data_6497 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 6497 _Entry.Title ; Magnetic Field Dependence of Nitrogen-Proton J Splittings in 15N-Enriched Human Ubiquitin Resulting from Relaxation Interference and Residual Dipolar Coupling ; _Entry.Type macromolecule _Entry.Version_type new _Entry.Submission_date 2005-02-09 _Entry.Accession_date 2005-02-09 _Entry.Last_release_date 2005-02-09 _Entry.Original_release_date 2005-02-09 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.2.14.0 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Nico Tjandra . . . . 6497 2 Stephan Grzesiek . . . . 6497 3 Ad Bax . . . . 6497 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID coupling_constants 7 6497 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID 'coupling constants' 395 6497 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2021-04-29 . original BMRB . 6497 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 6497 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID . _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Magnetic Field Dependence of Nitrogen-Proton J Splittings in 15N-Enriched Human Ubiquitin Resulting from Relaxation Interference and Residual Dipolar Coupling ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Am. Chem. Soc.' _Citation.Journal_name_full . _Citation.Journal_volume 118 _Citation.Journal_issue 26 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 6264 _Citation.Page_last 6272 _Citation.Year 1996 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Nico Tjandra . . . . 6497 1 2 Stephan Grzesiek . . . . 6497 1 3 Ad Bax . . . . 6497 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 6497 _Assembly.ID 1 _Assembly.Name Ub_id_15 _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites no _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state 'not present' _Assembly.Molecular_mass 8600 _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 Ubiquitin 1 $Ub . . yes native no no . . . 6497 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_Ub _Entity.Sf_category entity _Entity.Sf_framecode Ub _Entity.Entry_ID 6497 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name Ubiquitin _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; MQIFVKTLTGKTITLEVEPS DTIENVKAKIQDKEGIPPDQ QRLIFAGKQLEDGRTLSDYN IQKESTLHLVLRLRGG ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 76 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 8579.94 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_biological_function.Biological_function _Entity_biological_function.Entry_ID _Entity_biological_function.Entity_ID 'protein degradation' 6497 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . MET . 6497 1 2 . GLN . 6497 1 3 . ILE . 6497 1 4 . PHE . 6497 1 5 . VAL . 6497 1 6 . LYS . 6497 1 7 . THR . 6497 1 8 . LEU . 6497 1 9 . THR . 6497 1 10 . GLY . 6497 1 11 . LYS . 6497 1 12 . THR . 6497 1 13 . ILE . 6497 1 14 . THR . 6497 1 15 . LEU . 6497 1 16 . GLU . 6497 1 17 . VAL . 6497 1 18 . GLU . 6497 1 19 . PRO . 6497 1 20 . SER . 6497 1 21 . ASP . 6497 1 22 . THR . 6497 1 23 . ILE . 6497 1 24 . GLU . 6497 1 25 . ASN . 6497 1 26 . VAL . 6497 1 27 . LYS . 6497 1 28 . ALA . 6497 1 29 . LYS . 6497 1 30 . ILE . 6497 1 31 . GLN . 6497 1 32 . ASP . 6497 1 33 . LYS . 6497 1 34 . GLU . 6497 1 35 . GLY . 6497 1 36 . ILE . 6497 1 37 . PRO . 6497 1 38 . PRO . 6497 1 39 . ASP . 6497 1 40 . GLN . 6497 1 41 . GLN . 6497 1 42 . ARG . 6497 1 43 . LEU . 6497 1 44 . ILE . 6497 1 45 . PHE . 6497 1 46 . ALA . 6497 1 47 . GLY . 6497 1 48 . LYS . 6497 1 49 . GLN . 6497 1 50 . LEU . 6497 1 51 . GLU . 6497 1 52 . ASP . 6497 1 53 . GLY . 6497 1 54 . ARG . 6497 1 55 . THR . 6497 1 56 . LEU . 6497 1 57 . SER . 6497 1 58 . ASP . 6497 1 59 . TYR . 6497 1 60 . ASN . 6497 1 61 . ILE . 6497 1 62 . GLN . 6497 1 63 . LYS . 6497 1 64 . GLU . 6497 1 65 . SER . 6497 1 66 . THR . 6497 1 67 . LEU . 6497 1 68 . HIS . 6497 1 69 . LEU . 6497 1 70 . VAL . 6497 1 71 . LEU . 6497 1 72 . ARG . 6497 1 73 . LEU . 6497 1 74 . ARG . 6497 1 75 . GLY . 6497 1 76 . GLY . 6497 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . MET 1 1 6497 1 . GLN 2 2 6497 1 . ILE 3 3 6497 1 . PHE 4 4 6497 1 . VAL 5 5 6497 1 . LYS 6 6 6497 1 . THR 7 7 6497 1 . LEU 8 8 6497 1 . THR 9 9 6497 1 . GLY 10 10 6497 1 . LYS 11 11 6497 1 . THR 12 12 6497 1 . ILE 13 13 6497 1 . THR 14 14 6497 1 . LEU 15 15 6497 1 . GLU 16 16 6497 1 . VAL 17 17 6497 1 . GLU 18 18 6497 1 . PRO 19 19 6497 1 . SER 20 20 6497 1 . ASP 21 21 6497 1 . THR 22 22 6497 1 . ILE 23 23 6497 1 . GLU 24 24 6497 1 . ASN 25 25 6497 1 . VAL 26 26 6497 1 . LYS 27 27 6497 1 . ALA 28 28 6497 1 . LYS 29 29 6497 1 . ILE 30 30 6497 1 . GLN 31 31 6497 1 . ASP 32 32 6497 1 . LYS 33 33 6497 1 . GLU 34 34 6497 1 . GLY 35 35 6497 1 . ILE 36 36 6497 1 . PRO 37 37 6497 1 . PRO 38 38 6497 1 . ASP 39 39 6497 1 . GLN 40 40 6497 1 . GLN 41 41 6497 1 . ARG 42 42 6497 1 . LEU 43 43 6497 1 . ILE 44 44 6497 1 . PHE 45 45 6497 1 . ALA 46 46 6497 1 . GLY 47 47 6497 1 . LYS 48 48 6497 1 . GLN 49 49 6497 1 . LEU 50 50 6497 1 . GLU 51 51 6497 1 . ASP 52 52 6497 1 . GLY 53 53 6497 1 . ARG 54 54 6497 1 . THR 55 55 6497 1 . LEU 56 56 6497 1 . SER 57 57 6497 1 . ASP 58 58 6497 1 . TYR 59 59 6497 1 . ASN 60 60 6497 1 . ILE 61 61 6497 1 . GLN 62 62 6497 1 . LYS 63 63 6497 1 . GLU 64 64 6497 1 . SER 65 65 6497 1 . THR 66 66 6497 1 . LEU 67 67 6497 1 . HIS 68 68 6497 1 . LEU 69 69 6497 1 . VAL 70 70 6497 1 . LEU 71 71 6497 1 . ARG 72 72 6497 1 . LEU 73 73 6497 1 . ARG 74 74 6497 1 . GLY 75 75 6497 1 . GLY 76 76 6497 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 6497 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $Ub . 9606 . yes 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 6497 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 6497 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $Ub . 