARTKQTARKSTGGKAPRKQL ATKAARKSAPATGGVKKPHR YRPGTVALREIRRYQKSTEL LIRKLPFQRLVREIAQDFKT DLRFQSSAVMALQEACEAYL VGLFEDTNLCAIHAKRVTIM PKDIQLARRIRGERA ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states yes _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 135 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . ALA . 51140 1 2 . ARG . 51140 1 3 . THR . 51140 1 4 . LYS . 51140 1 5 . GLN . 51140 1 6 . THR . 51140 1 7 . ALA . 51140 1 8 . ARG . 51140 1 9 . LYS . 51140 1 10 . SER . 51140 1 11 . THR . 51140 1 12 . GLY . 51140 1 13 . GLY . 51140 1 14 . LYS . 51140 1 15 . ALA . 51140 1 16 . PRO . 51140 1 17 . ARG . 51140 1 18 . LYS . 51140 1 19 . GLN . 51140 1 20 . LEU . 51140 1 21 . ALA . 51140 1 22 . THR . 51140 1 23 . LYS . 51140 1 24 . ALA . 51140 1 25 . ALA . 51140 1 26 . ARG . 51140 1 27 . LYS . 51140 1 28 . SER . 51140 1 29 . ALA . 51140 1 30 . PRO . 51140 1 31 . ALA . 51140 1 32 . THR . 51140 1 33 . GLY . 51140 1 34 . GLY . 51140 1 35 . VAL . 51140 1 36 . LYS . 51140 1 37 . LYS . 51140 1 38 . PRO . 51140 1 39 . HIS . 51140 1 40 . ARG . 51140 1 41 . TYR . 51140 1 42 . ARG . 51140 1 43 . PRO . 51140 1 44 . GLY . 51140 1 45 . THR . 51140 1 46 . VAL . 51140 1 47 . ALA . 51140 1 48 . LEU . 51140 1 49 . ARG . 51140 1 50 . GLU . 51140 1 51 . ILE . 51140 1 52 . ARG . 51140 1 53 . ARG . 51140 1 54 . TYR . 51140 1 55 . GLN . 51140 1 56 . LYS . 51140 1 57 . SER . 51140 1 58 . THR . 51140 1 59 . GLU . 51140 1 60 . LEU . 51140 1 61 . LEU . 51140 1 62 . ILE . 51140 1 63 . ARG . 51140 1 64 . LYS . 51140 1 65 . LEU . 51140 1 66 . PRO . 51140 1 67 . PHE . 51140 1 68 . GLN . 51140 1 69 . ARG . 51140 1 70 . LEU . 51140 1 71 . VAL . 51140 1 72 . ARG . 51140 1 73 . GLU . 51140 1 74 . ILE . 51140 1 75 . ALA . 51140 1 76 . GLN . 51140 1 77 . ASP . 51140 1 78 . PHE . 51140 1 79 . LYS . 51140 1 80 . THR . 51140 1 81 . ASP . 51140 1 82 . LEU . 51140 1 83 . ARG . 51140 1 84 . PHE . 51140 1 85 . GLN . 51140 1 86 . SER . 51140 1 87 . SER . 51140 1 88 . ALA . 51140 1 89 . VAL . 51140 1 90 . MET . 51140 1 91 . ALA . 51140 1 92 . LEU . 51140 1 93 . GLN . 51140 1 94 . GLU . 51140 1 95 . ALA . 51140 1 96 . CYS . 51140 1 97 . GLU . 51140 1 98 . ALA . 51140 1 99 . TYR . 51140 1 100 . LEU . 51140 1 101 . VAL . 51140 1 102 . GLY . 51140 1 103 . LEU . 51140 1 104 . PHE . 51140 1 105 . GLU . 51140 1 106 . ASP . 51140 1 107 . THR . 51140 1 108 . ASN . 51140 1 109 . LEU . 51140 1 110 . CYS . 51140 1 111 . ALA . 51140 1 112 . ILE . 51140 1 113 . HIS . 51140 1 114 . ALA . 51140 1 115 . LYS . 51140 1 116 . ARG . 51140 1 117 . VAL . 51140 1 118 . THR . 51140 1 119 . ILE . 51140 1 120 . MET . 51140 1 121 . PRO . 51140 1 122 . LYS . 51140 1 123 . ASP . 51140 1 124 . ILE . 51140 1 125 . GLN . 51140 1 126 . LEU . 51140 1 127 . ALA . 51140 1 128 . ARG . 51140 1 129 . ARG . 51140 1 130 . ILE . 51140 1 131 . ARG . 51140 1 132 . GLY . 51140 1 133 . GLU . 51140 1 134 . ARG . 51140 1 135 . ALA . 51140 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . ALA 1 1 51140 1 . ARG 2 2 51140 1 . THR 3 3 51140 1 . LYS 4 4 51140 1 . GLN 5 5 51140 1 . THR 6 6 51140 1 . ALA 7 7 51140 1 . ARG 8 8 51140 1 . LYS 9 9 51140 1 . SER 10 10 51140 1 . THR 11 11 51140 1 . GLY 12 12 51140 1 . GLY 13 13 51140 1 . LYS 14 14 51140 1 . ALA 15 15 51140 1 . PRO 16 16 51140 1 . ARG 17 17 51140 1 . LYS 18 18 51140 1 . GLN 19 19 51140 1 . LEU 20 20 51140 1 . ALA 21 21 51140 1 . THR 22 22 51140 1 . LYS 23 23 51140 1 . ALA 24 24 51140 1 . ALA 25 25 51140 1 . ARG 26 26 51140 1 . LYS 27 27 51140 1 . SER 28 28 51140 1 . ALA 29 29 51140 1 . PRO 30 30 51140 1 . ALA 31 31 51140 1 . THR 32 32 51140 1 . GLY 33 33 51140 1 . GLY 34 34 51140 1 . VAL 35 35 51140 1 . LYS 36 36 51140 1 . LYS 37 37 51140 1 . PRO 38 38 51140 1 . HIS 39 39 51140 1 . ARG 40 40 51140 1 . TYR 41 41 51140 1 . ARG 42 42 51140 1 . PRO 43 43 51140 1 . GLY 44 44 51140 1 . THR 45 45 51140 1 . VAL 46 46 51140 1 . ALA 47 47 51140 1 . LEU 48 48 51140 1 . ARG 49 49 51140 1 . GLU 50 50 51140 1 . ILE 51 51 51140 1 . ARG 52 52 51140 1 . ARG 53 53 51140 1 . TYR 54 54 51140 1 . GLN 55 55 51140 1 . LYS 56 56 51140 1 . SER 57 57 51140 1 . THR 58 58 51140 1 . GLU 59 59 51140 1 . LEU 60 60 51140 1 . LEU 61 61 51140 1 . ILE 62 62 51140 1 . ARG 63 63 51140 1 . LYS 64 64 51140 1 . LEU 65 65 51140 1 . PRO 66 66 51140 1 . PHE 67 67 51140 1 . GLN 68 68 51140 1 . ARG 69 69 51140 1 . LEU 70 70 51140 1 . VAL 71 71 51140 1 . ARG 72 72 51140 1 . GLU 73 73 51140 1 . ILE 74 74 51140 1 . ALA 75 75 51140 1 . GLN 76 76 51140 1 . ASP 77 77 51140 1 . PHE 78 78 51140 1 . LYS 79 79 51140 1 . THR 80 80 51140 1 . ASP 81 81 51140 1 . LEU 82 82 51140 1 . ARG 83 83 51140 1 . PHE 84 84 51140 1 . GLN 85 85 51140 1 . SER 86 86 51140 1 . SER 87 87 51140 1 . ALA 88 88 51140 1 . VAL 89 89 51140 1 . MET 90 90 51140 1 . ALA 91 91 51140 1 . LEU 92 92 51140 1 . GLN 93 93 51140 1 . GLU 94 94 51140 1 . ALA 95 95 51140 1 . CYS 96 96 51140 1 . GLU 97 97 51140 1 . ALA 98 98 51140 1 . TYR 99 99 51140 1 . LEU 100 100 51140 1 . VAL 101 101 51140 1 . GLY 102 102 51140 1 . LEU 103 103 51140 1 . PHE 104 104 51140 1 . GLU 105 105 51140 1 . ASP 106 106 51140 1 . THR 107 107 51140 1 . ASN 108 108 51140 1 . LEU 109 109 51140 1 . CYS 110 110 51140 1 . ALA 111 111 51140 1 . ILE 112 112 51140 1 . HIS 113 113 51140 1 . ALA 114 114 51140 1 . LYS 115 115 51140 1 . ARG 116 116 51140 1 . VAL 117 117 51140 1 . THR 118 118 51140 1 . ILE 119 119 51140 1 . MET 120 120 51140 1 . PRO 121 121 51140 1 . LYS 122 122 51140 1 . ASP 123 123 51140 1 . ILE 124 124 51140 1 . GLN 125 125 51140 1 . LEU 126 126 51140 1 . ALA 127 127 51140 1 . ARG 128 128 51140 1 . ARG 129 129 51140 1 . ILE 130 130 51140 1 . ARG 131 131 51140 1 . GLY 132 132 51140 1 . GLU 133 133 51140 1 . ARG 134 134 51140 1 . ALA 135 135 51140 1 stop_ save_ save_entity_2 _Entity.Sf_category entity _Entity.Sf_framecode entity_2 _Entity.Entry_ID 51140 _Entity.ID 2 _Entity.BMRB_code . _Entity.Name entity_2 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GPGMSGRGKQGGKARAKAKT RSSRAGLQFPVGRVHRLLRK GNYSERVGAGAPVYLAAVLE YLTAEILELAGNAARDNKKT RIIPRHLQLAIRNDEELNKL LGRVTIAQGGVLPNIQAVLL PKKTESHHKAKGK ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 133 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 2 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . GLY . 51140 2 2 . PRO . 51140 2 3 . GLY . 51140 2 4 . MET . 51140 2 5 . SER . 51140 2 6 . GLY . 51140 2 7 . ARG . 51140 2 8 . GLY . 51140 2 9 . LYS . 51140 2 10 . GLN . 51140 2 11 . GLY . 51140 2 12 . GLY . 51140 2 13 . LYS . 51140 2 14 . ALA . 51140 2 15 . ARG . 51140 2 16 . ALA . 51140 2 17 . LYS . 51140 2 18 . ALA . 51140 2 19 . LYS . 51140 2 20 . THR . 51140 2 21 . ARG . 51140 2 22 . SER . 51140 2 23 . SER . 51140 2 24 . ARG . 51140 2 25 . ALA . 51140 2 26 . GLY . 51140 2 27 . LEU . 51140 2 28 . GLN . 51140 2 29 . PHE . 51140 2 30 . PRO . 51140 2 31 . VAL . 51140 2 32 . GLY . 51140 2 33 . ARG . 51140 2 34 . VAL . 51140 2 35 . HIS . 51140 2 36 . ARG . 51140 2 37 . LEU . 51140 2 38 . LEU . 51140 2 39 . ARG . 51140 2 40 . LYS . 51140 2 41 . GLY . 51140 2 42 . ASN . 51140 2 43 . TYR . 51140 2 44 . SER . 51140 2 45 . GLU . 51140 2 46 . ARG . 51140 2 47 . VAL . 51140 2 48 . GLY . 51140 2 49 . ALA . 51140 2 50 . GLY . 51140 2 51 . ALA . 51140 2 52 . PRO . 51140 2 53 . VAL . 51140 2 54 . TYR . 51140 2 55 . LEU . 51140 2 56 . ALA . 51140 2 57 . ALA . 51140 2 58 . VAL . 51140 2 59 . LEU . 51140 2 60 . GLU . 51140 2 61 . TYR . 51140 2 62 . LEU . 51140 2 63 . THR . 51140 2 64 . ALA . 