data_52232


#######################
#  Entry information  #
#######################
save_entry_information_1
   _Entry.Sf_category                    entry_information
   _Entry.Sf_framecode                   entry_information_1
   _Entry.ID                             52232
   _Entry.Title
;
Znf706 complex with cMyc DNA G4 qudruplex T1 and T2 relaxation
;
   _Entry.Type                           macromolecule
   _Entry.Version_type                   original
   _Entry.Submission_date                2023-12-05
   _Entry.Accession_date                 2023-12-05
   _Entry.Last_release_date              2023-12-06
   _Entry.Original_release_date          2023-12-06
   _Entry.Origination                    author
   _Entry.Format_name                    .
   _Entry.NMR_STAR_version               3.2.14.0
   _Entry.NMR_STAR_dict_location         .
   _Entry.Original_NMR_STAR_version      3.1
   _Entry.Experimental_method            NMR
   _Entry.Experimental_method_subtype    solution
   _Entry.Source_data_format             .
   _Entry.Source_data_format_version     .
   _Entry.Generated_software_name        .
   _Entry.Generated_software_version     .
   _Entry.Generated_software_ID          1
   _Entry.Generated_software_label       $software_1
   _Entry.Generated_date                 .
   _Entry.DOI                            .
   _Entry.UUID                           .
   _Entry.Related_coordinate_file_name   .
   _Entry.Details                        .
   _Entry.BMRB_internal_directory_name   .

   loop_
      _Entry_author.Ordinal
      _Entry_author.Given_name
      _Entry_author.Family_name
      _Entry_author.First_initial
      _Entry_author.Middle_initials
      _Entry_author.Family_title
      _Entry_author.ORCID
      _Entry_author.Entry_ID

      1   Bikash   SAHOO      .   R.     .   0000-0002-3683-1178   52232
      2   James    Bardwell   .   C.A.   .   0000-0003-1683-1944   52232
   stop_

   loop_
      _Data_set.Type
      _Data_set.Count
      _Data_set.Entry_ID

      heteronucl_T1_relaxation   1   52232
      heteronucl_T2_relaxation   1   52232
   stop_

   loop_
      _Datum.Type
      _Datum.Count
      _Datum.Entry_ID

      'T1 relaxation values'   53   52232
      'T2 relaxation values'   53   52232
   stop_

   loop_
      _Release.Release_number
      _Release.Format_type
      _Release.Format_version
      _Release.Date
      _Release.Submission_date
      _Release.Type
      _Release.Author
      _Release.Detail
      _Release.Entry_ID

      1   .   .   2024-08-28   .   original   BMRB   .   52232
   stop_

   loop_
      _Related_entries.Database_name
      _Related_entries.Database_accession_code
      _Related_entries.Relationship
      _Related_entries.Entry_ID

      BMRB   52229   'Human Znf706 15N-1H heteronuclear NOEs'                                 52232
      BMRB   52230   'Human Znf706 complexed with cMyc DNA G4Quadruplex heteronuclear NOEs'   52232
      BMRB   52231   'Znf706 T1 and T2 relaxation'                                            52232
   stop_
save_


###############
#  Citations  #
###############
save_citations_1
   _Citation.Sf_category                  citations
   _Citation.Sf_framecode                 citations_1
   _Citation.Entry_ID                     52232
   _Citation.ID                           1
   _Citation.Name                         .
   _Citation.Class                        'entry citation'
   _Citation.CAS_abstract_code            .
   _Citation.MEDLINE_UI_code              .
   _Citation.PubMed_ID                    38572746
   _Citation.DOI                          .
   _Citation.Full_citation                .
   _Citation.Title
;
Protein G-quadruplex interactions and their effects on phase transitions and protein aggregation
;
   _Citation.Status                       published
   _Citation.Type                         journal
   _Citation.Journal_abbrev               'Nucleic Acids Res.'
   _Citation.Journal_name_full            'Nucleic acids research'
   _Citation.Journal_volume               52
   _Citation.Journal_issue                8
   _Citation.Journal_ASTM                 .
   _Citation.Journal_ISSN                 1362-4962
   _Citation.Journal_CSD                  .
   _Citation.Book_title                   .
   _Citation.Book_chapter_title           .
   _Citation.Book_volume                  .
   _Citation.Book_series                  .
   _Citation.Book_publisher               .
   _Citation.Book_publisher_city          .
   _Citation.Book_ISBN                    .
   _Citation.Conference_title             .
   _Citation.Conference_site              .
   _Citation.Conference_state_province    .
   _Citation.Conference_country           .
   _Citation.Conference_start_date        .
   _Citation.Conference_end_date          .
   _Citation.Conference_abstract_number   .
   _Citation.Thesis_institution           .
   _Citation.Thesis_institution_city      .
   _Citation.Thesis_institution_country   .
   _Citation.WWW_URL                      .
   _Citation.Page_first                   4702
   _Citation.Page_last                    4722
   _Citation.Year                         2024
   _Citation.Details                      .

   loop_
      _Citation_author.Ordinal
      _Citation_author.Given_name
      _Citation_author.Family_name
      _Citation_author.First_initial
      _Citation_author.Middle_initials
      _Citation_author.Family_title
      _Citation_author.ORCID
      _Citation_author.Entry_ID
      _Citation_author.Citation_ID

      1    Bikash     Sahoo       B.   R.   .   .   52232   1
      2    Vojc       Kocman      V.   .    .   .   52232   1
      3    Nathan     Clark       N.   .    .   .   52232   1
      4    Nikhil     Myers       N.   .    .   .   52232   1
      5    Xiexiong   Deng        X.   .    .   .   52232   1
      6    Ee         Wong        E.   L.   .   .   52232   1
      7    Harry      Yang        H.   J.   .   .   52232   1
      8    Anita      Kotar       A.   .    .   .   52232   1
      9    Bryan      Guzman      B.   B.   .   .   52232   1
      10   Daniel     Dominguez   D.   .    .   .   52232   1
      11   Janez      Plavec      J.   .    .   .   52232   1
      12   James      Bardwell    .    .    .   .   52232   1
   stop_
save_