'obtained from a vendor' . . . . . . . . . . . . . . 'VLI Research, Southeastern PA' . 6497 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 6497 _Sample.ID 1 _Sample.Name . _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 Ubiquitin [U-15N] 1 $assembly 1 $Ub . protein 1.4 . . mM . . . . 6497 1 2 NaCl . . . . . . salt 10 . . mM . . . . 6497 1 stop_ save_ ####################### # Sample conditions # ####################### save_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode conditions_1 _Sample_condition_list.Entry_ID 6497 _Sample_condition_list.ID 1 _Sample_condition_list.Name . _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 4.7 0 pH 6497 1 temperature 300 0 K 6497 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_Bruker_AMX-360 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode Bruker_AMX-360 _NMR_spectrometer.Entry_ID 6497 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name . _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model AMX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 360 save_ save_Bruker_DMX-500 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode Bruker_DMX-500 _NMR_spectrometer.Entry_ID 6497 _NMR_spectrometer.ID 2 _NMR_spectrometer.Name . _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DMX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 500 save_ save_Bruker_AMX-600 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode Bruker_AMX-600 _NMR_spectrometer.Entry_ID 6497 _NMR_spectrometer.ID 3 _NMR_spectrometer.Name . _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model AMX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_Bruker_DMX-750 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode Bruker_DMX-750 _NMR_spectrometer.Entry_ID 6497 _NMR_spectrometer.ID 4 _NMR_spectrometer.Name . _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DMX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 750 save_ ############################# # NMR applied experiments # ############################# save_NMR_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode NMR_experiment_list _Experiment_list.Entry_ID 6497 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H15N HSQC' no . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6497 1 2 '1JNH-modulated 2D HSQC' no . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6497 1 stop_ save_ ######################## # Coupling constants # ######################## save_J_coupling_list_F1_360 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_F1_360 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 1 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 360 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 1 '2D 1H15N HSQC' 1 $sample_1 isotropic 6497 1 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.520 . . . . . . . . . . . . . . . . 6497 1 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.254 . . . . . . . . . . . . . . . . 6497 1 3 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.569 . . . . . . . . . . . . . . . . 6497 1 4 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.981 . . . . . . . . . . . . . . . . 6497 1 5 1JNH . 1 1 7 7 THR N N 15 . . 1 1 7 7 THR H H 1 . 94.606 . . . . . . . . . . . . . . . . 6497 1 6 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.411 . . . . . . . . . . . . . . . . 6497 1 7 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.768 . . . . . . . . . . . . . . . . 6497 1 8 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.994 . . . . . . . . . . . . . . . . 6497 1 9 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.626 . . . . . . . . . . . . . . . . 6497 1 10 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.607 . . . . . . . . . . . . . . . . 6497 1 11 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.968 . . . . . . . . . . . . . . . . 6497 1 12 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.496 . . . . . . . . . . . . . . . . 6497 1 13 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 95.210 . . . . . . . . . . . . . . . . 6497 1 14 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.728 . . . . . . . . . . . . . . . . 6497 1 15 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 94.308 . . . . . . . . . . . . . . . . 6497 1 16 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.487 . . . . . . . . . . . . . . . . 6497 1 17 1JNH . 1 1 34 34 GLU N N 15 . . 1 1 34 34 GLU H H 1 . 90.965 . . . . . . . . . . . . . . . . 6497 1 18 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.925 . . . . . . . . . . . . . . . . 6497 1 19 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.383 . . . . . . . . . . . . . . . . 6497 1 20 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.230 . . . . . . . . . . . . . . . . 6497 1 21 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 93.034 . . . . . . . . . . . . . . . . 6497 1 22 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.678 . . . . . . . . . . . . . . . . 6497 1 23 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.742 . . . . . . . . . . . . . . . . 6497 1 24 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 94.011 . . . . . . . . . . . . . . . . 6497 1 25 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.555 . . . . . . . . . . . . . . . . 6497 1 26 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.431 . . . . . . . . . . . . . . . . 6497 1 27 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.573 . . . . . . . . . . . . . . . . 6497 1 28 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 94.114 . . . . . . . . . . . . . . . . 6497 1 29 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.988 . . . . . . . . . . . . . . . . 6497 1 30 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 95.542 . . . . . . . . . . . . . . . . 