51140 2 65 . GLU . 51140 2 66 . ILE . 51140 2 67 . LEU . 51140 2 68 . GLU . 51140 2 69 . LEU . 51140 2 70 . ALA . 51140 2 71 . GLY . 51140 2 72 . ASN . 51140 2 73 . ALA . 51140 2 74 . ALA . 51140 2 75 . ARG . 51140 2 76 . ASP . 51140 2 77 . ASN . 51140 2 78 . LYS . 51140 2 79 . LYS . 51140 2 80 . THR . 51140 2 81 . ARG . 51140 2 82 . ILE . 51140 2 83 . ILE . 51140 2 84 . PRO . 51140 2 85 . ARG . 51140 2 86 . HIS . 51140 2 87 . LEU . 51140 2 88 . GLN . 51140 2 89 . LEU . 51140 2 90 . ALA . 51140 2 91 . ILE . 51140 2 92 . ARG . 51140 2 93 . ASN . 51140 2 94 . ASP . 51140 2 95 . GLU . 51140 2 96 . GLU . 51140 2 97 . LEU . 51140 2 98 . ASN . 51140 2 99 . LYS . 51140 2 100 . LEU . 51140 2 101 . LEU . 51140 2 102 . GLY . 51140 2 103 . ARG . 51140 2 104 . VAL . 51140 2 105 . THR . 51140 2 106 . ILE . 51140 2 107 . ALA . 51140 2 108 . GLN . 51140 2 109 . GLY . 51140 2 110 . GLY . 51140 2 111 . VAL . 51140 2 112 . LEU . 51140 2 113 . PRO . 51140 2 114 . ASN . 51140 2 115 . ILE . 51140 2 116 . GLN . 51140 2 117 . ALA . 51140 2 118 . VAL . 51140 2 119 . LEU . 51140 2 120 . LEU . 51140 2 121 . PRO . 51140 2 122 . LYS . 51140 2 123 . LYS . 51140 2 124 . THR . 51140 2 125 . GLU . 51140 2 126 . SER . 51140 2 127 . HIS . 51140 2 128 . HIS . 51140 2 129 . LYS . 51140 2 130 . ALA . 51140 2 131 . LYS . 51140 2 132 . GLY . 51140 2 133 . LYS . 51140 2 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . GLY 1 1 51140 2 . PRO 2 2 51140 2 . GLY 3 3 51140 2 . MET 4 4 51140 2 . SER 5 5 51140 2 . GLY 6 6 51140 2 . ARG 7 7 51140 2 . GLY 8 8 51140 2 . LYS 9 9 51140 2 . GLN 10 10 51140 2 . GLY 11 11 51140 2 . GLY 12 12 51140 2 . LYS 13 13 51140 2 . ALA 14 14 51140 2 . ARG 15 15 51140 2 . ALA 16 16 51140 2 . LYS 17 17 51140 2 . ALA 18 18 51140 2 . LYS 19 19 51140 2 . THR 20 20 51140 2 . ARG 21 21 51140 2 . SER 22 22 51140 2 . SER 23 23 51140 2 . ARG 24 24 51140 2 . ALA 25 25 51140 2 . GLY 26 26 51140 2 . LEU 27 27 51140 2 . GLN 28 28 51140 2 . PHE 29 29 51140 2 . PRO 30 30 51140 2 . VAL 31 31 51140 2 . GLY 32 32 51140 2 . ARG 33 33 51140 2 . VAL 34 34 51140 2 . HIS 35 35 51140 2 . ARG 36 36 51140 2 . LEU 37 37 51140 2 . LEU 38 38 51140 2 . ARG 39 39 51140 2 . LYS 40 40 51140 2 . GLY 41 41 51140 2 . ASN 42 42 51140 2 . TYR 43 43 51140 2 . SER 44 44 51140 2 . GLU 45 45 51140 2 . ARG 46 46 51140 2 . VAL 47 47 51140 2 . GLY 48 48 51140 2 . ALA 49 49 51140 2 . GLY 50 50 51140 2 . ALA 51 51 51140 2 . PRO 52 52 51140 2 . VAL 53 53 51140 2 . TYR 54 54 51140 2 . LEU 55 55 51140 2 . ALA 56 56 51140 2 . ALA 57 57 51140 2 . VAL 58 58 51140 2 . LEU 59 59 51140 2 . GLU 60 60 51140 2 . TYR 61 61 51140 2 . LEU 62 62 51140 2 . THR 63 63 51140 2 . ALA 64 64 51140 2 . GLU 65 65 51140 2 . ILE 66 66 51140 2 . LEU 67 67 51140 2 . GLU 68 68 51140 2 . LEU 69 69 51140 2 . ALA 70 70 51140 2 . GLY 71 71 51140 2 . ASN 72 72 51140 2 . ALA 73 73 51140 2 . ALA 74 74 51140 2 . ARG 75 75 51140 2 . ASP 76 76 51140 2 . ASN 77 77 51140 2 . LYS 78 78 51140 2 . LYS 79 79 51140 2 . THR 80 80 51140 2 . ARG 81 81 51140 2 . ILE 82 82 51140 2 . ILE 83 83 51140 2 . PRO 84 84 51140 2 . ARG 85 85 51140 2 . HIS 86 86 51140 2 . LEU 87 87 51140 2 . GLN 88 88 51140 2 . LEU 89 89 51140 2 . ALA 90 90 51140 2 . ILE 91 91 51140 2 . ARG 92 92 51140 2 . ASN 93 93 51140 2 . ASP 94 94 51140 2 . GLU 95 95 51140 2 . GLU 96 96 51140 2 . LEU 97 97 51140 2 . ASN 98 98 51140 2 . LYS 99 99 51140 2 . LEU 100 100 51140 2 . LEU 101 101 51140 2 . GLY 102 102 51140 2 . ARG 103 103 51140 2 . VAL 104 104 51140 2 . THR 105 105 51140 2 . ILE 106 106 51140 2 . ALA 107 107 51140 2 . GLN 108 108 51140 2 . GLY 109 109 51140 2 . GLY 110 110 51140 2 . VAL 111 111 51140 2 . LEU 112 112 51140 2 . PRO 113 113 51140 2 . ASN 114 114 51140 2 . ILE 115 115 51140 2 . GLN 116 116 51140 2 . ALA 117 117 51140 2 . VAL 118 118 51140 2 . LEU 119 119 51140 2 . LEU 120 120 51140 2 . PRO 121 121 51140 2 . LYS 122 122 51140 2 . LYS 123 123 51140 2 . THR 124 124 51140 2 . GLU 125 125 51140 2 . SER 126 126 51140 2 . HIS 127 127 51140 2 . HIS 128 128 51140 2 . LYS 129 129 51140 2 . ALA 130 130 51140 2 . LYS 131 131 51140 2 . GLY 132 132 51140 2 . LYS 133 133 51140 2 stop_ save_ save_entity_3 _Entity.Sf_category entity _Entity.Sf_framecode entity_3 _Entity.Entry_ID 51140 _Entity.ID 3 _Entity.BMRB_code . _Entity.Name entity_3 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GPGMPEPAKSAPAPKKGSKK AVTKAQKKDGKKRKRSRKES YSIYVYKVLKQVHPDTGISS KAMGIMNSFVNDIFERIAGE ASRLAHYNKRSTITSREIQT AVRLLLPGELAKHAVSEGTK AVTKYTSAK ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 129 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 3 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . GLY . 51140 3 2 . PRO . 51140 3 3 . GLY . 51140 3 4 . MET . 51140 3 5 . PRO . 51140 3 6 . GLU . 51140 3 7 . PRO . 51140 3 8 . ALA . 51140 3 9 . LYS . 51140 3 10 . SER . 51140 3 11 . ALA . 51140 3 12 . PRO . 51140 3 13 . ALA . 51140 3 14 . PRO . 51140 3 15 . LYS . 51140 3 16 . LYS . 51140 3 17 . GLY . 51140 3 18 . SER . 51140 3 19 . LYS . 51140 3 20 . LYS . 51140 3 21 . ALA . 51140 3 22 . VAL . 51140 3 23 . THR . 51140 3 24 . LYS . 51140 3 25 . ALA . 51140 3 26 . GLN . 51140 3 27 . LYS . 51140 3 28 . LYS . 51140 3 29 . ASP . 51140 3 30 . GLY . 51140 3 31 . LYS . 51140 3 32 . LYS . 51140 3 33 . ARG . 51140 3 34 . LYS . 51140 3 35 . ARG . 51140 3 36 . SER . 51140 3 37 . ARG . 51140 3 38 . LYS . 51140 3 39 . GLU . 51140 3 40 . SER . 51140 3 41 . TYR . 51140 3 42 . SER . 51140 3 43 . ILE . 51140 3 44 . TYR . 51140 3 45 . VAL . 51140 3 46 . TYR . 51140 3 47 . LYS . 51140 3 48 . VAL . 51140 3 49 . LEU . 51140 3 50 . LYS . 51140 3 51 . GLN . 51140 3 52 . VAL . 51140 3 53 . HIS . 51140 3 54 . PRO . 51140 3 55 . ASP . 51140 3 56 . THR . 51140 3 57 . GLY . 51140 3 58 . ILE . 51140 3 59 . SER . 51140 3 60 . SER . 51140 3 61 . LYS . 51140 3 62 . ALA . 51140 3 63 . MET . 51140 3 64 . GLY . 51140 3 65 . ILE . 51140 3 66 . MET . 51140 3 67 . ASN . 51140 3 68 . SER . 51140 3 69 . PHE . 51140 3 70 . VAL . 51140 3 71 . ASN . 51140 3 72 . ASP . 51140 3 73 . ILE . 51140 3 74 . PHE . 51140 3 75 . GLU . 51140 3 76 . ARG . 51140 3 77 . ILE . 51140 3 78 . ALA . 51140 3 79 . GLY . 51140 3 80 . GLU . 51140 3 81 . ALA . 51140 3 82 . SER . 51140 3 83 . ARG . 51140 3 84 . LEU . 51140 3 85 . ALA . 51140 3 86 . HIS . 51140 3 87 . TYR . 51140 3 88 . ASN . 51140 3 89 . LYS . 51140 3 90 . ARG . 51140 3 91 . SER . 51140 3 92 . THR . 51140 3 93 . ILE . 51140 3 94 . THR . 51140 3 95 . SER . 51140 3 96 . ARG . 51140 3 97 . GLU . 51140 3 98 . ILE . 51140 3 99 . GLN . 51140 3 100 . THR . 51140 3 101 . ALA . 51140 3 102 . VAL . 51140 3 103 . ARG . 51140 3 104 . LEU . 51140 3 105 . LEU . 51140 3 106 . LEU . 51140 3 107 . PRO . 51140 3 108 . GLY . 51140 3 109 . GLU . 51140 3 110 . LEU . 51140 3 111 . ALA . 51140 3 112 . LYS . 51140 3 113 . HIS . 51140 3 114 . ALA . 51140 3 115 . VAL . 51140 3 116 . SER . 51140 3 117 . GLU . 51140 3 118 . GLY . 51140 3 119 . THR . 51140 3 120 . LYS . 51140 3 121 . ALA . 51140 3 122 . VAL . 51140 3 123 . THR . 51140 3 124 . LYS . 51140 3 125 . TYR . 51140 3 126 . THR . 51140 3 127 . SER . 51140 3 128 . ALA . 51140 3 129 . LYS . 