#############################################
#  Molecular system (assembly) description  #
#############################################
save_assembly_1
   _Assembly.Sf_category                       assembly
   _Assembly.Sf_framecode                      assembly_1
   _Assembly.Entry_ID                          52232
   _Assembly.ID                                1
   _Assembly.Name                              'Znf706 complex with cMyc DNA G4 Quadruplex'
   _Assembly.BMRB_code                         .
   _Assembly.Number_of_components              2
   _Assembly.Organic_ligands                   0
   _Assembly.Metal_ions                        0
   _Assembly.Non_standard_bonds                no
   _Assembly.Ambiguous_conformational_states   no
   _Assembly.Ambiguous_chem_comp_sites         .
   _Assembly.Molecules_in_chemical_exchange    no
   _Assembly.Paramagnetic                      no
   _Assembly.Thiol_state                       .
   _Assembly.Molecular_mass                    .
   _Assembly.Enzyme_commission_number          .
   _Assembly.Details                           .
   _Assembly.DB_query_date                     .
   _Assembly.DB_query_revised_last_date        .

   loop_
      _Entity_assembly.ID
      _Entity_assembly.Entity_assembly_name
      _Entity_assembly.Entity_ID
      _Entity_assembly.Entity_label
      _Entity_assembly.Asym_ID
      _Entity_assembly.PDB_chain_ID
      _Entity_assembly.Experimental_data_reported
      _Entity_assembly.Physical_state
      _Entity_assembly.Conformational_isomer
      _Entity_assembly.Chemical_exchange_state
      _Entity_assembly.Magnetic_equivalence_group_code
      _Entity_assembly.Role
      _Entity_assembly.Details
      _Entity_assembly.Entry_ID
      _Entity_assembly.Assembly_ID

      1   Znf706                     1   $entity_1   .   .   yes   native   no   no   .   .   .   52232   1
      2   'cMyc DNA G4 Quadruplex'   2   $entity_2   .   .   no    native   no   no   .   .   .   52232   1
   stop_

   loop_
      _Assembly_bio_function.Biological_function
      _Assembly_bio_function.Entry_ID
      _Assembly_bio_function.Assembly_ID

      'Protein interaction with G4 quadruplex and its activity on gene expression and protein aggregation.'   52232   1
   stop_
save_


    ####################################
    #  Biological polymers and ligands #
    ####################################
save_entity_1
   _Entity.Sf_category                       entity
   _Entity.Sf_framecode                      entity_1
   _Entity.Entry_ID                          52232
   _Entity.ID                                1
   _Entity.BMRB_code                         .
   _Entity.Name                              entity_1
   _Entity.Type                              polymer
   _Entity.Polymer_common_type               .
   _Entity.Polymer_type                      polypeptide(L)
   _Entity.Polymer_type_details              .
   _Entity.Polymer_strand_ID                 .
   _Entity.Polymer_seq_one_letter_code_can   .
   _Entity.Polymer_seq_one_letter_code
;
MARGQQKIQSQQKNAKKQAG
QKKKQGHDQKAAAKAALIYT
CTVCRTQMPDPKTFKQHFES
KHPKTPLPPELADVQA
;
   _Entity.Target_identifier                 .
   _Entity.Polymer_author_defined_seq        .
   _Entity.Polymer_author_seq_details        .
   _Entity.Ambiguous_conformational_states   no
   _Entity.Ambiguous_chem_comp_sites         no
   _Entity.Nstd_monomer                      no
   _Entity.Nstd_chirality                    no
   _Entity.Nstd_linkage                      no
   _Entity.Nonpolymer_comp_ID                .
   _Entity.Nonpolymer_comp_label             .
   _Entity.Number_of_monomers                76
   _Entity.Number_of_nonpolymer_components   .
   _Entity.Paramagnetic                      no
   _Entity.Thiol_state                       'all other bound'
   _Entity.Src_method                        .
   _Entity.Parent_entity_ID                  1
   _Entity.Fragment                          .
   _Entity.Mutation                          .
   _Entity.EC_number                         .
   _Entity.Calc_isoelectric_point            .
   _Entity.Formula_weight                    .
   _Entity.Formula_weight_exptl              .
   _Entity.Formula_weight_exptl_meth         .
   _Entity.Details                           .
   _Entity.DB_query_date                     .
   _Entity.DB_query_revised_last_date        .

   loop_
      _Entity_comp_index.ID
      _Entity_comp_index.Auth_seq_ID
      _Entity_comp_index.Comp_ID
      _Entity_comp_index.Comp_label
      _Entity_comp_index.Entry_ID
      _Entity_comp_index.Entity_ID

      1    .   MET   .   52232   1
      2    .   ALA   .   52232   1
      3    .   ARG   .   52232   1
      4    .   GLY   .   52232   1
      5    .   GLN   .   52232   1
      6    .   GLN   .   52232   1
      7    .   LYS   .   52232   1
      8    .   ILE   .   52232   1
      9    .   GLN   .   52232   1
      10   .   SER   .   52232   1
      11   .   GLN   .   52232   1
      12   .   GLN   .   52232   1
      13   .   LYS   .   52232   1
      14   .   ASN   .   52232   1
      15   .   ALA   .   52232   1
      16   .   LYS   .   52232   1
      17   .   LYS   .   52232   1
      18   .   GLN   .   52232   1
      19   .   ALA   .   52232   1
      20   .   GLY   .   52232   1
      21   .   GLN   .   52232   1
      22   .   LYS   .   52232   1
      23   .   LYS   .   52232   1
      24   .   LYS   .   52232   1
      25   .   GLN   .   52232   1
      26   .   GLY   .   52232   1
      27   .   HIS   .   52232   1
      28   .   ASP   .   52232   1
      29   .   GLN   .   52232   1
      30   .   LYS   .   52232   1
      31   .   ALA   .   52232   1
      32   .   ALA   .   52232   1
      33   .   ALA   .   52232   1
      34   .   LYS   .   52232   1
      35   .   ALA   .   52232   1
      36   .   ALA   .   52232   1
      37   .   LEU   .   52232   1
      38   .   ILE   .   52232   1
      39   .   TYR   .   52232   1
      40   .   THR   .   52232   1
      41   .   CYS   .   52232   1
      42   .   THR   .   52232   1
      43   .   VAL   .   52232   1
      44   .   CYS   .   52232   1
      45   .   ARG   .   52232   1
      46   .   THR   .   52232   1
      47   .   GLN   .   52232   1
      48   .   MET   .   52232   1
      49   .   PRO   .   52232   1
      50   .   ASP   .   52232   1
      51   .   PRO   .   52232   1
      52   .   LYS   .   52232   1
      53   .   THR   .   52232   1
      54   .   PHE   .   52232   1
      55   .   LYS   .   52232   1
      56   .   GLN   .   52232   1
      57   .   HIS   .   52232   1
      58   .   PHE   .   52232   1
      59   .   GLU   .   52232   1
      60   .   SER   .   52232   1
      61   .   LYS   .   52232   1
      62   .   HIS   .   52232   1
      63   .   PRO   .   52232   1
      64   .   LYS   .   52232   1
      65   .   THR   .   52232   1
      66   .   PRO   .   52232   1
      67   .   LEU   .   52232   1
      68   .   PRO   .   52232   1
      69   .   PRO   .   52232   1
      70   .   GLU   .   52232   1
      71   .   LEU   .   52232   1
      72   .   ALA   .   52232   1
      73   .   ASP   .   52232   1
      74   .   VAL   .   52232   1
      75   .   GLN   .   52232   1
      76   .   ALA   .   52232   1
   stop_