6497 1 31 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.386 . . . . . . . . . . . . . . . . 6497 1 32 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.398 . . . . . . . . . . . . . . . . 6497 1 33 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.450 . . . . . . . . . . . . . . . . 6497 1 34 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.475 . . . . . . . . . . . . . . . . 6497 1 35 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.864 . . . . . . . . . . . . . . . . 6497 1 36 1JNH . 1 1 66 66 THR N N 15 . . 1 1 66 66 THR H H 1 . 92.272 . . . . . . . . . . . . . . . . 6497 1 37 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 94.127 . . . . . . . . . . . . . . . . 6497 1 38 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.890 . . . . . . . . . . . . . . . . 6497 1 39 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.502 . . . . . . . . . . . . . . . . 6497 1 stop_ save_ save_J_coupling_list_F1_500 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_F1_500 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 2 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 500 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 1 '2D 1H15N HSQC' 1 $sample_1 isotropic 6497 2 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.493 . . . . . . . . . . . . . . . . 6497 2 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.209 . . . . . . . . . . . . . . . . 6497 2 3 1JNH . 1 1 4 4 PHE N N 15 . . 1 1 4 4 PHE H H 1 . 94.082 . . . . . . . . . . . . . . . . 6497 2 4 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.238 . . . . . . . . . . . . . . . . 6497 2 5 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.780 . . . . . . . . . . . . . . . . 6497 2 6 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.247 . . . . . . . . . . . . . . . . 6497 2 7 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.929 . . . . . . . . . . . . . . . . 6497 2 8 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.915 . . . . . . . . . . . . . . . . 6497 2 9 1JNH . 1 1 12 12 THR N N 15 . . 1 1 12 12 THR H H 1 . 92.657 . . . . . . . . . . . . . . . . 6497 2 10 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 93.146 . . . . . . . . . . . . . . . . 6497 2 11 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.351 . . . . . . . . . . . . . . . . 6497 2 12 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.426 . . . . . . . . . . . . . . . . 6497 2 13 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.848 . . . . . . . . . . . . . . . . 6497 2 14 1JNH . 1 1 18 18 GLU N N 15 . . 1 1 18 18 GLU H H 1 . 92.833 . . . . . . . . . . . . . . . . 6497 2 15 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.424 . . . . . . . . . . . . . . . . 6497 2 16 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.663 . . . . . . . . . . . . . . . . 6497 2 17 1JNH . 1 1 23 23 ILE N N 15 . . 1 1 23 23 ILE H H 1 . 94.280 . . . . . . . . . . . . . . . . 6497 2 18 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 95.021 . . . . . . . . . . . . . . . . 6497 2 19 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.341 . . . . . . . . . . . . . . . . 6497 2 20 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.663 . . . . . . . . . . . . . . . . 6497 2 21 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 94.102 . . . . . . . . . . . . . . . . 6497 2 22 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.622 . . . . . . . . . . . . . . . . 6497 2 23 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.388 . . . . . . . . . . . . . . . . 6497 2 24 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 94.248 . . . . . . . . . . . . . . . . 6497 2 25 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.365 . . . . . . . . . . . . . . . . 6497 2 26 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.150 . . . . . . . . . . . . . . . . 6497 2 27 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.990 . . . . . . . . . . . . . . . . 6497 2 28 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 94.145 . . . . . . . . . . . . . . . . 6497 2 29 1JNH . 1 1 42 42 ARG N N 15 . . 1 1 42 42 ARG H H 1 . 93.700 . . . . . . . . . . . . . . . . 6497 2 30 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.727 . . . . . . . . . . . . . . . . 6497 2 31 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.507 . . . . . . . . . . . . . . . . 6497 2 32 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 94.070 . . . . . . . . . . . . . . . . 6497 2 33 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.492 . . . . . . . . . . . . . . . . 6497 2 34 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.217 . . . . . . . . . . . . . . . . 6497 2 35 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.654 . . . . . . . . . . . . . . . . 6497 2 36 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.386 . . . . . . . . . . . . . . . . 6497 2 37 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.140 . . . . . . . . . . . . . . . . 6497 2 38 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.791 . . . . . . . . . . . . . . . . 6497 2 39 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.790 . . . . . . . . . . . . . . . . 6497 2 40 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.222 . . . . . . . . . . . . . . . . 6497 2 41 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.419 . . . . . . . . . . . . . . . . 6497 2 42 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.487 . . . . . . . . . . . . . . . . 6497 2 43 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.510 . . . . . . . . . . . . . . . . 6497 2 44 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.893 . . . . . . . . . . . . . . . . 6497 2 45 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.712 . . . . . . . . . . . . . . . . 6497 2 46 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.775 . . . . . . . . . . . . . . . . 