51140 3 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . GLY 1 1 51140 3 . PRO 2 2 51140 3 . GLY 3 3 51140 3 . MET 4 4 51140 3 . PRO 5 5 51140 3 . GLU 6 6 51140 3 . PRO 7 7 51140 3 . ALA 8 8 51140 3 . LYS 9 9 51140 3 . SER 10 10 51140 3 . ALA 11 11 51140 3 . PRO 12 12 51140 3 . ALA 13 13 51140 3 . PRO 14 14 51140 3 . LYS 15 15 51140 3 . LYS 16 16 51140 3 . GLY 17 17 51140 3 . SER 18 18 51140 3 . LYS 19 19 51140 3 . LYS 20 20 51140 3 . ALA 21 21 51140 3 . VAL 22 22 51140 3 . THR 23 23 51140 3 . LYS 24 24 51140 3 . ALA 25 25 51140 3 . GLN 26 26 51140 3 . LYS 27 27 51140 3 . LYS 28 28 51140 3 . ASP 29 29 51140 3 . GLY 30 30 51140 3 . LYS 31 31 51140 3 . LYS 32 32 51140 3 . ARG 33 33 51140 3 . LYS 34 34 51140 3 . ARG 35 35 51140 3 . SER 36 36 51140 3 . ARG 37 37 51140 3 . LYS 38 38 51140 3 . GLU 39 39 51140 3 . SER 40 40 51140 3 . TYR 41 41 51140 3 . SER 42 42 51140 3 . ILE 43 43 51140 3 . TYR 44 44 51140 3 . VAL 45 45 51140 3 . TYR 46 46 51140 3 . LYS 47 47 51140 3 . VAL 48 48 51140 3 . LEU 49 49 51140 3 . LYS 50 50 51140 3 . GLN 51 51 51140 3 . VAL 52 52 51140 3 . HIS 53 53 51140 3 . PRO 54 54 51140 3 . ASP 55 55 51140 3 . THR 56 56 51140 3 . GLY 57 57 51140 3 . ILE 58 58 51140 3 . SER 59 59 51140 3 . SER 60 60 51140 3 . LYS 61 61 51140 3 . ALA 62 62 51140 3 . MET 63 63 51140 3 . GLY 64 64 51140 3 . ILE 65 65 51140 3 . MET 66 66 51140 3 . ASN 67 67 51140 3 . SER 68 68 51140 3 . PHE 69 69 51140 3 . VAL 70 70 51140 3 . ASN 71 71 51140 3 . ASP 72 72 51140 3 . ILE 73 73 51140 3 . PHE 74 74 51140 3 . GLU 75 75 51140 3 . ARG 76 76 51140 3 . ILE 77 77 51140 3 . ALA 78 78 51140 3 . GLY 79 79 51140 3 . GLU 80 80 51140 3 . ALA 81 81 51140 3 . SER 82 82 51140 3 . ARG 83 83 51140 3 . LEU 84 84 51140 3 . ALA 85 85 51140 3 . HIS 86 86 51140 3 . TYR 87 87 51140 3 . ASN 88 88 51140 3 . LYS 89 89 51140 3 . ARG 90 90 51140 3 . SER 91 91 51140 3 . THR 92 92 51140 3 . ILE 93 93 51140 3 . THR 94 94 51140 3 . SER 95 95 51140 3 . ARG 96 96 51140 3 . GLU 97 97 51140 3 . ILE 98 98 51140 3 . GLN 99 99 51140 3 . THR 100 100 51140 3 . ALA 101 101 51140 3 . VAL 102 102 51140 3 . ARG 103 103 51140 3 . LEU 104 104 51140 3 . LEU 105 105 51140 3 . LEU 106 106 51140 3 . PRO 107 107 51140 3 . GLY 108 108 51140 3 . GLU 109 109 51140 3 . LEU 110 110 51140 3 . ALA 111 111 51140 3 . LYS 112 112 51140 3 . HIS 113 113 51140 3 . ALA 114 114 51140 3 . VAL 115 115 51140 3 . SER 116 116 51140 3 . GLU 117 117 51140 3 . GLY 118 118 51140 3 . THR 119 119 51140 3 . LYS 120 120 51140 3 . ALA 121 121 51140 3 . VAL 122 122 51140 3 . THR 123 123 51140 3 . LYS 124 124 51140 3 . TYR 125 125 51140 3 . THR 126 126 51140 3 . SER 127 127 51140 3 . ALA 128 128 51140 3 . LYS 129 129 51140 3 stop_ save_ save_entity_4 _Entity.Sf_category entity _Entity.Sf_framecode entity_4 _Entity.Entry_ID 51140 _Entity.ID 4 _Entity.BMRB_code . _Entity.Name entity_4 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; SGRGKGGKGLGKGGAKRHRK VLRDNIQGITKPAIRRLARR GGVKRISGLIYEETRGVLKV FLENVIRDAVTYTEHAKRKT VTAMDVVYALKRQGRTLYGF GG ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 102 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 4 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . SER . 51140 4 2 . GLY . 51140 4 3 . ARG . 51140 4 4 . GLY . 51140 4 5 . LYS . 51140 4 6 . GLY . 51140 4 7 . GLY . 51140 4 8 . LYS . 51140 4 9 . GLY . 51140 4 10 . LEU . 51140 4 11 . GLY . 51140 4 12 . LYS . 51140 4 13 . GLY . 51140 4 14 . GLY . 51140 4 15 . ALA . 51140 4 16 . LYS . 51140 4 17 . ARG . 51140 4 18 . HIS . 51140 4 19 . ARG . 51140 4 20 . LYS . 51140 4 21 . VAL . 51140 4 22 . LEU . 51140 4 23 . ARG . 51140 4 24 . ASP . 51140 4 25 . ASN . 51140 4 26 . ILE . 51140 4 27 . GLN . 51140 4 28 . GLY . 51140 4 29 . ILE . 51140 4 30 . THR . 51140 4 31 . LYS . 51140 4 32 . PRO . 51140 4 33 . ALA . 51140 4 34 . ILE . 51140 4 35 . ARG . 51140 4 36 . ARG . 51140 4 37 . LEU . 51140 4 38 . ALA . 51140 4 39 . ARG . 51140 4 40 . ARG . 51140 4 41 . GLY . 51140 4 42 . GLY . 51140 4 43 . VAL . 51140 4 44 . LYS . 51140 4 45 . ARG . 51140 4 46 . ILE . 51140 4 47 . SER . 51140 4 48 . GLY . 51140 4 49 . LEU . 51140 4 50 . ILE . 51140 4 51 . TYR . 51140 4 52 . GLU . 51140 4 53 . GLU . 51140 4 54 . THR . 51140 4 55 . ARG . 51140 4 56 . GLY . 51140 4 57 . VAL . 51140 4 58 . LEU . 51140 4 59 . LYS . 51140 4 60 . VAL . 51140 4 61 . PHE . 51140 4 62 . LEU . 51140 4 63 . GLU . 51140 4 64 . ASN . 51140 4 65 . VAL . 51140 4 66 . ILE . 51140 4 67 . ARG . 51140 4 68 . ASP . 51140 4 69 . ALA . 51140 4 70 . VAL . 51140 4 71 . THR . 51140 4 72 . TYR . 51140 4 73 . THR . 51140 4 74 . GLU . 51140 4 75 . HIS . 51140 4 76 . ALA . 51140 4 77 . LYS . 51140 4 78 . ARG . 51140 4 79 . LYS . 51140 4 80 . THR . 51140 4 81 . VAL . 51140 4 82 . THR . 51140 4 83 . ALA . 51140 4 84 . MET . 51140 4 85 . ASP . 51140 4 86 . VAL . 51140 4 87 . VAL . 51140 4 88 . TYR . 51140 4 89 . ALA . 51140 4 90 . LEU . 51140 4 91 . LYS . 51140 4 92 . ARG . 51140 4 93 . GLN . 51140 4 94 . GLY . 51140 4 95 . ARG . 51140 4 96 . THR . 51140 4 97 . LEU . 51140 4 98 . TYR . 51140 4 99 . GLY . 51140 4 100 . PHE . 51140 4 101 . GLY . 51140 4 102 . GLY . 51140 4 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . SER 1 1 51140 4 . GLY 2 2 51140 4 . ARG 3 3 51140 4 . GLY 4 4 51140 4 . LYS 5 5 51140 4 . GLY 6 6 51140 4 . GLY 7 7 51140 4 . LYS 8 8 51140 4 . GLY 9 9 51140 4 . LEU 10 10 51140 4 . GLY 11 11 51140 4 . LYS 12 12 51140 4 . GLY 13 13 51140 4 . GLY 14 14 51140 4 . ALA 15 15 51140 4 . LYS 16 16 51140 4 . ARG 17 17 51140 4 . HIS 18 18 51140 4 . ARG 19 19 51140 4 . LYS 20 20 51140 4 . VAL 21 21 51140 4 . LEU 22 22 51140 4 . ARG 23 23 51140 4 . ASP 24 24 51140 4 . ASN 25 25 51140 4 . ILE 26 26 51140 4 . GLN 27 27 51140 4 . GLY 28 28 51140 4 . ILE 29 29 51140 4 . THR 30 30 51140 4 . LYS 31 31 51140 4 . PRO 32 32 51140 4 . ALA 33 33 51140 4 . ILE 34 34 51140 4 . ARG 35 35 51140 4 . ARG 36 36 51140 4 . LEU 37 37 51140 4 . ALA 38 38 51140 4 . ARG 39 39 51140 4 . ARG 40 40 51140 4 . GLY 41 41 51140 4 . GLY 42 42 51140 4 . VAL 43 43 51140 4 . LYS 44 44 51140 4 . ARG 45 45 51140 4 . ILE 46 46 51140 4 . SER 47 47 51140 4 . GLY 48 48 51140 4 . LEU 49 49 51140 4 . ILE 50 50 51140 4 . TYR 51 51 51140 4 . GLU 52 52 51140 4 . GLU 53 53 51140 4 . THR 54 54 51140 4 . ARG 55 55 51140 4 . GLY 56 56 51140 4 . VAL 57 57 51140 4 . LEU 58 58 51140 4 . LYS 59 59 51140 4 . VAL 60 60 51140 4 . PHE 61 61 51140 4 . LEU 62 62 51140 4 . GLU 63 63 51140 4 . ASN 64 64 51140 4 . VAL 65 65 51140 4 . ILE 66 66 51140 4 . ARG 67 67 51140 4 . ASP 68 68 51140 4 . ALA 69 69 51140 4 . VAL 70 70 51140 4 . THR 71 71 51140 4 . TYR 72 72 51140 4 . THR 73 73 51140 4 . GLU 74 74 51140 4 . HIS 75 75 51140 4 . ALA 76 76 51140 4 . LYS 77 77 51140 4 . ARG 78 78 51140 4 . LYS 79 79 51140 4 . THR 80 80 51140 4 . VAL 81 81 51140 4 . THR 82 82 51140 4 . ALA 83 83 51140 4 . MET 84 84 51140 4 . ASP 85 85 51140 4 . VAL 86 86 51140 4 . VAL 87 87 51140 4 . TYR 88 88 51140 4 . ALA 89 89 51140 4 . LEU 90 90 51140 4 . LYS 91 91 51140 4 . ARG 92 92 51140 4 . GLN 93 93 51140 4 . GLY 94 94 51140 4 . ARG 95 95 51140 4 . THR 96 96 51140 4 . LEU 97 97 51140 4 . TYR 98 98 51140 4 . GLY 99 99 51140 4 . PHE 100 100 51140 4 . GLY 101 101 51140 4 . GLY 102 102 51140 4 stop_ save_ save_entity_5 _Entity.Sf_category entity _Entity.Sf_framecode entity_5 _Entity.Entry_ID 51140 _Entity.ID 5 _Entity.BMRB_code . _Entity.Name entity_5 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polydeoxyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; ATCGGACCCTATCGCGAGCC AGGCCTGAGAATCCGGTGCC GAGGCCGCTCAATTGGTCGT AGACAGCTCTAGCACCGCTT AAACGCACGTACGCGCTGTC CCCCGCGTTTTAACCGCCAA GGGGATTACTCCCTAGTCTC CAGGCACGTGTCAGATATAT ACATCCAGGCCTTGTGTCGC GAAATTCATAGAT ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 193 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 5 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . DA . 