   loop_
      _Entity_poly_seq.Hetero
      _Entity_poly_seq.Mon_ID
      _Entity_poly_seq.Num
      _Entity_poly_seq.Comp_index_ID
      _Entity_poly_seq.Entry_ID
      _Entity_poly_seq.Entity_ID

      .   MET   1    1    52232   1
      .   ALA   2    2    52232   1
      .   ARG   3    3    52232   1
      .   GLY   4    4    52232   1
      .   GLN   5    5    52232   1
      .   GLN   6    6    52232   1
      .   LYS   7    7    52232   1
      .   ILE   8    8    52232   1
      .   GLN   9    9    52232   1
      .   SER   10   10   52232   1
      .   GLN   11   11   52232   1
      .   GLN   12   12   52232   1
      .   LYS   13   13   52232   1
      .   ASN   14   14   52232   1
      .   ALA   15   15   52232   1
      .   LYS   16   16   52232   1
      .   LYS   17   17   52232   1
      .   GLN   18   18   52232   1
      .   ALA   19   19   52232   1
      .   GLY   20   20   52232   1
      .   GLN   21   21   52232   1
      .   LYS   22   22   52232   1
      .   LYS   23   23   52232   1
      .   LYS   24   24   52232   1
      .   GLN   25   25   52232   1
      .   GLY   26   26   52232   1
      .   HIS   27   27   52232   1
      .   ASP   28   28   52232   1
      .   GLN   29   29   52232   1
      .   LYS   30   30   52232   1
      .   ALA   31   31   52232   1
      .   ALA   32   32   52232   1
      .   ALA   33   33   52232   1
      .   LYS   34   34   52232   1
      .   ALA   35   35   52232   1
      .   ALA   36   36   52232   1
      .   LEU   37   37   52232   1
      .   ILE   38   38   52232   1
      .   TYR   39   39   52232   1
      .   THR   40   40   52232   1
      .   CYS   41   41   52232   1
      .   THR   42   42   52232   1
      .   VAL   43   43   52232   1
      .   CYS   44   44   52232   1
      .   ARG   45   45   52232   1
      .   THR   46   46   52232   1
      .   GLN   47   47   52232   1
      .   MET   48   48   52232   1
      .   PRO   49   49   52232   1
      .   ASP   50   50   52232   1
      .   PRO   51   51   52232   1
      .   LYS   52   52   52232   1
      .   THR   53   53   52232   1
      .   PHE   54   54   52232   1
      .   LYS   55   55   52232   1
      .   GLN   56   56   52232   1
      .   HIS   57   57   52232   1
      .   PHE   58   58   52232   1
      .   GLU   59   59   52232   1
      .   SER   60   60   52232   1
      .   LYS   61   61   52232   1
      .   HIS   62   62   52232   1
      .   PRO   63   63   52232   1
      .   LYS   64   64   52232   1
      .   THR   65   65   52232   1
      .   PRO   66   66   52232   1
      .   LEU   67   67   52232   1
      .   PRO   68   68   52232   1
      .   PRO   69   69   52232   1
      .   GLU   70   70   52232   1
      .   LEU   71   71   52232   1
      .   ALA   72   72   52232   1
      .   ASP   73   73   52232   1
      .   VAL   74   74   52232   1
      .   GLN   75   75   52232   1
      .   ALA   76   76   52232   1
   stop_
save_

save_entity_2
   _Entity.Sf_category                       entity
   _Entity.Sf_framecode                      entity_2
   _Entity.Entry_ID                          52232
   _Entity.ID                                2
   _Entity.BMRB_code                         .
   _Entity.Name                              entity_2
   _Entity.Type                              polymer
   _Entity.Polymer_common_type               .
   _Entity.Polymer_type                      polydeoxyribonucleotide
   _Entity.Polymer_type_details              .
   _Entity.Polymer_strand_ID                 .
   _Entity.Polymer_seq_one_letter_code_can   .
   _Entity.Polymer_seq_one_letter_code
;
TAGGGAGGGTAGGGAGGGT
;
   _Entity.Target_identifier                 .
   _Entity.Polymer_author_defined_seq        .
   _Entity.Polymer_author_seq_details        .
   _Entity.Ambiguous_conformational_states   no
   _Entity.Ambiguous_chem_comp_sites         no
   _Entity.Nstd_monomer                      no
   _Entity.Nstd_chirality                    no
   _Entity.Nstd_linkage                      no
   _Entity.Nonpolymer_comp_ID                .
   _Entity.Nonpolymer_comp_label             .
   _Entity.Number_of_monomers                19
   _Entity.Number_of_nonpolymer_components   .
   _Entity.Paramagnetic                      no
   _Entity.Thiol_state                       'not present'
   _Entity.Src_method                        .
   _Entity.Parent_entity_ID                  2
   _Entity.Fragment                          .
   _Entity.Mutation                          .
   _Entity.EC_number                         .
   _Entity.Calc_isoelectric_point            .
   _Entity.Formula_weight                    .
   _Entity.Formula_weight_exptl              .
   _Entity.Formula_weight_exptl_meth         .
   _Entity.Details                           "cMyc DNA G-quadruplex (5'-TAG GGA GGG TAG GGA GGG T-3')"
   _Entity.DB_query_date                     .
   _Entity.DB_query_revised_last_date        .