6497 2 47 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.884 . . . . . . . . . . . . . . . . 6497 2 48 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.695 . . . . . . . . . . . . . . . . 6497 2 stop_ save_ save_J_coupling_list_F1_600 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_F1_600 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 3 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 600 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 1 '2D 1H15N HSQC' 1 $sample_1 isotropic 6497 3 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.435 . . . . . . . . . . . . . . . . 6497 3 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.120 . . . . . . . . . . . . . . . . 6497 3 3 1JNH . 1 1 4 4 PHE N N 15 . . 1 1 4 4 PHE H H 1 . 93.962 . . . . . . . . . . . . . . . . 6497 3 4 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.088 . . . . . . . . . . . . . . . . 6497 3 5 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.730 . . . . . . . . . . . . . . . . 6497 3 6 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.195 . . . . . . . . . . . . . . . . 6497 3 7 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.902 . . . . . . . . . . . . . . . . 6497 3 8 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.757 . . . . . . . . . . . . . . . . 6497 3 9 1JNH . 1 1 13 13 ILE N N 15 . . 1 1 13 13 ILE H H 1 . 93.322 . . . . . . . . . . . . . . . . 6497 3 10 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 93.024 . . . . . . . . . . . . . . . . 6497 3 11 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.426 . . . . . . . . . . . . . . . . 6497 3 12 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.562 . . . . . . . . . . . . . . . . 6497 3 13 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.785 . . . . . . . . . . . . . . . . 6497 3 14 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.540 . . . . . . . . . . . . . . . . 6497 3 15 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.746 . . . . . . . . . . . . . . . . 6497 3 16 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 94.937 . . . . . . . . . . . . . . . . 6497 3 17 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.602 . . . . . . . . . . . . . . . . 6497 3 18 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.473 . . . . . . . . . . . . . . . . 6497 3 19 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 93.968 . . . . . . . . . . . . . . . . 6497 3 20 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.407 . . . . . . . . . . . . . . . . 6497 3 21 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.421 . . . . . . . . . . . . . . . . 6497 3 22 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.923 . . . . . . . . . . . . . . . . 6497 3 23 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.474 . . . . . . . . . . . . . . . . 6497 3 24 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.137 . . . . . . . . . . . . . . . . 6497 3 25 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.859 . . . . . . . . . . . . . . . . 6497 3 26 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 93.726 . . . . . . . . . . . . . . . . 6497 3 27 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.525 . . . . . . . . . . . . . . . . 6497 3 28 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.497 . . . . . . . . . . . . . . . . 6497 3 29 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 93.901 . . . . . . . . . . . . . . . . 6497 3 30 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.410 . . . . . . . . . . . . . . . . 6497 3 31 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.359 . . . . . . . . . . . . . . . . 6497 3 32 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.552 . . . . . . . . . . . . . . . . 6497 3 33 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.362 . . . . . . . . . . . . . . . . 6497 3 34 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.621 . . . . . . . . . . . . . . . . 6497 3 35 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.266 . . . . . . . . . . . . . . . . 6497 3 36 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.444 . . . . . . . . . . . . . . . . 6497 3 37 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.735 . . . . . . . . . . . . . . . . 6497 3 38 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 95.161 . . . . . . . . . . . . . . . . 6497 3 39 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.161 . . . . . . . . . . . . . . . . 6497 3 40 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.140 . . . . . . . . . . . . . . . . 6497 3 41 1JNH . 1 1 59 59 TYR N N 15 . . 1 1 59 59 TYR H H 1 . 93.107 . . . . . . . . . . . . . . . . 6497 3 42 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.395 . . . . . . . . . . . . . . . . 6497 3 43 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.486 . . . . . . . . . . . . . . . . 6497 3 44 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.656 . . . . . . . . . . . . . . . . 6497 3 45 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.904 . . . . . . . . . . . . . . . . 6497 3 46 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.614 . . . . . . . . . . . . . . . . 6497 3 47 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.551 . . . . . . . . . . . . . . . . 6497 3 48 1JNH . 1 1 67 67 LEU N N 15 . . 1 1 67 67 LEU H H 1 . 93.975 . . . . . . . . . . . . . . . . 6497 3 49 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.603 . . . . . . . . . . . . . . . . 6497 3 50 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.945 . . . . . . . . . . . . . . . . 6497 3 51 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.618 . . . . . . . . . . . . . . . . 