51140 5 2 . DT . 51140 5 3 . DC . 51140 5 4 . DG . 51140 5 5 . DG . 51140 5 6 . DA . 51140 5 7 . DC . 51140 5 8 . DC . 51140 5 9 . DC . 51140 5 10 . DT . 51140 5 11 . DA . 51140 5 12 . DT . 51140 5 13 . DC . 51140 5 14 . DG . 51140 5 15 . DC . 51140 5 16 . DG . 51140 5 17 . DA . 51140 5 18 . DG . 51140 5 19 . DC . 51140 5 20 . DC . 51140 5 21 . DA . 51140 5 22 . DG . 51140 5 23 . DG . 51140 5 24 . DC . 51140 5 25 . DC . 51140 5 26 . DT . 51140 5 27 . DG . 51140 5 28 . DA . 51140 5 29 . DG . 51140 5 30 . DA . 51140 5 31 . DA . 51140 5 32 . DT . 51140 5 33 . DC . 51140 5 34 . DC . 51140 5 35 . DG . 51140 5 36 . DG . 51140 5 37 . DT . 51140 5 38 . DG . 51140 5 39 . DC . 51140 5 40 . DC . 51140 5 41 . DG . 51140 5 42 . DA . 51140 5 43 . DG . 51140 5 44 . DG . 51140 5 45 . DC . 51140 5 46 . DC . 51140 5 47 . DG . 51140 5 48 . DC . 51140 5 49 . DT . 51140 5 50 . DC . 51140 5 51 . DA . 51140 5 52 . DA . 51140 5 53 . DT . 51140 5 54 . DT . 51140 5 55 . DG . 51140 5 56 . DG . 51140 5 57 . DT . 51140 5 58 . DC . 51140 5 59 . DG . 51140 5 60 . DT . 51140 5 61 . DA . 51140 5 62 . DG . 51140 5 63 . DA . 51140 5 64 . DC . 51140 5 65 . DA . 51140 5 66 . DG . 51140 5 67 . DC . 51140 5 68 . DT . 51140 5 69 . DC . 51140 5 70 . DT . 51140 5 71 . DA . 51140 5 72 . DG . 51140 5 73 . DC . 51140 5 74 . DA . 51140 5 75 . DC . 51140 5 76 . DC . 51140 5 77 . DG . 51140 5 78 . DC . 51140 5 79 . DT . 51140 5 80 . DT . 51140 5 81 . DA . 51140 5 82 . DA . 51140 5 83 . DA . 51140 5 84 . DC . 51140 5 85 . DG . 51140 5 86 . DC . 51140 5 87 . DA . 51140 5 88 . DC . 51140 5 89 . DG . 51140 5 90 . DT . 51140 5 91 . DA . 51140 5 92 . DC . 51140 5 93 . DG . 51140 5 94 . DC . 51140 5 95 . DG . 51140 5 96 . DC . 51140 5 97 . DT . 51140 5 98 . DG . 51140 5 99 . DT . 51140 5 100 . DC . 51140 5 101 . DC . 51140 5 102 . DC . 51140 5 103 . DC . 51140 5 104 . DC . 51140 5 105 . DG . 51140 5 106 . DC . 51140 5 107 . DG . 51140 5 108 . DT . 51140 5 109 . DT . 51140 5 110 . DT . 51140 5 111 . DT . 51140 5 112 . DA . 51140 5 113 . DA . 51140 5 114 . DC . 51140 5 115 . DC . 51140 5 116 . DG . 51140 5 117 . DC . 51140 5 118 . DC . 51140 5 119 . DA . 51140 5 120 . DA . 51140 5 121 . DG . 51140 5 122 . DG . 51140 5 123 . DG . 51140 5 124 . DG . 51140 5 125 . DA . 51140 5 126 . DT . 51140 5 127 . DT . 51140 5 128 . DA . 51140 5 129 . DC . 51140 5 130 . DT . 51140 5 131 . DC . 51140 5 132 . DC . 51140 5 133 . DC . 51140 5 134 . DT . 51140 5 135 . DA . 51140 5 136 . DG . 51140 5 137 . DT . 51140 5 138 . DC . 51140 5 139 . DT . 51140 5 140 . DC . 51140 5 141 . DC . 51140 5 142 . DA . 51140 5 143 . DG . 51140 5 144 . DG . 51140 5 145 . DC . 51140 5 146 . DA . 51140 5 147 . DC . 51140 5 148 . DG . 51140 5 149 . DT . 51140 5 150 . DG . 51140 5 151 . DT . 51140 5 152 . DC . 51140 5 153 . DA . 51140 5 154 . DG . 51140 5 155 . DA . 51140 5 156 . DT . 51140 5 157 . DA . 51140 5 158 . DT . 51140 5 159 . DA . 51140 5 160 . DT . 51140 5 161 . DA . 51140 5 162 . DC . 51140 5 163 . DA . 51140 5 164 . DT . 51140 5 165 . DC . 51140 5 166 . DC . 51140 5 167 . DA . 51140 5 168 . DG . 51140 5 169 . DG . 51140 5 170 . DC . 51140 5 171 . DC . 51140 5 172 . DT . 51140 5 173 . DT . 51140 5 174 . DG . 51140 5 175 . DT . 51140 5 176 . DG . 51140 5 177 . DT . 51140 5 178 . DC . 51140 5 179 . DG . 51140 5 180 . DC . 51140 5 181 . DG . 51140 5 182 . DA . 51140 5 183 . DA . 51140 5 184 . DA . 51140 5 185 . DT . 51140 5 186 . DT . 51140 5 187 . DC . 51140 5 188 . DA . 51140 5 189 . DT . 51140 5 190 . DA . 51140 5 191 . DG . 51140 5 192 . DA . 51140 5 193 . DT . 51140 5 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . DA 1 1 51140 5 . DT 2 2 51140 5 . DC 3 3 51140 5 . DG 4 4 51140 5 . DG 5 5 51140 5 . DA 6 6 51140 5 . DC 7 7 51140 5 . DC 8 8 51140 5 . DC 9 9 51140 5 . DT 10 10 51140 5 . DA 11 11 51140 5 . DT 12 12 51140 5 . DC 13 13 51140 5 . DG 14 14 51140 5 . DC 15 15 51140 5 . DG 16 16 51140 5 . DA 17 17 51140 5 . DG 18 18 51140 5 . DC 19 19 51140 5 . DC 20 20 51140 5 . DA 21 21 51140 5 . DG 22 22 51140 5 . DG 23 23 51140 5 . DC 24 24 51140 5 . DC 25 25 51140 5 . DT 26 26 51140 5 . DG 27 27 51140 5 . DA 28 28 51140 5 . DG 29 29 51140 5 . DA 30 30 51140 5 . DA 31 31 51140 5 . DT 32 32 51140 5 . DC 33 33 51140 5 . DC 34 34 51140 5 . DG 35 35 51140 5 . DG 36 36 51140 5 . DT 37 37 51140 5 . DG 38 38 51140 5 . DC 39 39 51140 5 . DC 40 40 51140 5 . DG 41 41 51140 5 . DA 42 42 51140 5 . DG 43 43 51140 5 . DG 44 44 51140 5 . DC 45 45 51140 5 . DC 46 46 51140 5 . DG 47 47 51140 5 . DC 48 48 51140 5 . DT 49 49 51140 5 . DC 50 50 51140 5 . DA 51 51 51140 5 . DA 52 52 51140 5 . DT 53 53 51140 5 . DT 54 54 51140 5 . DG 55 55 51140 5 . DG 56 56 51140 5 . DT 57 57 51140 5 . DC 58 58 51140 5 . DG 59 59 51140 5 . DT 60 60 51140 5 . DA 61 61 51140 5 . DG 62 62 51140 5 . DA 63 63 51140 5 . DC 64 64 51140 5 . DA 65 65 51140 5 . DG 66 66 51140 5 . DC 67 67 51140 5 . DT 68 68 51140 5 . DC 69 69 51140 5 . DT 70 70 51140 5 . DA 71 71 51140 5 . DG 72 72 51140 5 . DC 73 73 51140 5 . DA 74 74 51140 5 . DC 75 75 51140 5 . DC 76 76 51140 5 . DG 77 77 51140 5 . DC 78 78 51140 5 . DT 79 79 51140 5 . DT 80 80 51140 5 . DA 81 81 51140 5 . DA 82 82 51140 5 . DA 83 83 51140 5 . DC 84 84 51140 5 . DG 85 85 51140 5 . DC 86 86 51140 5 . DA 87 87 51140 5 . DC 88 88 51140 5 . DG 89 89 51140 5 . DT 90 90 51140 5 . DA 91 91 51140 5 . DC 92 92 51140 5 . DG 93 93 51140 5 . DC 94 94 51140 5 . DG 95 95 51140 5 . DC 96 96 51140 5 . DT 97 97 51140 5 . DG 98 98 51140 5 . DT 99 99 51140 5 . DC 100 100 51140 5 . DC 101 101 51140 5 . DC 102 102 51140 5 . DC 103 103 51140 5 . DC 104 104 51140 5 . DG 105 105 51140 5 . DC 106 106 51140 5 . DG 107 107 51140 5 . DT 108 108 51140 5 . DT 109 109 51140 5 . DT 110 110 51140 5 . DT 111 111 51140 5 . DA 112 112 51140 5 . DA 113 113 51140 5 . DC 114 114 51140 5 . DC 115 115 51140 5 . DG 116 116 51140 5 . DC 117 117 51140 5 . DC 118 118 51140 5 . DA 119 119 51140 5 . DA 120 120 51140 5 . DG 121 121 51140 5 . DG 122 122 51140 5 . DG 123 123 51140 5 . DG 124 124 51140 5 . DA 125 125 51140 5 . DT 126 126 51140 5 . DT 127 127 51140 5 . DA 128 128 51140 5 . DC 129 129 51140 5 . DT 130 130 51140 5 . DC 131 131 51140 5 . DC 132 132 51140 5 . DC 133 133 51140 5 . DT 134 134 51140 5 . DA 135 135 51140 5 . DG 136 136 51140 5 . DT 137 137 51140 5 . DC 138 138 51140 5 . DT 139 139 51140 5 . DC 140 140 51140 5 . DC 141 141 51140 5 . DA 142 142 51140 5 . DG 143 143 51140 5 . DG 144 144 51140 5 . DC 145 145 51140 5 . DA 146 146 51140 5 . DC 147 147 51140 5 . DG 148 148 51140 5 . DT 149 149 51140 5 . DG 150 150 51140 5 . DT 151 151 51140 5 . DC 152 152 51140 5 . DA 153 153 51140 5 . DG 154 154 51140 5 . DA 155 155 51140 5 . DT 156 156 51140 5 . DA 157 157 51140 5 . DT 158 158 51140 5 . DA 159 159 51140 5 . DT 160 160 51140 5 . DA 161 161 51140 5 . DC 162 162 51140 5 . DA 163 163 51140 5 . DT 164 164 51140 5 . DC 165 165 51140 5 . DC 166 166 51140 5 . DA 167 167 51140 5 . DG 168 168 51140 5 . DG 169 169 51140 5 . DC 170 170 51140 5 . DC 171 171 51140 5 . DT 172 172 51140 5 . DT 173 173 51140 5 . DG 174 174 51140 5 . DT 175 175 51140 5 . DG 176 176 51140 5 . DT 177 177 51140 5 . DC 178 178 51140 5 . DG 179 179 51140 5 . DC 180 180 51140 5 . DG 181 181 51140 5 . DA 182 182 51140 5 . DA 183 183 51140 5 . DA 184 184 51140 5 . DT 185 185 51140 5 . DT 186 186 51140 5 . DC 187 187 51140 5 . DA 188 188 51140 5 . DT 189 189 51140 5 . DA 190 190 51140 5 . DG 191 191 51140 5 . DA 192 192 51140 5 . DT 193 193 51140 5 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 51140 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 51140 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 51140 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET . . . 51140 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 51140 _Sample.ID 1 _Sample.Name '193-bp nucleosome' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'histone H3' '[U-100% 13C; U-100% 15N; U-H]' . . 1 $entity_1 . . 10-60 . . uM . . . . 51140 1 2 'histone H2A' 'natural abundance' . . 2 $entity_2 . . 10-60 . . uM . . . . 51140 1 3 'histone H2B' 'natural abundance' . . 3 $entity_3 . . 10-60 . . uM . . . . 51140 1 4 'histone H4' 'natural abundance' . . 4 $entity_4 . . 10-60 . . uM . . . . 51140 1 5 '193-bp DNA' 'natural abundance' . . 5 $entity_5 . . 5-30 . . uM . . . . 51140 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 51140 _Sample_condition_list.ID 1 _Sample_condition_list.Name 'pH 6, 25 mM KCl' _Sample_condition_list.Details '25 mM MES pH 6.0, 25 mM KCl, 2 mM DTT' loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 25 . mM 51140 1 pH 6 . pH 51140 1 pressure 1 . atm 51140 1 temperature 293 . K 51140 1 stop_ save_ save_sample_conditions_2 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_2 _Sample_condition_list.Entry_ID 51140 _Sample_condition_list.ID 2 _Sample_condition_list.Name 'pH 6, 100 mM KCl' _Sample_condition_list.Details '25 mM MES pH 6.0, 100 mM KCl, 2 mM DTT' loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 100 . mM 51140 2 pH 6 . pH 51140 2 pressure 1 . atm 51140 2 temperature 293 . K 51140 2 stop_ save_ save_sample_conditions_3 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_3 _Sample_condition_list.Entry_ID 51140 _Sample_condition_list.ID 3 _Sample_condition_list.Name 'pH 6, 200 mM KCl' _Sample_condition_list.Details '25 mM MES pH 6.0, 200 mM KCl, 2 mM DTT' loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 200 . mM 51140 3 pH 6 . pH 51140 3 pressure 1 . atm 51140 3 temperature 293 . K 51140 3 stop_ save_ save_sample_conditions_4 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_4 _Sample_condition_list.Entry_ID 51140 _Sample_condition_list.ID 4 _Sample_condition_list.Name 'pH 6, 300 mM KCl' _Sample_condition_list.Details '25 mM MES pH 6.0, 300 mM KCl, 2 mM DTT' loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 300 . mM 51140 4 pH 6 . pH 51140 4 pressure 1 . atm 51140 4 temperature 293 . K 51140 4 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 51140 _Software.ID 1 _Software.Type . _Software.Name Olivia _Software.Version 1.16.x _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' . 51140 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 51140 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name 'Avance III HD 950-MHz spectrometer' _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'AVANCE III' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 950 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 51140 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 2 '3D HNCA' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 3 '3D HNCO' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 4 '3D HN(CA)CO' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 5 '3D HNCACB' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 6 '3D HN(CO)CACB' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 7 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 2 $sample_conditions_2 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 8 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 3 $sample_conditions_3 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 9 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 4 $sample_conditions_4 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 10 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 11 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 2 $sample_conditions_2 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 12 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 3 $sample_conditions_3 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 13 '2D 1H-15N TROSY' no . . . . . . . . . . . . 1 $sample_1 isotropic . . 4 $sample_conditions_4 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51140 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 51140 _Chem_shift_reference.ID 1 _Chem_shift_reference.Name DSS _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . MHz 950.14987365 external direct 1 . . . . . 51140 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Name H3-193-pH6-25KCl_1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 10 '2D 1H-15N TROSY' . . . 51140 1 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7380 0.0000 . 1 . . . . . 2 ARG H . 51140 1 2 . 1 . 1 2 2 ARG N N 15 121.1260 0.0000 . 1 . . . . . 2 ARG N . 51140 1 3 . 1 . 1 3 3 THR H H 1 8.3840 0.0000 . 1 . . . . . 3 THR H . 51140 1 4 . 1 . 1 3 3 THR N N 15 117.2910 0.0000 . 1 . . . . . 3 THR N . 51140 1 5 . 1 . 1 4 4 LYS H H 1 8.5230 0.0000 . 1 . . . . . 4 LYS H . 51140 1 6 . 1 . 1 4 4 LYS N N 15 124.5900 0.0000 . 1 . . . . . 4 LYS N . 51140 1 7 . 1 . 1 5 5 GLN H H 1 8.6030 0.0000 . 1 . . . . . 5 GLN H . 51140 1 8 . 1 . 1 5 5 GLN N N 15 122.6290 0.0000 . 1 . . . . . 5 GLN N . 51140 1 9 . 1 . 1 6 6 THR H H 1 8.1710 0.0000 . 1 . . . . . 6 THR H . 51140 1 10 . 1 . 1 6 6 THR N N 15 116.0920 0.0000 . 1 . . . . . 6 THR N . 51140 1 11 . 1 . 1 7 7 ALA H H 1 8.3660 0.0000 . 1 . . . . . 7 ALA H . 51140 1 12 . 1 . 1 7 7 ALA N N 15 126.8330 0.0000 . 1 . . . . . 7 ALA N . 51140 1 13 . 1 . 1 8 8 ARG H H 1 8.3260 0.0000 . 1 . . . . . 8 ARG H . 51140 1 14 . 1 . 1 8 8 ARG N N 15 121.0660 0.0000 . 1 . . . . . 8 ARG N . 51140 1 15 . 1 . 1 9 9 LYS H H 1 8.4580 0.0000 . 1 . . . . . 9 LYS H . 51140 1 16 . 1 . 1 9 9 LYS N N 15 123.3990 0.0000 . 1 . . . . . 9 LYS N . 51140 1 17 . 1 . 1 10 10 SER H H 1 8.4450 0.0000 . 1 . . . . . 10 SER H . 51140 1 18 . 1 . 1 10 10 SER N N 15 117.6610 0.0000 . 1 . . . . . 10 SER N . 51140 1 19 . 1 . 1 11 11 THR H H 1 8.2680 0.0000 . 1 . . . . . 11 THR H . 51140 1 20 . 1 . 1 11 11 THR N N 15 115.8420 0.0000 . 1 . . . . . 11 THR N . 51140 1 21 . 1 . 1 12 12 GLY H H 1 8.4410 0.0000 . 1 . . . . . 12 GLY H . 51140 1 22 . 1 . 1 12 12 GLY N N 15 111.4020 0.0000 . 1 . . . . . 12 GLY N . 51140 1 23 . 1 . 1 13 13 GLY H H 1 8.2980 0.0000 . 1 . . . . . 13 GLY H . 51140 1 24 . 1 . 1 13 13 GLY N N 15 109.3300 0.0000 . 1 . . . . . 13 GLY N . 51140 1 25 . 1 . 1 14 14 LYS H H 1 8.1820 0.0000 . 1 . . . . . 14 LYS H . 51140 1 26 . 1 . 1 14 14 LYS N N 15 121.3110 0.0000 . 1 . . . . . 14 LYS N . 51140 1 27 . 1 . 1 15 15 ALA H H 1 8.4300 0.0000 . 1 . . . . . 15 ALA H . 51140 1 28 . 1 . 1 15 15 ALA N N 15 127.3870 0.0000 . 1 . . . . . 15 ALA N . 51140 1 29 . 1 . 1 17 17 ARG H H 1 8.4730 0.0000 . 1 . . . . . 17 ARG H . 51140 1 30 . 1 . 1 17 17 ARG N N 15 122.0990 0.0000 . 1 . . . . . 17 ARG N . 51140 1 31 . 1 . 1 18 18 LYS H H 1 8.4490 0.0000 . 1 . . . . . 18 LYS H . 51140 1 32 . 1 . 1 18 18 LYS N N 15 123.3250 0.0000 . 1 . . . . . 18 LYS N . 51140 1 33 . 1 . 1 19 19 GLN H H 1 8.4300 0.0000 . 1 . . . . . 19 GLN H . 51140 1 34 . 1 . 1 19 19 GLN N N 15 122.1910 0.0000 . 1 . . . . . 19 GLN N . 51140 1 35 . 1 . 1 20 20 LEU H H 1 8.3310 0.0000 . 1 . . . . . 20 LEU H . 51140 1 36 . 1 . 1 20 20 LEU N N 15 124.2050 0.0000 . 1 . . . . . 20 LEU N . 51140 1 37 . 1 . 1 21 21 ALA H H 1 8.3770 0.0000 . 