   loop_
      _Entity_comp_index.ID
      _Entity_comp_index.Auth_seq_ID
      _Entity_comp_index.Comp_ID
      _Entity_comp_index.Comp_label
      _Entity_comp_index.Entry_ID
      _Entity_comp_index.Entity_ID

      1    .   DT   .   52232   2
      2    .   DA   .   52232   2
      3    .   DG   .   52232   2
      4    .   DG   .   52232   2
      5    .   DG   .   52232   2
      6    .   DA   .   52232   2
      7    .   DG   .   52232   2
      8    .   DG   .   52232   2
      9    .   DG   .   52232   2
      10   .   DT   .   52232   2
      11   .   DA   .   52232   2
      12   .   DG   .   52232   2
      13   .   DG   .   52232   2
      14   .   DG   .   52232   2
      15   .   DA   .   52232   2
      16   .   DG   .   52232   2
      17   .   DG   .   52232   2
      18   .   DG   .   52232   2
      19   .   DT   .   52232   2
   stop_

   loop_
      _Entity_poly_seq.Hetero
      _Entity_poly_seq.Mon_ID
      _Entity_poly_seq.Num
      _Entity_poly_seq.Comp_index_ID
      _Entity_poly_seq.Entry_ID
      _Entity_poly_seq.Entity_ID

      .   DT   1    1    52232   2
      .   DA   2    2    52232   2
      .   DG   3    3    52232   2
      .   DG   4    4    52232   2
      .   DG   5    5    52232   2
      .   DA   6    6    52232   2
      .   DG   7    7    52232   2
      .   DG   8    8    52232   2
      .   DG   9    9    52232   2
      .   DT   10   10   52232   2
      .   DA   11   11   52232   2
      .   DG   12   12   52232   2
      .   DG   13   13   52232   2
      .   DG   14   14   52232   2
      .   DA   15   15   52232   2
      .   DG   16   16   52232   2
      .   DG   17   17   52232   2
      .   DG   18   18   52232   2
      .   DT   19   19   52232   2
   stop_
save_


    ####################
    #  Natural source  #
    ####################
save_natural_source_1
   _Entity_natural_src_list.Sf_category    natural_source
   _Entity_natural_src_list.Sf_framecode   natural_source_1
   _Entity_natural_src_list.Entry_ID       52232
   _Entity_natural_src_list.ID             1

   loop_
      _Entity_natural_src.ID
      _Entity_natural_src.Entity_ID
      _Entity_natural_src.Entity_label
      _Entity_natural_src.Entity_chimera_segment_ID
      _Entity_natural_src.NCBI_taxonomy_ID
      _Entity_natural_src.Type
      _Entity_natural_src.Common
      _Entity_natural_src.Organism_name_scientific
      _Entity_natural_src.Organism_name_common
      _Entity_natural_src.Organism_acronym
      _Entity_natural_src.ICTVdb_decimal_code
      _Entity_natural_src.Superkingdom
      _Entity_natural_src.Kingdom
      _Entity_natural_src.Genus
      _Entity_natural_src.Species
      _Entity_natural_src.Strain
      _Entity_natural_src.Variant
      _Entity_natural_src.Organ
      _Entity_natural_src.Tissue
      _Entity_natural_src.Tissue_fraction
      _Entity_natural_src.Cell_line
      _Entity_natural_src.Cell_type
      _Entity_natural_src.ATCC_number
      _Entity_natural_src.Organelle
      _Entity_natural_src.Secretion
      _Entity_natural_src.Plasmid
      _Entity_natural_src.Gene_mnemonic
      _Entity_natural_src.Details
      _Entity_natural_src.Entry_ID
      _Entity_natural_src.Entity_natural_src_list_ID

      1   1   $entity_1   .   9606   organism   .   'Homo sapiens'   Human   .   .   Eukaryota   Metazoa   Homo   sapiens   .   .   .   .   .   .   .   .   .   .   .   .   .   52232   1
   stop_
save_


    #########################
    #  Experimental source  #
    #########################
save_experimental_source_1
   _Entity_experimental_src_list.Sf_category    experimental_source
   _Entity_experimental_src_list.Sf_framecode   experimental_source_1
   _Entity_experimental_src_list.Entry_ID       52232
   _Entity_experimental_src_list.ID             1

   loop_
      _Entity_experimental_src.ID
      _Entity_experimental_src.Entity_ID
      _Entity_experimental_src.Entity_label
      _Entity_experimental_src.Entity_chimera_segment_ID
      _Entity_experimental_src.Production_method
      _Entity_experimental_src.Host_org_scientific_name
      _Entity_experimental_src.Host_org_name_common
      _Entity_experimental_src.Host_org_details
      _Entity_experimental_src.Host_org_NCBI_taxonomy_ID
      _Entity_experimental_src.Host_org_genus
      _Entity_experimental_src.Host_org_species
      _Entity_experimental_src.Host_org_strain
      _Entity_experimental_src.Host_org_variant
      _Entity_experimental_src.Host_org_ATCC_number
      _Entity_experimental_src.Vector_type
      _Entity_experimental_src.PDBview_host_org_vector_name
      _Entity_experimental_src.PDBview_plasmid_name
      _Entity_experimental_src.Vector_name
      _Entity_experimental_src.Vector_details
      _Entity_experimental_src.Vendor_name
      _Entity_experimental_src.Details
      _Entity_experimental_src.Entry_ID
      _Entity_experimental_src.Entity_experimental_src_list_ID

      1   1   $entity_1   .   'recombinant technology'   'Escherichia coli'   .   .   .   Escherichia   coli   .   .   .   plasmid   .   .   pET28   .   .   .   52232   1
   stop_
save_


#####################################
#  Sample contents and methodology  #
#####################################
	 