6497 3 stop_ save_ save_J_coupling_list_F1_750 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_F1_750 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 4 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 750 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 1 '2D 1H15N HSQC' 1 $sample_1 isotropic 6497 4 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.367 . . . . . . . . . . . . . . . . 6497 4 2 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.160 . . . . . . . . . . . . . . . . 6497 4 3 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.776 . . . . . . . . . . . . . . . . 6497 4 4 1JNH . 1 1 7 7 THR N N 15 . . 1 1 7 7 THR H H 1 . 94.333 . . . . . . . . . . . . . . . . 6497 4 5 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.106 . . . . . . . . . . . . . . . . 6497 4 6 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.886 . . . . . . . . . . . . . . . . 6497 4 7 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.898 . . . . . . . . . . . . . . . . 6497 4 8 1JNH . 1 1 12 12 THR N N 15 . . 1 1 12 12 THR H H 1 . 92.639 . . . . . . . . . . . . . . . . 6497 4 9 1JNH . 1 1 13 13 ILE N N 15 . . 1 1 13 13 ILE H H 1 . 93.150 . . . . . . . . . . . . . . . . 6497 4 10 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 93.174 . . . . . . . . . . . . . . . . 6497 4 11 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.022 . . . . . . . . . . . . . . . . 6497 4 12 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.137 . . . . . . . . . . . . . . . . 6497 4 13 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.645 . . . . . . . . . . . . . . . . 6497 4 14 1JNH . 1 1 18 18 GLU N N 15 . . 1 1 18 18 GLU H H 1 . 92.799 . . . . . . . . . . . . . . . . 6497 4 15 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.525 . . . . . . . . . . . . . . . . 6497 4 16 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.941 . . . . . . . . . . . . . . . . 6497 4 17 1JNH . 1 1 23 23 ILE N N 15 . . 1 1 23 23 ILE H H 1 . 93.885 . . . . . . . . . . . . . . . . 6497 4 18 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 94.771 . . . . . . . . . . . . . . . . 6497 4 19 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.263 . . . . . . . . . . . . . . . . 6497 4 20 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.292 . . . . . . . . . . . . . . . . 6497 4 21 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 93.929 . . . . . . . . . . . . . . . . 6497 4 22 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.547 . . . . . . . . . . . . . . . . 6497 4 23 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.282 . . . . . . . . . . . . . . . . 6497 4 24 1JNH . 1 1 34 34 GLU N N 15 . . 1 1 34 34 GLU H H 1 . 91.101 . . . . . . . . . . . . . . . . 6497 4 25 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.972 . . . . . . . . . . . . . . . . 6497 4 26 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.335 . . . . . . . . . . . . . . . . 6497 4 27 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 93.975 . . . . . . . . . . . . . . . . 6497 4 28 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.870 . . . . . . . . . . . . . . . . 6497 4 29 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 93.987 . . . . . . . . . . . . . . . . 6497 4 30 1JNH . 1 1 42 42 ARG N N 15 . . 1 1 42 42 ARG H H 1 . 93.773 . . . . . . . . . . . . . . . . 6497 4 31 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.540 . . . . . . . . . . . . . . . . 6497 4 32 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.238 . . . . . . . . . . . . . . . . 6497 4 33 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.421 . . . . . . . . . . . . . . . . 6497 4 34 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.242 . . . . . . . . . . . . . . . . 6497 4 35 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.562 . . . . . . . . . . . . . . . . 6497 4 36 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.189 . . . . . . . . . . . . . . . . 6497 4 37 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.377 . . . . . . . . . . . . . . . . 6497 4 38 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.631 . . . . . . . . . . . . . . . . 6497 4 39 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 94.891 . . . . . . . . . . . . . . . . 6497 4 40 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.348 . . . . . . . . . . . . . . . . 6497 4 41 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.344 . . . . . . . . . . . . . . . . 6497 4 42 1JNH . 1 1 59 59 TYR N N 15 . . 1 1 59 59 TYR H H 1 . 93.200 . . . . . . . . . . . . . . . . 6497 4 43 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.581 . . . . . . . . . . . . . . . . 6497 4 44 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.201 . . . . . . . . . . . . . . . . 6497 4 45 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.481 . . . . . . . . . . . . . . . . 6497 4 46 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.929 . . . . . . . . . . . . . . . . 6497 4 47 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.576 . . . . . . . . . . . . . . . . 6497 4 48 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.779 . . . . . . . . . . . . . . . . 6497 4 49 1JNH . 1 1 66 66 THR N N 15 . . 1 1 66 66 THR H H 1 . 91.890 . . . . . . . . . . . . . . . . 6497 4 50 1JNH . 1 1 67 67 LEU N N 15 . . 1 1 67 67 LEU H H 1 . 93.939 . . . . . . . . . . . . . . . . 6497 4 51 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.564 . . . . . . . . . . . . . . . . 6497 4 52 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.607 . . . . . . . . . . . . . . . . 6497 4 53 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.776 . . . . . . . . . . . . . . . . 6497 4 stop_ save_ save_J_coupling_list_J_mod_360 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_J_mod_360 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 5 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 360 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 2 '1JNH-modulated 2D HSQC' 1 $sample_1 isotropic 6497 5 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.570 . . . . . . . . . . . . . . . . 