1 . . . . . 21 ALA H . 51140 1 38 . 1 . 1 21 21 ALA N N 15 125.1280 0.0000 . 1 . . . . . 21 ALA N . 51140 1 39 . 1 . 1 22 22 THR H H 1 8.0510 0.0000 . 1 . . . . . 22 THR H . 51140 1 40 . 1 . 1 22 22 THR N N 15 114.0110 0.0000 . 1 . . . . . 22 THR N . 51140 1 41 . 1 . 1 23 23 LYS H H 1 8.3040 0.0000 . 1 . . . . . 23 LYS H . 51140 1 42 . 1 . 1 23 23 LYS N N 15 124.0470 0.0000 . 1 . . . . . 23 LYS N . 51140 1 43 . 1 . 1 24 24 ALA H H 1 8.2840 0.0000 . 1 . . . . . 24 ALA H . 51140 1 44 . 1 . 1 24 24 ALA N N 15 125.1750 0.0000 . 1 . . . . . 24 ALA N . 51140 1 45 . 1 . 1 25 25 ALA H H 1 8.1880 0.0000 . 1 . . . . . 25 ALA H . 51140 1 46 . 1 . 1 25 25 ALA N N 15 123.5460 0.0000 . 1 . . . . . 25 ALA N . 51140 1 47 . 1 . 1 26 26 ARG H H 1 8.2230 0.0000 . 1 . . . . . 26 ARG H . 51140 1 48 . 1 . 1 26 26 ARG N N 15 120.6800 0.0000 . 1 . . . . . 26 ARG N . 51140 1 49 . 1 . 1 27 27 LYS H H 1 8.3540 0.0000 . 1 . . . . . 27 LYS H . 51140 1 50 . 1 . 1 27 27 LYS N N 15 122.9100 0.0000 . 1 . . . . . 27 LYS N . 51140 1 51 . 1 . 1 28 28 SER H H 1 8.2360 0.0000 . 1 . . . . . 28 SER H . 51140 1 52 . 1 . 1 28 28 SER N N 15 117.3210 0.0000 . 1 . . . . . 28 SER N . 51140 1 53 . 1 . 1 29 29 ALA H H 1 8.2810 0.0000 . 1 . . . . . 29 ALA H . 51140 1 54 . 1 . 1 29 29 ALA N N 15 127.4050 0.0000 . 1 . . . . . 29 ALA N . 51140 1 55 . 1 . 1 31 31 ALA H H 1 8.5130 0.0000 . 1 . . . . . 31 ALA H . 51140 1 56 . 1 . 1 31 31 ALA N N 15 124.9260 0.0000 . 1 . . . . . 31 ALA N . 51140 1 57 . 1 . 1 32 32 THR H H 1 8.0890 0.0000 . 1 . . . . . 32 THR H . 51140 1 58 . 1 . 1 32 32 THR N N 15 112.9280 0.0000 . 1 . . . . . 32 THR N . 51140 1 59 . 1 . 1 33 33 GLY H H 1 8.3980 0.0000 . 1 . . . . . 33 GLY H . 51140 1 60 . 1 . 1 33 33 GLY N N 15 111.4160 0.0000 . 1 . . . . . 33 GLY N . 51140 1 61 . 1 . 1 34 34 GLY H H 1 8.2630 0.0000 . 1 . . . . . 34 GLY H . 51140 1 62 . 1 . 1 34 34 GLY N N 15 109.3560 0.0000 . 1 . . . . . 34 GLY N . 51140 1 63 . 1 . 1 35 35 VAL H H 1 7.9460 0.0000 . 1 . . . . . 35 VAL H . 51140 1 64 . 1 . 1 35 35 VAL N N 15 119.8720 0.0000 . 1 . . . . . 35 VAL N . 51140 1 65 . 1 . 1 36 36 LYS H H 1 8.3640 0.0000 . 1 . . . . . 36 LYS H . 51140 1 66 . 1 . 1 36 36 LYS N N 15 126.4870 0.0000 . 1 . . . . . 36 LYS N . 51140 1 stop_ save_ save_assigned_chemical_shifts_2 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_2 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 2 _Assigned_chem_shift_list.Name H3-193-pH6-25KCl_1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 10 '2D 1H-15N TROSY' . . . 51140 2 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 2 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7690 0.0000 . 1 . . . . . 2 ARG H . 51140 2 2 . 1 . 1 2 2 ARG N N 15 121.1560 0.0000 . 1 . . . . . 2 ARG N . 51140 2 3 . 1 . 1 5 5 GLN H H 1 8.6110 0.0000 . 1 . . . . . 5 GLN H . 51140 2 4 . 1 . 1 5 5 GLN N N 15 122.6910 0.0000 . 1 . . . . . 5 GLN N . 51140 2 5 . 1 . 1 32 32 THR H H 1 8.1160 0.0000 . 1 . . . . . 32 THR H . 51140 2 6 . 1 . 1 32 32 THR N N 15 113.1240 0.0000 . 1 . . . . . 32 THR N . 51140 2 7 . 1 . 1 35 35 VAL H H 1 7.9740 0.0000 . 1 . . . . . 35 VAL H . 51140 2 8 . 1 . 1 35 35 VAL N N 15 119.9180 0.0000 . 1 . . . . . 35 VAL N . 51140 2 stop_ save_ save_assigned_chemical_shifts_3 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_3 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 3 _Assigned_chem_shift_list.Name H3-193-pH6-100KCl_1 _Assigned_chem_shift_list.Sample_condition_list_ID 2 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_2 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 11 '2D 1H-15N TROSY' . . . 51140 3 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 3 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7460 0.0000 . 1 . . . . . 2 ARG H . 51140 3 2 . 1 . 1 2 2 ARG N N 15 121.1710 0.0000 . 1 . . . . . 2 ARG N . 51140 3 3 . 1 . 1 3 3 THR H H 1 8.3830 0.0000 . 1 . . . . . 3 THR H . 51140 3 4 . 1 . 1 3 3 THR N N 15 117.2950 0.0000 . 1 . . . . . 3 THR N . 51140 3 5 . 1 . 1 4 4 LYS H H 1 8.5260 0.0000 . 1 . . . . . 4 LYS H . 51140 3 6 . 1 . 1 4 4 LYS N N 15 124.6030 0.0000 . 1 . . . . . 4 LYS N . 51140 3 7 . 1 . 1 5 5 GLN H H 1 8.5980 0.0000 . 1 . . . . . 5 GLN H . 51140 3 8 . 1 . 1 5 5 GLN N N 15 122.6930 0.0000 . 1 . . . . . 5 GLN N . 51140 3 9 . 1 . 1 6 6 THR H H 1 8.1800 0.0000 . 1 . . . . . 6 THR H . 51140 3 10 . 1 . 1 6 6 THR N N 15 116.1420 0.0000 . 1 . . . . . 6 THR N . 51140 3 11 . 1 . 1 7 7 ALA H H 1 8.3680 0.0000 . 1 . . . . . 7 ALA H . 51140 3 12 . 1 . 1 7 7 ALA N N 15 126.9010 0.0000 . 1 . . . . . 7 ALA N . 51140 3 13 . 1 . 1 8 8 ARG H H 1 8.3270 0.0000 . 1 . . . . . 8 ARG H . 51140 3 14 . 1 . 1 8 8 ARG N N 15 121.1010 0.0000 . 1 . . . . . 8 ARG N . 51140 3 15 . 1 . 1 9 9 LYS H H 1 8.4410 0.0000 . 1 . . . . . 9 LYS H . 51140 3 16 . 1 . 1 9 9 LYS N N 15 123.3430 0.0000 . 1 . . . . . 9 LYS N . 51140 3 17 . 1 . 1 10 10 SER H H 1 8.4470 0.0000 . 1 . . . . . 10 SER H . 51140 3 18 . 1 . 1 10 10 SER N N 15 117.7020 0.0000 . 1 . . . . . 10 SER N . 51140 3 19 . 1 . 1 11 11 THR H H 1 8.2680 0.0000 . 1 . . . . . 11 THR H . 51140 3 20 . 1 . 1 11 11 THR N N 15 115.8710 0.0000 . 1 . . . . . 11 THR N . 51140 3 21 . 1 . 1 12 12 GLY H H 1 8.4450 0.0000 . 1 . . . . . 12 GLY H . 51140 3 22 . 1 . 1 12 12 GLY N N 15 111.4040 0.0000 . 1 . . . . . 12 GLY N . 51140 3 23 . 1 . 1 13 13 GLY H H 1 8.3030 0.0000 . 1 . . . . . 13 GLY H . 51140 3 24 . 1 . 1 13 13 GLY N N 15 109.3530 0.0000 . 1 . . . . . 13 GLY N . 51140 3 25 . 1 . 1 14 14 LYS H H 1 8.1860 0.0000 . 1 . . . . . 14 LYS H . 51140 3 26 . 1 . 1 14 14 LYS N N 15 121.3090 0.0000 . 1 . . . . . 14 LYS N . 51140 3 27 . 1 . 1 15 15 ALA H H 1 8.4150 0.0000 . 1 . . . . . 15 ALA H . 51140 3 28 . 1 . 1 15 15 ALA N N 15 127.3160 0.0000 . 1 . . . . . 15 ALA N . 51140 3 29 . 1 . 1 17 17 ARG H H 1 8.4640 0.0000 . 1 . . . . . 17 ARG H . 51140 3 30 . 1 . 1 17 17 ARG N N 15 122.0670 0.0000 . 1 . . . . . 17 ARG N . 51140 3 31 . 1 . 1 18 18 LYS H H 1 8.4460 0.0000 . 1 . . . . . 18 LYS H . 51140 3 32 . 1 . 1 18 18 LYS N N 15 123.3760 0.0000 . 1 . . . . . 18 LYS N . 51140 3 33 . 1 . 1 19 19 GLN H H 1 8.4340 0.0000 . 1 . . . . . 19 GLN H . 51140 3 34 . 1 . 1 19 19 GLN N N 15 122.2790 0.0000 . 1 . . . . . 19 GLN N . 51140 3 35 . 1 . 1 20 20 LEU H H 1 8.3270 0.0000 . 1 . . . . . 20 LEU H . 51140 3 36 . 1 . 1 20 20 LEU N N 15 124.2300 0.0000 . 1 . . . . . 20 LEU N . 51140 3 37 . 1 . 1 21 21 ALA H H 1 8.3790 0.0000 . 1 . . . . . 21 ALA H . 51140 3 38 . 1 . 1 21 21 ALA N N 15 125.2160 0.0000 . 1 . . . . . 21 ALA N . 51140 3 39 . 1 . 1 22 22 THR H H 1 8.0520 0.0000 . 1 . . . . . 22 THR H . 51140 3 40 . 1 . 1 22 22 THR N N 15 114.0000 0.0000 . 1 . . . . . 22 THR N . 51140 3 41 . 1 . 1 23 23 LYS H H 1 8.3110 0.0000 . 1 . . . . . 23 LYS H . 51140 3 42 . 1 . 1 23 23 LYS N N 15 124.0400 0.0000 . 1 . . . . . 23 LYS N . 51140 3 43 . 1 . 1 24 24 ALA H H 1 8.2800 0.0000 . 1 . . . . . 24 ALA H . 51140 3 44 . 1 . 1 24 24 ALA N N 15 125.1990 0.0000 . 1 . . . . . 24 ALA N . 51140 3 45 . 1 . 1 25 25 ALA H H 1 8.1950 0.0000 . 1 . . . . . 25 ALA H . 51140 3 46 . 1 . 1 25 25 ALA N N 15 123.6480 0.0000 . 1 . . . . . 25 ALA N . 51140 3 47 . 1 . 1 26 26 ARG H H 1 8.2270 0.0000 . 1 . . . . . 26 ARG H . 51140 3 48 . 1 . 1 26 26 ARG N N 15 120.7060 0.0000 . 1 . . . . . 26 ARG N . 51140 3 49 . 1 . 1 27 27 LYS H H 1 8.3660 0.0000 . 1 . . . . . 27 LYS H . 51140 3 50 . 1 . 1 27 27 LYS N N 15 123.0650 0.0000 . 1 . . . . . 27 LYS N . 51140 3 51 . 1 . 1 28 28 SER H H 1 8.2530 0.0000 . 