    ########################
    #  Sample description  #
    ########################
save_sample_1
   _Sample.Sf_category                      sample
   _Sample.Sf_framecode                     sample_1
   _Sample.Entry_ID                         52232
   _Sample.ID                               1
   _Sample.Name                             'Znf706 complex with cMyc DNA G4 Quadruplex'
   _Sample.Type                             solution
   _Sample.Sub_type                         .
   _Sample.Details                          .
   _Sample.Aggregate_sample_number          0
   _Sample.Solvent_system                   '92.5% H2O/7.5% D2O'
   _Sample.Preparation_date                 .
   _Sample.Preparation_expiration_date      .
   _Sample.Polycrystallization_protocol     .
   _Sample.Single_crystal_protocol          .
   _Sample.Crystal_grow_apparatus           .
   _Sample.Crystal_grow_atmosphere          .
   _Sample.Crystal_grow_details             .
   _Sample.Crystal_grow_method              .
   _Sample.Crystal_grow_method_cit_ID       .
   _Sample.Crystal_grow_pH                  .
   _Sample.Crystal_grow_pH_range            .
   _Sample.Crystal_grow_pressure            .
   _Sample.Crystal_grow_pressure_esd        .
   _Sample.Crystal_grow_seeding             .
   _Sample.Crystal_grow_seeding_cit_ID      .
   _Sample.Crystal_grow_temp                .
   _Sample.Crystal_grow_temp_details        .
   _Sample.Crystal_grow_temp_esd            .
   _Sample.Crystal_grow_time                .
   _Sample.Oriented_sample_prep_protocol    .
   _Sample.Lyophilization_cryo_protectant   .
   _Sample.Storage_protocol                 .

   loop_
      _Sample_component.ID
      _Sample_component.Mol_common_name
      _Sample_component.Isotopic_labeling
      _Sample_component.Assembly_ID
      _Sample_component.Assembly_label
      _Sample_component.Entity_ID
      _Sample_component.Entity_label
      _Sample_component.Product_ID
      _Sample_component.Type
      _Sample_component.Concentration_val
      _Sample_component.Concentration_val_min
      _Sample_component.Concentration_val_max
      _Sample_component.Concentration_val_units
      _Sample_component.Concentration_val_err
      _Sample_component.Vendor
      _Sample_component.Vendor_product_name
      _Sample_component.Vendor_product_code
      _Sample_component.Entry_ID
      _Sample_component.Sample_ID

      1   'Znf706 complex with cMyc DNA G4 Quadruplex'                 '[U-100% 15N]'        .   .   1   $entity_1   .   .   0.2   .   .   mM   .   .   .   .   52232   1
      2   "cMyc DNA G-quadruplex (5'-TAG GGA GGG TAG GGA GGG T-3' )"   'natural abundance'   .   .   2   $entity_2   .   .   0.1   .   .   mM   .   .   .   .   52232   1
      3   'Sodium phosphate buffer'                                    'natural abundance'   .   .   .   .           .   .   20    .   .   mM   .   .   .   .   52232   1
      4   KCl                                                          'natural abundance'   .   .   .   .           .   .   100   .   .   mM   .   .   .   .   52232   1
   stop_
save_


#######################
#  Sample conditions  #
#######################
save_sample_conditions_1
   _Sample_condition_list.Sf_category    sample_conditions
   _Sample_condition_list.Sf_framecode   sample_conditions_1
   _Sample_condition_list.Entry_ID       52232
   _Sample_condition_list.ID             1
   _Sample_condition_list.Name           'Protein and G4 quadruplex in sodium phosophate buffer'
   _Sample_condition_list.Details        .

   loop_
      _Sample_condition_variable.Type
      _Sample_condition_variable.Val
      _Sample_condition_variable.Val_err
      _Sample_condition_variable.Val_units
      _Sample_condition_variable.Entry_ID
      _Sample_condition_variable.Sample_condition_list_ID

      'ionic strength'   0.1     .   M     52232   1
      pH                 7.4     .   pH    52232   1
      pressure           1       .   atm   52232   1
      temperature        277.1   .   K     52232   1
   stop_
save_


############################
#  Computer software used  #
############################
save_software_1
   _Software.Sf_category    software
   _Software.Sf_framecode   software_1
   _Software.Entry_ID       52232
   _Software.ID             1
   _Software.Type           .
   _Software.Name           NMRFAM-SPARKY
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Task.Task
      _Task.Software_module
      _Task.Entry_ID
      _Task.Software_ID

      'data analysis'   .   52232   1
   stop_
save_


#########################
#  Experimental detail  #
#########################

    ##################################
    #  NMR Spectrometer definitions  #
    ##################################
save_NMR_spectrometer_1
   _NMR_spectrometer.Sf_category      NMR_spectrometer
   _NMR_spectrometer.Sf_framecode     NMR_spectrometer_1
   _NMR_spectrometer.Entry_ID         52232
   _NMR_spectrometer.ID               1
   _NMR_spectrometer.Name             'Bruker 600 MHz w/cryoprobe BioNMR Core University of Michigan'
   _NMR_spectrometer.Details          .
   _NMR_spectrometer.Manufacturer     Bruker
   _NMR_spectrometer.Model            Avance
   _NMR_spectrometer.Serial_number    .
   _NMR_spectrometer.Field_strength   600
save_


    #############################
    #  NMR applied experiments  #
    #############################
save_experiment_list_1
   _Experiment_list.Sf_category    experiment_list
   _Experiment_list.Sf_framecode   experiment_list_1
   _Experiment_list.Entry_ID       52232
   _Experiment_list.ID             1
   _Experiment_list.Details        .

   loop_
      _Experiment.ID
      _Experiment.Name
      _Experiment.Raw_data_flag
      _Experiment.NUS_flag
      _Experiment.Interleaved_flag
      _Experiment.NMR_spec_expt_ID
      _Experiment.NMR_spec_expt_label
      _Experiment.MS_expt_ID
      _Experiment.MS_expt_label
      _Experiment.SAXS_expt_ID
      _Experiment.SAXS_expt_label
      _Experiment.FRET_expt_ID
      _Experiment.FRET_expt_label
      _Experiment.EMR_expt_ID
      _Experiment.EMR_expt_label
      _Experiment.Sample_ID
      _Experiment.Sample_label
      _Experiment.Sample_state
      _Experiment.Sample_volume
      _Experiment.Sample_volume_units
      _Experiment.Sample_condition_list_ID
      _Experiment.Sample_condition_list_label
      _Experiment.Sample_spinning_rate
      _Experiment.Sample_angle
      _Experiment.NMR_tube_type
      _Experiment.NMR_spectrometer_ID
      _Experiment.NMR_spectrometer_label
      _Experiment.NMR_spectrometer_probe_ID
      _Experiment.NMR_spectrometer_probe_label
      _Experiment.NMR_spectral_processing_ID
      _Experiment.NMR_spectral_processing_label
      _Experiment.Mass_spectrometer_ID
      _Experiment.Mass_spectrometer_label
      _Experiment.Xray_instrument_ID
      _Experiment.Xray_instrument_label
      _Experiment.Fluorescence_instrument_ID
      _Experiment.Fluorescence_instrument_label
      _Experiment.EMR_instrument_ID
      _Experiment.EMR_instrument_label
      _Experiment.Chromatographic_system_ID
      _Experiment.Chromatographic_system_label
      _Experiment.Chromatographic_column_ID
      _Experiment.Chromatographic_column_label
      _Experiment.Details
      _Experiment.Entry_ID
      _Experiment.Experiment_list_ID