6497 5 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.252 . . . . . . . . . . . . . . . . 6497 5 3 1JNH . 1 1 4 4 PHE N N 15 . . 1 1 4 4 PHE H H 1 . 94.063 . . . . . . . . . . . . . . . . 6497 5 4 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.219 . . . . . . . . . . . . . . . . 6497 5 5 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.925 . . . . . . . . . . . . . . . . 6497 5 6 1JNH . 1 1 7 7 THR N N 15 . . 1 1 7 7 THR H H 1 . 94.651 . . . . . . . . . . . . . . . . 6497 5 7 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.257 . . . . . . . . . . . . . . . . 6497 5 8 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.938 . . . . . . . . . . . . . . . . 6497 5 9 1JNH . 1 1 10 10 GLY N N 15 . . 1 1 10 10 GLY H H 1 . 93.746 . . . . . . . . . . . . . . . . 6497 5 10 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.961 . . . . . . . . . . . . . . . . 6497 5 11 1JNH . 1 1 12 12 THR N N 15 . . 1 1 12 12 THR H H 1 . 92.923 . . . . . . . . . . . . . . . . 6497 5 12 1JNH . 1 1 13 13 ILE N N 15 . . 1 1 13 13 ILE H H 1 . 93.632 . . . . . . . . . . . . . . . . 6497 5 13 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 93.170 . . . . . . . . . . . . . . . . 6497 5 14 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.500 . . . . . . . . . . . . . . . . 6497 5 15 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.551 . . . . . . . . . . . . . . . . 6497 5 16 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.893 . . . . . . . . . . . . . . . . 6497 5 17 1JNH . 1 1 18 18 GLU N N 15 . . 1 1 18 18 GLU H H 1 . 92.888 . . . . . . . . . . . . . . . . 6497 5 18 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.550 . . . . . . . . . . . . . . . . 6497 5 19 1JNH . 1 1 21 21 ASP N N 15 . . 1 1 21 21 ASP H H 1 . 95.208 . . . . . . . . . . . . . . . . 6497 5 20 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.900 . . . . . . . . . . . . . . . . 6497 5 21 1JNH . 1 1 23 23 ILE N N 15 . . 1 1 23 23 ILE H H 1 . 94.387 . . . . . . . . . . . . . . . . 6497 5 22 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 95.086 . . . . . . . . . . . . . . . . 6497 5 23 1JNH . 1 1 26 26 VAL N N 15 . . 1 1 26 26 VAL H H 1 . 94.068 . . . . . . . . . . . . . . . . 6497 5 24 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.459 . . . . . . . . . . . . . . . . 6497 5 25 1JNH . 1 1 28 28 ALA N N 15 . . 1 1 28 28 ALA H H 1 . 95.182 . . . . . . . . . . . . . . . . 6497 5 26 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.745 . . . . . . . . . . . . . . . . 6497 5 27 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 94.158 . . . . . . . . . . . . . . . . 6497 5 28 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.736 . . . . . . . . . . . . . . . . 6497 5 29 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.576 . . . . . . . . . . . . . . . . 6497 5 30 1JNH . 1 1 34 34 GLU N N 15 . . 1 1 34 34 GLU H H 1 . 91.222 . . . . . . . . . . . . . . . . 6497 5 31 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.996 . . . . . . . . . . . . . . . . 6497 5 32 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.496 . . . . . . . . . . . . . . . . 6497 5 33 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.259 . . . . . . . . . . . . . . . . 6497 5 34 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.924 . . . . . . . . . . . . . . . . 6497 5 35 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 94.183 . . . . . . . . . . . . . . . . 6497 5 36 1JNH . 1 1 42 42 ARG N N 15 . . 1 1 42 42 ARG H H 1 . 93.984 . . . . . . . . . . . . . . . . 6497 5 37 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.918 . . . . . . . . . . . . . . . . 6497 5 38 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.629 . . . . . . . . . . . . . . . . 6497 5 39 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 94.044 . . . . . . . . . . . . . . . . 6497 5 40 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.540 . . . . . . . . . . . . . . . . 6497 5 41 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.364 . . . . . . . . . . . . . . . . 6497 5 42 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.640 . . . . . . . . . . . . . . . . 6497 5 43 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.428 . . . . . . . . . . . . . . . . 6497 5 44 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.836 . . . . . . . . . . . . . . . . 6497 5 45 1JNH . 1 1 51 51 GLU N N 15 . . 1 1 51 51 GLU H H 1 . 93.522 . . . . . . . . . . . . . . . . 6497 5 46 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.392 . . . . . . . . . . . . . . . . 6497 5 47 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.827 . . . . . . . . . . . . . . . . 6497 5 48 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.978 . . . . . . . . . . . . . . . . 6497 5 49 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 95.173 . . . . . . . . . . . . . . . . 6497 5 50 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.289 . . . . . . . . . . . . . . . . 6497 5 51 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.552 . . . . . . . . . . . . . . . . 6497 5 52 1JNH . 1 1 59 59 TYR N N 15 . . 1 1 59 59 TYR H H 1 . 93.410 . . . . . . . . . . . . . . . . 6497 5 53 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.318 . . . . . . . . . . . . . . . . 6497 5 54 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.444 . . . . . . . . . . . . . . . . 6497 5 55 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.531 . . . . . . . . . . . . . . . . 6497 5 56 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.960 . . . . . . . . . . . . . . . . 6497 5 57 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.611 . . . . . . . . . . . . . . . . 