1 . . . . . 28 SER H . 51140 3 52 . 1 . 1 28 28 SER N N 15 117.4200 0.0000 . 1 . . . . . 28 SER N . 51140 3 53 . 1 . 1 29 29 ALA H H 1 8.2900 0.0000 . 1 . . . . . 29 ALA H . 51140 3 54 . 1 . 1 29 29 ALA N N 15 127.4080 0.0000 . 1 . . . . . 29 ALA N . 51140 3 55 . 1 . 1 31 31 ALA H H 1 8.5150 0.0000 . 1 . . . . . 31 ALA H . 51140 3 56 . 1 . 1 31 31 ALA N N 15 124.9460 0.0000 . 1 . . . . . 31 ALA N . 51140 3 57 . 1 . 1 32 32 THR H H 1 8.0940 0.0000 . 1 . . . . . 32 THR H . 51140 3 58 . 1 . 1 32 32 THR N N 15 112.9850 0.0000 . 1 . . . . . 32 THR N . 51140 3 59 . 1 . 1 33 33 GLY H H 1 8.4010 0.0000 . 1 . . . . . 33 GLY H . 51140 3 60 . 1 . 1 33 33 GLY N N 15 111.4150 0.0000 . 1 . . . . . 33 GLY N . 51140 3 61 . 1 . 1 34 34 GLY H H 1 8.2720 0.0000 . 1 . . . . . 34 GLY H . 51140 3 62 . 1 . 1 34 34 GLY N N 15 109.3850 0.0000 . 1 . . . . . 34 GLY N . 51140 3 63 . 1 . 1 35 35 VAL H H 1 7.9580 0.0000 . 1 . . . . . 35 VAL H . 51140 3 64 . 1 . 1 35 35 VAL N N 15 119.9000 0.0000 . 1 . . . . . 35 VAL N . 51140 3 65 . 1 . 1 36 36 LYS H H 1 8.3660 0.0000 . 1 . . . . . 36 LYS H . 51140 3 66 . 1 . 1 36 36 LYS N N 15 126.4990 0.0000 . 1 . . . . . 36 LYS N . 51140 3 stop_ save_ save_assigned_chemical_shifts_4 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_4 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 4 _Assigned_chem_shift_list.Name H3-193-pH6-100KCl_2 _Assigned_chem_shift_list.Sample_condition_list_ID 2 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_2 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 11 '2D 1H-15N TROSY' . . . 51140 4 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 4 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7680 0.0000 . 1 . . . . . 2 ARG H . 51140 4 2 . 1 . 1 2 2 ARG N N 15 121.1950 0.0000 . 1 . . . . . 2 ARG N . 51140 4 3 . 1 . 1 27 27 LYS H H 1 8.3570 0.0000 . 1 . . . . . 27 LYS H . 51140 4 4 . 1 . 1 27 27 LYS N N 15 122.9990 0.0000 . 1 . . . . . 27 LYS N . 51140 4 5 . 1 . 1 32 32 THR H H 1 8.1170 0.0000 . 1 . . . . . 32 THR H . 51140 4 6 . 1 . 1 32 32 THR N N 15 113.1530 0.0000 . 1 . . . . . 32 THR N . 51140 4 7 . 1 . 1 35 35 VAL H H 1 7.9760 0.0000 . 1 . . . . . 35 VAL H . 51140 4 8 . 1 . 1 35 35 VAL N N 15 119.9240 0.0000 . 1 . . . . . 35 VAL N . 51140 4 stop_ save_ save_assigned_chemical_shifts_5 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_5 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 5 _Assigned_chem_shift_list.Name H3-193-pH6-200KCl_1 _Assigned_chem_shift_list.Sample_condition_list_ID 3 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_3 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 12 '2D 1H-15N TROSY' . . . 51140 5 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 5 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7620 0.0000 . 1 . . . . . 2 ARG H . 51140 5 2 . 1 . 1 2 2 ARG N N 15 121.2180 0.0000 . 1 . . . . . 2 ARG N . 51140 5 3 . 1 . 1 3 3 THR H H 1 8.3800 0.0000 . 1 . . . . . 3 THR H . 51140 5 4 . 1 . 1 3 3 THR N N 15 117.3110 0.0000 . 1 . . . . . 3 THR N . 51140 5 5 . 1 . 1 4 4 LYS H H 1 8.5310 0.0000 . 1 . . . . . 4 LYS H . 51140 5 6 . 1 . 1 4 4 LYS N N 15 124.6560 0.0000 . 1 . . . . . 4 LYS N . 51140 5 7 . 1 . 1 5 5 GLN H H 1 8.5890 0.0000 . 1 . . . . . 5 GLN H . 51140 5 8 . 1 . 1 5 5 GLN N N 15 122.7040 0.0000 . 1 . . . . . 5 GLN N . 51140 5 9 . 1 . 1 6 6 THR H H 1 8.1960 0.0000 . 1 . . . . . 6 THR H . 51140 5 10 . 1 . 1 6 6 THR N N 15 116.2870 0.0000 . 1 . . . . . 6 THR N . 51140 5 11 . 1 . 1 7 7 ALA H H 1 8.3710 0.0000 . 1 . . . . . 7 ALA H . 51140 5 12 . 1 . 1 7 7 ALA N N 15 126.9770 0.0000 . 1 . . . . . 7 ALA N . 51140 5 13 . 1 . 1 8 8 ARG H H 1 8.3300 0.0000 . 1 . . . . . 8 ARG H . 51140 5 14 . 1 . 1 8 8 ARG N N 15 121.1530 0.0000 . 1 . . . . . 8 ARG N . 51140 5 15 . 1 . 1 9 9 LYS H H 1 8.4290 0.0000 . 1 . . . . . 9 LYS H . 51140 5 16 . 1 . 1 9 9 LYS N N 15 123.3230 0.0000 . 1 . . . . . 9 LYS N . 51140 5 17 . 1 . 1 10 10 SER H H 1 8.4540 0.0000 . 1 . . . . . 10 SER H . 51140 5 18 . 1 . 1 10 10 SER N N 15 117.7810 0.0000 . 1 . . . . . 10 SER N . 51140 5 19 . 1 . 1 11 11 THR H H 1 8.2730 0.0000 . 1 . . . . . 11 THR H . 51140 5 20 . 1 . 1 11 11 THR N N 15 115.8960 0.0000 . 1 . . . . . 11 THR N . 51140 5 21 . 1 . 1 12 12 GLY H H 1 8.4470 0.0000 . 1 . . . . . 12 GLY H . 51140 5 22 . 1 . 1 12 12 GLY N N 15 111.4070 0.0000 . 1 . . . . . 12 GLY N . 51140 5 23 . 1 . 1 13 13 GLY H H 1 8.3070 0.0000 . 1 . . . . . 13 GLY H . 51140 5 24 . 1 . 1 13 13 GLY N N 15 109.3750 0.0000 . 1 . . . . . 13 GLY N . 51140 5 25 . 1 . 1 14 14 LYS H H 1 8.1910 0.0000 . 1 . . . . . 14 LYS H . 51140 5 26 . 1 . 1 14 14 LYS N N 15 121.3110 0.0000 . 1 . . . . . 14 LYS N . 51140 5 27 . 1 . 1 15 15 ALA H H 1 8.4050 0.0000 . 1 . . . . . 15 ALA H . 51140 5 28 . 1 . 1 15 15 ALA N N 15 127.3080 0.0000 . 1 . . . . . 15 ALA N . 51140 5 29 . 1 . 1 17 17 ARG H H 1 8.4590 0.0000 . 1 . . . . . 17 ARG H . 51140 5 30 . 1 . 1 17 17 ARG N N 15 122.0470 0.0000 . 1 . . . . . 17 ARG N . 51140 5 31 . 1 . 1 18 18 LYS H H 1 8.4440 0.0000 . 1 . . . . . 18 LYS H . 51140 5 32 . 1 . 1 18 18 LYS N N 15 123.4060 0.0000 . 1 . . . . . 18 LYS N . 51140 5 33 . 1 . 1 19 19 GLN H H 1 8.4390 0.0000 . 1 . . . . . 19 GLN H . 51140 5 34 . 1 . 1 19 19 GLN N N 15 122.3460 0.0000 . 1 . . . . . 19 GLN N . 51140 5 35 . 1 . 1 20 20 LEU H H 1 8.3280 0.0000 . 1 . . . . . 20 LEU H . 51140 5 36 . 1 . 1 20 20 LEU N N 15 124.3910 0.0000 . 1 . . . . . 20 LEU N . 51140 5 37 . 1 . 1 21 21 ALA H H 1 8.3830 0.0000 . 1 . . . . . 21 ALA H . 51140 5 38 . 1 . 1 21 21 ALA N N 15 125.2930 0.0000 . 1 . . . . . 21 ALA N . 51140 5 39 . 1 . 1 22 22 THR H H 1 8.0560 0.0000 . 1 . . . . . 22 THR H . 51140 5 40 . 1 . 1 22 22 THR N N 15 114.0120 0.0000 . 1 . . . . . 22 THR N . 51140 5 41 . 1 . 1 23 23 LYS H H 1 8.3200 0.0000 . 1 . . . . . 23 LYS H . 51140 5 42 . 1 . 1 23 23 LYS N N 15 124.0470 0.0000 . 1 . . . . . 23 LYS N . 51140 5 43 . 1 . 1 24 24 ALA H H 1 8.2810 0.0000 . 1 . . . . . 24 ALA H . 51140 5 44 . 1 . 1 24 24 ALA N N 15 125.2830 0.0000 . 1 . . . . . 24 ALA N . 51140 5 45 . 1 . 1 25 25 ALA H H 1 8.2050 0.0000 . 1 . . . . . 25 ALA H . 51140 5 46 . 1 . 1 25 25 ALA N N 15 123.7060 0.0000 . 1 . . . . . 25 ALA N . 51140 5 47 . 1 . 1 26 26 ARG H H 1 8.2360 0.0000 . 1 . . . . . 26 ARG H . 51140 5 48 . 1 . 1 26 26 ARG N N 15 120.7750 0.0000 . 1 . . . . . 26 ARG N . 51140 5 49 . 1 . 1 27 27 LYS H H 1 8.3740 0.0000 . 1 . . . . . 27 LYS H . 51140 5 50 . 1 . 1 27 27 LYS N N 15 123.1790 0.0000 . 1 . . . . . 27 LYS N . 51140 5 51 . 1 . 1 28 28 SER H H 1 8.2680 0.0000 . 1 . . . . . 28 SER H . 51140 5 52 . 1 . 1 28 28 SER N N 15 117.5060 0.0000 . 1 . . . . . 28 SER N . 51140 5 53 . 1 . 1 29 29 ALA H H 1 8.3000 0.0000 . 1 . . . . . 29 ALA H . 51140 5 54 . 1 . 1 29 29 ALA N N 15 127.4400 0.0000 . 1 . . . . . 29 ALA N . 51140 5 55 . 1 . 1 31 31 ALA H H 1 8.5180 0.0000 . 1 . . . . . 31 ALA H . 51140 5 56 . 1 . 1 31 31 ALA N N 15 124.9800 0.0000 . 1 . . . . . 31 ALA N . 51140 5 57 . 1 . 1 32 32 THR H H 1 8.0990 0.0000 . 1 . . . . . 32 THR H . 51140 5 58 . 1 . 1 32 32 THR N N 15 112.9950 0.0000 . 1 . . . . . 32 THR N . 51140 5 59 . 1 . 1 33 33 GLY H H 1 8.4080 0.0000 . 1 . . . . . 33 GLY H . 51140 5 60 . 1 . 1 33 33 GLY N N 15 111.4140 0.0000 . 1 . . . . . 33 GLY N . 51140 5 61 . 1 . 1 34 34 GLY H H 1 8.2810 0.0000 . 1 . . . . . 34 GLY H . 51140 5 62 . 1 . 1 34 34 GLY N N 15 109.4000 0.0000 . 1 . . . . . 34 GLY N . 51140 5 63 . 1 . 1 35 35 VAL H H 1 7.9700 0.0000 . 1 . . . . . 35 VAL H . 51140 5 64 . 1 . 