      1   'T1/R1 relaxation'   no   no   no   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $NMR_spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   52232   1
      2   'T2/R2 relaxation'   no   no   no   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $NMR_spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   52232   1
   stop_
save_


    ########################################
    #  Heteronuclear T1 relaxation values  #
    ########################################
save_heteronucl_T1_relaxation_1
   _Heteronucl_T1_list.Sf_category                   heteronucl_T1_relaxation
   _Heteronucl_T1_list.Sf_framecode                  heteronucl_T1_relaxation_1
   _Heteronucl_T1_list.Entry_ID                      52232
   _Heteronucl_T1_list.ID                            1
   _Heteronucl_T1_list.Name                          '20, 50, 90, 130, 200, 320, 450, 580, 750, 900, 1200, 2005 ms'
   _Heteronucl_T1_list.Sample_condition_list_ID      1
   _Heteronucl_T1_list.Sample_condition_list_label   $sample_conditions_1
   _Heteronucl_T1_list.Spectrometer_frequency_1H     600
   _Heteronucl_T1_list.T1_coherence_type             Iz
   _Heteronucl_T1_list.T1_val_units                  ms
   _Heteronucl_T1_list.Details                       .
   _Heteronucl_T1_list.Text_data_format              .
   _Heteronucl_T1_list.Text_data                     .

   loop_
      _Heteronucl_T1_experiment.Experiment_ID
      _Heteronucl_T1_experiment.Experiment_name
      _Heteronucl_T1_experiment.Sample_ID
      _Heteronucl_T1_experiment.Sample_label
      _Heteronucl_T1_experiment.Sample_state
      _Heteronucl_T1_experiment.Entry_ID
      _Heteronucl_T1_experiment.Heteronucl_T1_list_ID

      1   'T1/R1 relaxation'   .   .   .   52232   1
   stop_

   loop_
      _Heteronucl_T1_software.Software_ID
      _Heteronucl_T1_software.Software_label
      _Heteronucl_T1_software.Method_ID
      _Heteronucl_T1_software.Method_label
      _Heteronucl_T1_software.Entry_ID
      _Heteronucl_T1_software.Heteronucl_T1_list_ID

      1   $software_1   .   .   52232   1
   stop_

   loop_
      _T1.ID
      _T1.Assembly_atom_ID
      _T1.Entity_assembly_ID
      _T1.Entity_ID
      _T1.Comp_index_ID
      _T1.Seq_ID
      _T1.Comp_ID
      _T1.Atom_ID
      _T1.Atom_type
      _T1.Atom_isotope_number
      _T1.Val
      _T1.Val_err
      _T1.Resonance_ID
      _T1.Auth_entity_assembly_ID
      _T1.Auth_seq_ID
      _T1.Auth_comp_ID
      _T1.Auth_atom_ID
      _T1.Entry_ID
      _T1.Heteronucl_T1_list_ID