6497 5 58 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.696 . . . . . . . . . . . . . . . . 6497 5 59 1JNH . 1 1 66 66 THR N N 15 . . 1 1 66 66 THR H H 1 . 92.200 . . . . . . . . . . . . . . . . 6497 5 60 1JNH . 1 1 67 67 LEU N N 15 . . 1 1 67 67 LEU H H 1 . 93.876 . . . . . . . . . . . . . . . . 6497 5 61 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.873 . . . . . . . . . . . . . . . . 6497 5 62 1JNH . 1 1 69 69 LEU N N 15 . . 1 1 69 69 LEU H H 1 . 93.533 . . . . . . . . . . . . . . . . 6497 5 63 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.919 . . . . . . . . . . . . . . . . 6497 5 64 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.733 . . . . . . . . . . . . . . . . 6497 5 65 1JNH . 1 1 73 73 LEU N N 15 . . 1 1 73 73 LEU H H 1 . 93.522 . . . . . . . . . . . . . . . . 6497 5 66 1JNH . 1 1 74 74 ARG N N 15 . . 1 1 74 74 ARG H H 1 . 93.354 . . . . . . . . . . . . . . . . 6497 5 67 1JNH . 1 1 75 75 GLY N N 15 . . 1 1 75 75 GLY H H 1 . 94.010 . . . . . . . . . . . . . . . . 6497 5 68 1JNH . 1 1 76 76 GLY N N 15 . . 1 1 76 76 GLY H H 1 . 93.434 . . . . . . . . . . . . . . . . 6497 5 stop_ save_ save_J_coupling_list_J_mod_500 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_J_mod_500 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 6 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 500 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 2 '1JNH-modulated 2D HSQC' 1 $sample_1 isotropic 6497 6 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.475 . . . . . . . . . . . . . . . . 6497 6 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.130 . . . . . . . . . . . . . . . . 6497 6 3 1JNH . 1 1 4 4 PHE N N 15 . . 1 1 4 4 PHE H H 1 . 93.978 . . . . . . . . . . . . . . . . 6497 6 4 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 93.085 . . . . . . . . . . . . . . . . 6497 6 5 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.800 . . . . . . . . . . . . . . . . 6497 6 6 1JNH . 1 1 7 7 THR N N 15 . . 1 1 7 7 THR H H 1 . 94.570 . . . . . . . . . . . . . . . . 6497 6 7 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.232 . . . . . . . . . . . . . . . . 6497 6 8 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.880 . . . . . . . . . . . . . . . . 6497 6 9 1JNH . 1 1 10 10 GLY N N 15 . . 1 1 10 10 GLY H H 1 . 93.564 . . . . . . . . . . . . . . . . 6497 6 10 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.896 . . . . . . . . . . . . . . . . 6497 6 11 1JNH . 1 1 12 12 THR N N 15 . . 1 1 12 12 THR H H 1 . 92.771 . . . . . . . . . . . . . . . . 6497 6 12 1JNH . 1 1 13 13 ILE N N 15 . . 1 1 13 13 ILE H H 1 . 93.367 . . . . . . . . . . . . . . . . 6497 6 13 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 93.081 . . . . . . . . . . . . . . . . 6497 6 14 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.418 . . . . . . . . . . . . . . . . 6497 6 15 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.535 . . . . . . . . . . . . . . . . 6497 6 16 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.796 . . . . . . . . . . . . . . . . 6497 6 17 1JNH . 1 1 18 18 GLU N N 15 . . 1 1 18 18 GLU H H 1 . 92.810 . . . . . . . . . . . . . . . . 6497 6 18 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.505 . . . . . . . . . . . . . . . . 6497 6 19 1JNH . 1 1 21 21 ASP N N 15 . . 1 1 21 21 ASP H H 1 . 95.050 . . . . . . . . . . . . . . . . 6497 6 20 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.764 . . . . . . . . . . . . . . . . 6497 6 21 1JNH . 1 1 23 23 ILE N N 15 . . 1 1 23 23 ILE H H 1 . 94.229 . . . . . . . . . . . . . . . . 6497 6 22 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 94.943 . . . . . . . . . . . . . . . . 6497 6 23 1JNH . 1 1 26 26 VAL N N 15 . . 1 1 26 26 VAL H H 1 . 93.923 . . . . . . . . . . . . . . . . 6497 6 24 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.313 . . . . . . . . . . . . . . . . 6497 6 25 1JNH . 1 1 28 28 ALA N N 15 . . 1 1 28 28 ALA H H 1 . 95.050 . . . . . . . . . . . . . . . . 6497 6 26 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.602 . . . . . . . . . . . . . . . . 6497 6 27 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 94.023 . . . . . . . . . . . . . . . . 6497 6 28 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.604 . . . . . . . . . . . . . . . . 6497 6 29 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.506 . . . . . . . . . . . . . . . . 6497 6 30 1JNH . 1 1 34 34 GLU N N 15 . . 1 1 34 34 GLU H H 1 . 91.135 . . . . . . . . . . . . . . . . 6497 6 31 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.946 . . . . . . . . . . . . . . . . 6497 6 32 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.394 . . . . . . . . . . . . . . . . 6497 6 33 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.155 . . . . . . . . . . . . . . . . 6497 6 34 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.858 . . . . . . . . . . . . . . . . 6497 6 35 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 94.121 . . . . . . . . . . . . . . . . 6497 6 36 1JNH . 1 1 42 42 ARG N N 15 . . 1 1 42 42 ARG H H 1 . 93.882 . . . . . . . . . . . . . . . . 6497 6 37 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.807 . . . . . . . . . . . . . . . . 6497 6 38 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.540 . . . . . . . . . . . . . . . . 6497 6 39 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 93.911 . . . . . . . . . . . . . . . . 6497 6 40 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.450 . . . . . . . . . . . . . . . . 6497 6 41 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.214 . . . . . . . . . . . . . . . . 6497 6 42 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.578 . . . . . . . . . . . . . . . . 6497 6 43 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.410 . . . . . . . . . . . . . . . . 