1 35 35 VAL N N 15 119.9160 0.0000 . 1 . . . . . 35 VAL N . 51140 5 65 . 1 . 1 36 36 LYS H H 1 8.3770 0.0000 . 1 . . . . . 36 LYS H . 51140 5 66 . 1 . 1 36 36 LYS N N 15 126.4590 0.0000 . 1 . . . . . 36 LYS N . 51140 5 stop_ save_ save_assigned_chemical_shifts_6 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_6 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 6 _Assigned_chem_shift_list.Name H3-193-pH6-200KCl_2 _Assigned_chem_shift_list.Sample_condition_list_ID 3 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_3 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 12 '2D 1H-15N TROSY' . . . 51140 6 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 6 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 27 27 LYS H H 1 8.3660 0.0000 . 1 . . . . . 27 LYS H . 51140 6 2 . 1 . 1 27 27 LYS N N 15 123.1060 0.0000 . 1 . . . . . 27 LYS N . 51140 6 3 . 1 . 1 32 32 THR H H 1 8.1190 0.0000 . 1 . . . . . 32 THR H . 51140 6 4 . 1 . 1 32 32 THR N N 15 113.1750 0.0000 . 1 . . . . . 32 THR N . 51140 6 5 . 1 . 1 35 35 VAL H H 1 7.9890 0.0000 . 1 . . . . . 35 VAL H . 51140 6 6 . 1 . 1 35 35 VAL N N 15 119.9860 0.0000 . 1 . . . . . 35 VAL N . 51140 6 stop_ save_ save_assigned_chemical_shifts_7 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_7 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 7 _Assigned_chem_shift_list.Name H3-193-pH6-300KCl_1 _Assigned_chem_shift_list.Sample_condition_list_ID 4 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_4 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 13 '2D 1H-15N TROSY' . . . 51140 7 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 7 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 2 2 ARG H H 1 8.7570 0.0000 . 1 . . . . . 2 ARG H . 51140 7 2 . 1 . 1 2 2 ARG N N 15 121.2570 0.0000 . 1 . . . . . 2 ARG N . 51140 7 3 . 1 . 1 3 3 THR H H 1 8.3780 0.0000 . 1 . . . . . 3 THR H . 51140 7 4 . 1 . 1 3 3 THR N N 15 117.3160 0.0000 . 1 . . . . . 3 THR N . 51140 7 5 . 1 . 1 4 4 LYS H H 1 8.5320 0.0000 . 1 . . . . . 4 LYS H . 51140 7 6 . 1 . 1 4 4 LYS N N 15 124.7020 0.0000 . 1 . . . . . 4 LYS N . 51140 7 7 . 1 . 1 5 5 GLN H H 1 8.5820 0.0000 . 1 . . . . . 5 GLN H . 51140 7 8 . 1 . 1 5 5 GLN N N 15 122.7390 0.0000 . 1 . . . . . 5 GLN N . 51140 7 9 . 1 . 1 6 6 THR H H 1 8.2110 0.0000 . 1 . . . . . 6 THR H . 51140 7 10 . 1 . 1 6 6 THR N N 15 116.3940 0.0000 . 1 . . . . . 6 THR N . 51140 7 11 . 1 . 1 7 7 ALA H H 1 8.3750 0.0000 . 1 . . . . . 7 ALA H . 51140 7 12 . 1 . 1 7 7 ALA N N 15 127.0340 0.0000 . 1 . . . . . 7 ALA N . 51140 7 13 . 1 . 1 8 8 ARG H H 1 8.3360 0.0000 . 1 . . . . . 8 ARG H . 51140 7 14 . 1 . 1 8 8 ARG N N 15 121.2070 0.0000 . 1 . . . . . 8 ARG N . 51140 7 15 . 1 . 1 9 9 LYS H H 1 8.4190 0.0000 . 1 . . . . . 9 LYS H . 51140 7 16 . 1 . 1 9 9 LYS N N 15 123.3240 0.0000 . 1 . . . . . 9 LYS N . 51140 7 17 . 1 . 1 10 10 SER H H 1 8.4570 0.0000 . 1 . . . . . 10 SER H . 51140 7 18 . 1 . 1 10 10 SER N N 15 117.8080 0.0000 . 1 . . . . . 10 SER N . 51140 7 19 . 1 . 1 11 11 THR H H 1 8.2760 0.0000 . 1 . . . . . 11 THR H . 51140 7 20 . 1 . 1 11 11 THR N N 15 115.8980 0.0000 . 1 . . . . . 11 THR N . 51140 7 21 . 1 . 1 12 12 GLY H H 1 8.4500 0.0000 . 1 . . . . . 12 GLY H . 51140 7 22 . 1 . 1 12 12 GLY N N 15 111.4520 0.0000 . 1 . . . . . 12 GLY N . 51140 7 23 . 1 . 1 13 13 GLY H H 1 8.3120 0.0000 . 1 . . . . . 13 GLY H . 51140 7 24 . 1 . 1 13 13 GLY N N 15 109.4010 0.0000 . 1 . . . . . 13 GLY N . 51140 7 25 . 1 . 1 14 14 LYS H H 1 8.1950 0.0000 . 1 . . . . . 14 LYS H . 51140 7 26 . 1 . 1 14 14 LYS N N 15 121.3650 0.0000 . 1 . . . . . 14 LYS N . 51140 7 27 . 1 . 1 15 15 ALA H H 1 8.3970 0.0000 . 1 . . . . . 15 ALA H . 51140 7 28 . 1 . 1 15 15 ALA N N 15 127.3040 0.0000 . 1 . . . . . 15 ALA N . 51140 7 29 . 1 . 1 17 17 ARG H H 1 8.4540 0.0000 . 1 . . . . . 17 ARG H . 51140 7 30 . 1 . 1 17 17 ARG N N 15 122.0240 0.0000 . 1 . . . . . 17 ARG N . 51140 7 31 . 1 . 1 18 18 LYS H H 1 8.4440 0.0000 . 1 . . . . . 18 LYS H . 51140 7 32 . 1 . 1 18 18 LYS N N 15 123.4740 0.0000 . 1 . . . . . 18 LYS N . 51140 7 33 . 1 . 1 19 19 GLN H H 1 8.4410 0.0000 . 1 . . . . . 19 GLN H . 51140 7 34 . 1 . 1 19 19 GLN N N 15 122.4020 0.0000 . 1 . . . . . 19 GLN N . 51140 7 35 . 1 . 1 20 20 LEU H H 1 8.3280 0.0000 . 1 . . . . . 20 LEU H . 51140 7 36 . 1 . 1 20 20 LEU N N 15 124.4030 0.0000 . 1 . . . . . 20 LEU N . 51140 7 37 . 1 . 1 21 21 ALA H H 1 8.3830 0.0000 . 1 . . . . . 21 ALA H . 51140 7 38 . 1 . 1 21 21 ALA N N 15 125.3330 0.0000 . 1 . . . . . 21 ALA N . 51140 7 39 . 1 . 1 22 22 THR H H 1 8.0610 0.0000 . 1 . . . . . 22 THR H . 51140 7 40 . 1 . 1 22 22 THR N N 15 114.0400 0.0000 . 1 . . . . . 22 THR N . 51140 7 41 . 1 . 1 23 23 LYS H H 1 8.3220 0.0000 . 1 . . . . . 23 LYS H . 51140 7 42 . 1 . 1 23 23 LYS N N 15 124.0320 0.0000 . 1 . . . . . 23 LYS N . 51140 7 43 . 1 . 1 24 24 ALA H H 1 8.2790 0.0000 . 1 . . . . . 24 ALA H . 51140 7 44 . 1 . 1 24 24 ALA N N 15 125.3040 0.0000 . 1 . . . . . 24 ALA N . 51140 7 45 . 1 . 1 25 25 ALA H H 1 8.2110 0.0000 . 1 . . . . . 25 ALA H . 51140 7 46 . 1 . 1 25 25 ALA N N 15 123.7680 0.0000 . 1 . . . . . 25 ALA N . 51140 7 47 . 1 . 1 26 26 ARG H H 1 8.2430 0.0000 . 1 . . . . . 26 ARG H . 51140 7 48 . 1 . 1 26 26 ARG N N 15 120.8000 0.0000 . 1 . . . . . 26 ARG N . 51140 7 49 . 1 . 1 27 27 LYS H H 1 8.3790 0.0000 . 1 . . . . . 27 LYS H . 51140 7 50 . 1 . 1 27 27 LYS N N 15 123.2110 0.0000 . 1 . . . . . 27 LYS N . 51140 7 51 . 1 . 1 28 28 SER H H 1 8.2810 0.0000 . 1 . . . . . 28 SER H . 51140 7 52 . 1 . 1 28 28 SER N N 15 117.5860 0.0000 . 1 . . . . . 28 SER N . 51140 7 53 . 1 . 1 29 29 ALA H H 1 8.3070 0.0000 . 1 . . . . . 29 ALA H . 51140 7 54 . 1 . 1 29 29 ALA N N 15 127.4260 0.0000 . 1 . . . . . 29 ALA N . 51140 7 55 . 1 . 1 31 31 ALA H H 1 8.5210 0.0000 . 1 . . . . . 31 ALA H . 51140 7 56 . 1 . 1 31 31 ALA N N 15 124.9900 0.0000 . 1 . . . . . 31 ALA N . 51140 7 57 . 1 . 1 32 32 THR H H 1 8.1070 0.0000 . 1 . . . . . 32 THR H . 51140 7 58 . 1 . 1 32 32 THR N N 15 113.0080 0.0000 . 1 . . . . . 32 THR N . 51140 7 59 . 1 . 1 33 33 GLY H H 1 8.4130 0.0000 . 1 . . . . . 33 GLY H . 51140 7 60 . 1 . 1 33 33 GLY N N 15 111.4240 0.0000 . 1 . . . . . 33 GLY N . 51140 7 61 . 1 . 1 34 34 GLY H H 1 8.2850 0.0000 . 1 . . . . . 34 GLY H . 51140 7 62 . 1 . 1 34 34 GLY N N 15 109.4160 0.0000 . 1 . . . . . 34 GLY N . 51140 7 63 . 1 . 1 35 35 VAL H H 1 7.9840 0.0000 . 1 . . . . . 35 VAL H . 51140 7 64 . 1 . 1 35 35 VAL N N 15 119.9890 0.0000 . 1 . . . . . 35 VAL N . 51140 7 65 . 1 . 1 36 36 LYS H H 1 8.3910 0.0000 . 1 . . . . . 36 LYS H . 51140 7 66 . 1 . 1 36 36 LYS N N 15 126.5430 0.0000 . 1 . . . . . 36 LYS N . 51140 7 stop_ save_ save_assigned_chemical_shifts_8 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_8 _Assigned_chem_shift_list.Entry_ID 51140 _Assigned_chem_shift_list.ID 8 _Assigned_chem_shift_list.Name H3-193-pH6-300KCl_2 _Assigned_chem_shift_list.Sample_condition_list_ID 4 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_4 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 13 '2D 1H-15N TROSY' . . . 51140 8 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51140 8 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 32 32 THR H H 1 8.1290 0.0000 . 1 . . . . . 32 THR H . 51140 8 2 . 1 . 1 32 32 THR N N 15 113.1740 0.0000 . 1 . . . . . 32 THR N . 51140 8 3 . 1 . 1 35 35 VAL H H 1 8.0070 0.0000 . 1 . . . . . 35 VAL H . 51140 8 4 . 1 . 1 35 35 VAL N N 15 120.0030 0.0000 . 1 . . . . . 35 VAL N . 51140 8 stop_ save_