      1    .   1   1   2    2    ALA   N   N   15   707.3   95.5   .   .   .   .   .   52232   1
      2    .   1   1   5    5    GLN   N   N   15   749.8   27.6   .   .   .   .   .   52232   1
      3    .   1   1   6    6    GLN   N   N   15   655.8   32.4   .   .   .   .   .   52232   1
      4    .   1   1   7    7    LYS   N   N   15   701.7   41.5   .   .   .   .   .   52232   1
      5    .   1   1   10   10   SER   N   N   15   765     57.3   .   .   .   .   .   52232   1
      6    .   1   1   11   11   GLN   N   N   15   692.9   111    .   .   .   .   .   52232   1
      7    .   1   1   12   12   GLN   N   N   15   716.5   65.3   .   .   .   .   .   52232   1
      8    .   1   1   14   14   ASN   N   N   15   757.6   86.8   .   .   .   .   .   52232   1
      9    .   1   1   15   15   ALA   N   N   15   726.4   32.4   .   .   .   .   .   52232   1
      10   .   1   1   16   16   LYS   N   N   15   764.7   42.6   .   .   .   .   .   52232   1
      11   .   1   1   17   17   LYS   N   N   15   703     56.5   .   .   .   .   .   52232   1
      12   .   1   1   18   18   GLN   N   N   15   731.4   46.6   .   .   .   .   .   52232   1
      13   .   1   1   19   19   ALA   N   N   15   736.7   19.6   .   .   .   .   .   52232   1
      14   .   1   1   20   20   GLY   N   N   15   799.8   76     .   .   .   .   .   52232   1
      15   .   1   1   21   21   GLN   N   N   15   764.6   31.7   .   .   .   .   .   52232   1
      16   .   1   1   22   22   LYS   N   N   15   690.3   72.9   .   .   .   .   .   52232   1
      17   .   1   1   23   23   LYS   N   N   15   694.4   30.2   .   .   .   .   .   52232   1
      18   .   1   1   24   24   LYS   N   N   15   680.1   32.2   .   .   .   .   .   52232   1
      19   .   1   1   25   25   GLN   N   N   15   748.6   23     .   .   .   .   .   52232   1
      20   .   1   1   26   26   GLY   N   N   15   746.2   53.6   .   .   .   .   .   52232   1
      21   .   1   1   27   27   HIS   N   N   15   725     45.4   .   .   .   .   .   52232   1
      22   .   1   1   28   28   ASP   N   N   15   733.2   66.5   .   .   .   .   .   52232   1
      23   .   1   1   29   29   GLN   N   N   15   733.2   70.8   .   .   .   .   .   52232   1
      24   .   1   1   31   31   ALA   N   N   15   745.6   38.4   .   .   .   .   .   52232   1
      25   .   1   1   32   32   ALA   N   N   15   728.9   42.2   .   .   .   .   .   52232   1
      26   .   1   1   33   33   ALA   N   N   15   743.1   34.7   .   .   .   .   .   52232   1
      27   .   1   1   34   34   LYS   N   N   15   756     22.4   .   .   .   .   .   52232   1
      28   .   1   1   35   35   ALA   N   N   15   701.5   20     .   .   .   .   .   52232   1
      29   .   1   1   36   36   ALA   N   N   15   798     21.3   .   .   .   .   .   52232   1
      30   .   1   1   37   37   LEU   N   N   15   821     16.8   .   .   .   .   .   52232   1
      31   .   1   1   38   38   ILE   N   N   15   845.1   17.2   .   .   .   .   .   52232   1
      32   .   1   1   39   39   TYR   N   N   15   743.3   18.2   .   .   .   .   .   52232   1
      33   .   1   1   40   40   THR   N   N   15   798.2   24     .   .   .   .   .   52232   1
      34   .   1   1   41   41   CYS   N   N   15   731.5   20.4   .   .   .   .   .   52232   1
      35   .   1   1   44   44   CYS   N   N   15   869.7   31.1   .   .   .   .   .   52232   1
      36   .   1   1   46   46   THR   N   N   15   797.4   62.5   .   .   .   .   .   52232   1
      37   .   1   1   47   47   GLN   N   N   15   825.8   36.4   .   .   .   .   .   52232   1
      38   .   1   1   48   48   MET   N   N   15   839.7   61.2   .   .   .   .   .   52232   1
      39   .   1   1   56   56   GLN   N   N   15   826.7   22.3   .   .   .   .   .   52232   1
      40   .   1   1   57   57   HIS   N   N   15   827.7   77.2   .   .   .   .   .   52232   1
      41   .   1   1   58   58   PHE   N   N   15   769     43.6   .   .   .   .   .   52232   1
      42   .   1   1   59   59   GLU   N   N   15   881.1   52.6   .   .   .   .   .   52232   1
      43   .   1   1   60   60   SER   N   N   15   906.9   46.8   .   .   .   .   .   52232   1
      44   .   1   1   61   61   LYS   N   N   15   824.5   32.9   .   .   .   .   .   52232   1
      45   .   1   1   62   62   HIS   N   N   15   767.6   43.5   .   .   .   .   .   52232   1
      46   .   1   1   67   67   LEU   N   N   15   800.9   8.98   .   .   .   .   .   52232   1
      47   .   1   1   70   70   GLU   N   N   15   702.2   18.4   .   .   .   .   .   52232   1
      48   .   1   1   71   71   LEU   N   N   15   703.2   11.7   .   .   .   .   .   52232   1
      49   .   1   1   72   72   ALA   N   N   15   683.2   17.6   .   .   .   .   .   52232   1
      50   .   1   1   73   73   ASP   N   N   15   696.2   16     .   .   .   .   .   52232   1
      51   .   1   1   74   74   VAL   N   N   15   703.2   16.7   .   .   .   .   .   52232   1
      52   .   1   1   75   75   GLN   N   N   15   706.3   15.3   .   .   .   .   .   52232   1
      53   .   1   1   76   76   ALA   N   N   15   817.5   17.7   .   .   .   .   .   52232   1
   stop_
save_


    ########################################
    #  Heteronuclear T2 relaxation values  #
    ########################################
save_heteronucl_T2_relaxation_1
   _Heteronucl_T2_list.Sf_category                   heteronucl_T2_relaxation
   _Heteronucl_T2_list.Sf_framecode                  heteronucl_T2_relaxation_1
   _Heteronucl_T2_list.Entry_ID                      52232
   _Heteronucl_T2_list.ID                            1
   _Heteronucl_T2_list.Name                          '16.96, 50.88, 84.80, 135.68, 169.60, 220.48, 305.28, 373.12, 457.92, 542.72, 678.40, 1356.80 ms'
   _Heteronucl_T2_list.Sample_condition_list_ID      1
   _Heteronucl_T2_list.Sample_condition_list_label   $sample_conditions_1
   _Heteronucl_T2_list.Temp_calibration_method       'no calibration applied'
   _Heteronucl_T2_list.Temp_control_method           'no temperature control applied'
   _Heteronucl_T2_list.Spectrometer_frequency_1H     600
   _Heteronucl_T2_list.T2_coherence_type             I(+,-)
   _Heteronucl_T2_list.T2_val_units                  ms
   _Heteronucl_T2_list.Rex_units                     .
   _Heteronucl_T2_list.Details                       .
   _Heteronucl_T2_list.Text_data_format              .
   _Heteronucl_T2_list.Text_data                     .

   loop_
      _Heteronucl_T2_experiment.Experiment_ID
      _Heteronucl_T2_experiment.Experiment_name
      _Heteronucl_T2_experiment.Sample_ID
      _Heteronucl_T2_experiment.Sample_label
      _Heteronucl_T2_experiment.Sample_state
      _Heteronucl_T2_experiment.Entry_ID
      _Heteronucl_T2_experiment.Heteronucl_T2_list_ID

      2   'T2/R2 relaxation'   .   .   .   52232   1
   stop_

   loop_
      _Heteronucl_T2_software.Software_ID
      _Heteronucl_T2_software.Software_label
      _Heteronucl_T2_software.Method_ID
      _Heteronucl_T2_software.Method_label
      _Heteronucl_T2_software.Entry_ID
      _Heteronucl_T2_software.Heteronucl_T2_list_ID

      1   $software_1   .   .   52232   1
   stop_

   loop_
      _T2.ID
      _T2.Assembly_atom_ID
      _T2.Entity_assembly_ID
      _T2.Entity_ID
      _T2.Comp_index_ID
      _T2.Seq_ID
      _T2.Comp_ID
      _T2.Atom_ID
      _T2.Atom_type
      _T2.Atom_isotope_number
      _T2.T2_val
      _T2.T2_val_err
      _T2.Rex_val
      _T2.Rex_err
      _T2.Resonance_ID
      _T2.Auth_entity_assembly_ID
      _T2.Auth_seq_ID
      _T2.Auth_comp_ID
      _T2.Auth_atom_ID
      _T2.Entry_ID
      _T2.Heteronucl_T2_list_ID

      1    .   1   1   2    2    ALA   N   N   15   60.35   6.3     .   .   .   .   .   .   .   52232   1
      2    .   1   1   5    5    GLN   N   N   15   219.7   5.91    .   .   .   .   .   .   .   52232   1
      3    .   1   1   6    6    GLN   N   N   15   38.49   2.48    .   .   .   .   .   .   .   52232   1
      4    .   1   1   7    7    LYS   N   N   15   55.95   1.02    .   .   .   .   .   .   .   52232   1
      5    .   1   1   8    8    ILE   N   N   15   47.6    2.79    .   .   .   .   .   .   .   52232   1
      6    .   1   1   10   10   SER   N   N   15   40.98   8.09    .   .   .   .   .   .   .   52232   1
      7    .   1   1   12   12   GLN   N   N   15   72.21   0.887   .   .   .   .   .   .   .   52232   1
      8    .   1   1   14   14   ASN   N   N   15   62.23   3.15    .   .   .   .   .   .   .   52232   1
      9    .   1   1   15   15   ALA   N   N   15   53.5    2.61    .   .   .   .   .   .   .   52232   1
      10   .   1   1   16   16   LYS   N   N   15   47.74   2.98    .   .   .   .   .   .   .   52232   1
      11   .   1   1   17   17   LYS   N   N   15   71.3    4.68    .   .   .   .   .   .   .   52232   1
      12   .   1   1   18   18   GLN   N   N   15   47.05   1.87    .   .   .   .   .   .   .   52232   1
      13   .   1   1   19   19   ALA   N   N   15   66.26   0.332   .   .   .   .   .   .   .   52232   1
      14   .   1   1   20   20   GLY   N   N   15   65      2.7     .   .   .   .   .   .   .   52232   1
      15   .   1   1   21   21   GLN   N   N   15   83.14   3.67    .   .   .   .   .   .   .   52232   1
      16   .   1   1   22   22   LYS   N   N   15   56.89   1.41    .   .   .   .   .   .   .   52232   1
      17   .   1   1   23   23   LYS   N   N   15   78.68   2.3     .   .   .   .   .   .   .   52232   1
      18   .   1   1   24   24   LYS   N   N   15   45.31   7.52    .   .   .   .   .   .   .   52232   1
      19   .   1   1   25   25   GLN   N   N   15   40.89   2.33    .   .   .   .   .   .   .   52232   1
      20   .   1   1   26   26   GLY   N   N   15   83.76   3.08    .   .   .   .   .   .   .   52232   1
      21   .   1   1   27   27   HIS   N   N   15   64.27   1.94    .   .   .   .   .   .   .   52232   1
      22   .   1   1   28   28   ASP   N   N   15   79.18   2.17    .   .   .   .   .   .   .   52232   1
      23   .   1   1   29   29   GLN   N   N   15   79.18   2.68    .   .   .   .   .   .   .   52232   1
      24   .   1   1   31   31   ALA   N   N   15   44.3    3.44    .   .   .   .   .   .   .   52232   1
      25   .   1   1   32   32   ALA   N   N   15   79.89   0.571   .   .   .   .   .   .   .   52232   1
      26   .   1   1   33   33   ALA   N   N   15   78.04   1.42    .   .   .   .   .   .   .   52232   1
      27   .   1   1   34   34   LYS   N   N   15   79.36   1.39    .   .   .   .   .   .   .   52232   1
      28   .   1   1   35   35   ALA   N   N   15   73.55   1.48    .   .   .   .   .   .   .   52232   1
      29   .   1   1   36   36   ALA   N   N   15   74.56   0.895   .   .   .   .   .   .   .   52232   1
      30   .   1   1   37   37   LEU   N   N   15   70.96   2.13    .   .   .   .   .   .   .   52232   1
      31   .   1   1   38   38   ILE   N   N   15   59.61   1.17    .   .   .   .   .   .   .   52232   1
      32   .   1   1   39   39   TYR   N   N   15   50.39   2.1     .   .   .   .   .   .   .   52232   1
      33   .   1   1   40   40   THR   N   N   15   58.23   2.11    .   .   .   .   .   .   .   52232   1
      34   .   1   1   41   41   CYS   N   N   15   55.08   2.12    .   .   .   .   .   .   .   52232   1
      35   .   1   1   44   44   CYS   N   N   15   48.96   0.592   .   .   .   .   .   .   .   52232   1
      36   .   1   1   46   46   THR   N   N   15   38.95   0.735   .   .   .   .   .   .   .   52232   1
      37   .   1   1   47   47   GLN   N   N   15   51.39   2.04    .   .   .   .   .   .   .   52232   1
      38   .   1   1   48   48   MET   N   N   15   48.99   1.82    .   .   .   .   .   .   .   52232   1
      39   .   1   1   56   56   GLN   N   N   15   43.08   1.5     .   .   .   .   .   .   .   52232   1
      40   .   1   1   57   57   HIS   N   N   15   49.52   2.22    .   .   .   .   .   .   .   52232   1
      41   .   1   1   58   58   PHE   N   N   15   43.98   2.71    .   .   .   .   .   .   .   52232   1
      42   .   1   1   59   59   GLU   N   N   15   42.63   1.06    .   .   .   .   .   .   .   52232   1
      43   .   1   1   60   60   SER   N   N   15   45.45   0.715   .   .   .   .   .   .   .   52232   1
      44   .   1   1   61   61   LYS   N   N   15   47.11   2.73    .   .   .   .   .   .   .   52232   1
      45   .   1   1   62   62   HIS   N   N   15   59.09   2.53    .   .   .   .   .   .   .   52232   1
      46   .   1   1   67   67   LEU   N   N   15   66.15   0.457   .   .   .   .   .   .   .   52232   1
      47   .   1   1   70   70   GLU   N   N   15   59.68   1.23    .   .   .   .   .   .   .   52232   1
      48   .   1   1   71   71   LEU   N   N   15   44.64   1.08    .   .   .   .   .   .   .   52232   1
      49   .   1   1   72   72   ALA   N   N   15   75.5    0.747   .   .   .   .   .   .   .   52232   1
      50   .   1   1   73   73   ASP   N   N   15   79.01   0.945   .   .   .   .   .   .   .   52232   1
      51   .   1   1   74   74   VAL   N   N   15   138.5   4.4     .   .   .   .   .   .   .   52232   1
      52   .   1   1   75   75   GLN   N   N   15   120.6   2.6     .   .   .   .   .   .   .   52232   1
      53   .   1   1   76   76   ALA   N   N   15   180.5   2.68    .   .   .   .   .   .   .   52232   1
   stop_
save_