6497 6 44 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.720 . . . . . . . . . . . . . . . . 6497 6 45 1JNH . 1 1 51 51 GLU N N 15 . . 1 1 51 51 GLU H H 1 . 93.336 . . . . . . . . . . . . . . . . 6497 6 46 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.284 . . . . . . . . . . . . . . . . 6497 6 47 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.724 . . . . . . . . . . . . . . . . 6497 6 48 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.840 . . . . . . . . . . . . . . . . 6497 6 49 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 95.063 . . . . . . . . . . . . . . . . 6497 6 50 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.195 . . . . . . . . . . . . . . . . 6497 6 51 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.417 . . . . . . . . . . . . . . . . 6497 6 52 1JNH . 1 1 59 59 TYR N N 15 . . 1 1 59 59 TYR H H 1 . 93.317 . . . . . . . . . . . . . . . . 6497 6 53 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.289 . . . . . . . . . . . . . . . . 6497 6 54 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.367 . . . . . . . . . . . . . . . . 6497 6 55 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.561 . . . . . . . . . . . . . . . . 6497 6 56 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.872 . . . . . . . . . . . . . . . . 6497 6 57 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.519 . . . . . . . . . . . . . . . . 6497 6 58 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.639 . . . . . . . . . . . . . . . . 6497 6 59 1JNH . 1 1 66 66 THR N N 15 . . 1 1 66 66 THR H H 1 . 92.084 . . . . . . . . . . . . . . . . 6497 6 60 1JNH . 1 1 67 67 LEU N N 15 . . 1 1 67 67 LEU H H 1 . 93.781 . . . . . . . . . . . . . . . . 6497 6 61 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.788 . . . . . . . . . . . . . . . . 6497 6 62 1JNH . 1 1 69 69 LEU N N 15 . . 1 1 69 69 LEU H H 1 . 93.475 . . . . . . . . . . . . . . . . 6497 6 63 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.774 . . . . . . . . . . . . . . . . 6497 6 64 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.758 . . . . . . . . . . . . . . . . 6497 6 65 1JNH . 1 1 73 73 LEU N N 15 . . 1 1 73 73 LEU H H 1 . 93.475 . . . . . . . . . . . . . . . . 6497 6 66 1JNH . 1 1 74 74 ARG N N 15 . . 1 1 74 74 ARG H H 1 . 93.331 . . . . . . . . . . . . . . . . 6497 6 67 1JNH . 1 1 75 75 GLY N N 15 . . 1 1 75 75 GLY H H 1 . 94.018 . . . . . . . . . . . . . . . . 6497 6 68 1JNH . 1 1 76 76 GLY N N 15 . . 1 1 76 76 GLY H H 1 . 93.464 . . . . . . . . . . . . . . . . 6497 6 stop_ save_ save_J_coupling_list_J_mod_600 _Coupling_constant_list.Sf_category coupling_constants _Coupling_constant_list.Sf_framecode J_coupling_list_J_mod_600 _Coupling_constant_list.Entry_ID 6497 _Coupling_constant_list.ID 7 _Coupling_constant_list.Name . _Coupling_constant_list.Sample_condition_list_ID 1 _Coupling_constant_list.Sample_condition_list_label $conditions_1 _Coupling_constant_list.Spectrometer_frequency_1H 600 _Coupling_constant_list.Details . _Coupling_constant_list.Text_data_format . _Coupling_constant_list.Text_data . loop_ _Coupling_constant_experiment.Experiment_ID _Coupling_constant_experiment.Experiment_name _Coupling_constant_experiment.Sample_ID _Coupling_constant_experiment.Sample_label _Coupling_constant_experiment.Sample_state _Coupling_constant_experiment.Entry_ID _Coupling_constant_experiment.Coupling_constant_list_ID 2 '1JNH-modulated 2D HSQC' 1 $sample_1 isotropic 6497 7 stop_ loop_ _Coupling_constant.ID _Coupling_constant.Code _Coupling_constant.Assembly_atom_ID_1 _Coupling_constant.Entity_assembly_ID_1 _Coupling_constant.Entity_ID_1 _Coupling_constant.Comp_index_ID_1 _Coupling_constant.Seq_ID_1 _Coupling_constant.Comp_ID_1 _Coupling_constant.Atom_ID_1 _Coupling_constant.Atom_type_1 _Coupling_constant.Atom_isotope_number_1 _Coupling_constant.Ambiguity_code_1 _Coupling_constant.Assembly_atom_ID_2 _Coupling_constant.Entity_assembly_ID_2 _Coupling_constant.Entity_ID_2 _Coupling_constant.Comp_index_ID_2 _Coupling_constant.Seq_ID_2 _Coupling_constant.Comp_ID_2 _Coupling_constant.Atom_ID_2 _Coupling_constant.Atom_type_2 _Coupling_constant.Atom_isotope_number_2 _Coupling_constant.Ambiguity_code_2 _Coupling_constant.Val _Coupling_constant.Val_min _Coupling_constant.Val_max _Coupling_constant.Val_err _Coupling_constant.Resonance_ID_1 _Coupling_constant.Resonance_ID_2 _Coupling_constant.Auth_entity_assembly_ID_1 _Coupling_constant.Auth_asym_ID_1 _Coupling_constant.Auth_seq_ID_1 _Coupling_constant.Auth_comp_ID_1 _Coupling_constant.Auth_atom_ID_1 _Coupling_constant.Auth_entity_assembly_ID_2 _Coupling_constant.Auth_asym_ID_2 _Coupling_constant.Auth_seq_ID_2 _Coupling_constant.Auth_comp_ID_2 _Coupling_constant.Auth_atom_ID_2 _Coupling_constant.Details _Coupling_constant.Entry_ID _Coupling_constant.Coupling_constant_list_ID 1 1JNH . 1 1 2 2 GLN N N 15 . . 1 1 2 2 GLN H H 1 . 93.444 . . . . . . . . . . . . . . . . 6497 7 2 1JNH . 1 1 3 3 ILE N N 15 . . 1 1 3 3 ILE H H 1 . 93.104 . . . . . . . . . . . . . . . . 6497 7 3 1JNH . 1 1 4 4 PHE N N 15 . . 1 1 4 4 PHE H H 1 . 93.934 . . . . . . . . . . . . . . . . 6497 7 4 1JNH . 1 1 5 5 VAL N N 15 . . 1 1 5 5 VAL H H 1 . 92.994 . . . . . . . . . . . . . . . . 6497 7 5 1JNH . 1 1 6 6 LYS N N 15 . . 1 1 6 6 LYS H H 1 . 93.722 . . . . . . . . . . . . . . . . 6497 7 6 1JNH . 1 1 7 7 THR N N 15 . . 1 1 7 7 THR H H 1 . 94.499 . . . . . . . . . . . . . . . . 6497 7 7 1JNH . 1 1 8 8 LEU N N 15 . . 1 1 8 8 LEU H H 1 . 93.248 . . . . . . . . . . . . . . . . 6497 7 8 1JNH . 1 1 9 9 THR N N 15 . . 1 1 9 9 THR H H 1 . 92.904 . . . . . . . . . . . . . . . . 6497 7 9 1JNH . 1 1 10 10 GLY N N 15 . . 1 1 10 10 GLY H H 1 . 93.589 . . . . . . . . . . . . . . . . 6497 7 10 1JNH . 1 1 11 11 LYS N N 15 . . 1 1 11 11 LYS H H 1 . 93.866 . . . . . . . . . . . . . . . . 6497 7 11 1JNH . 1 1 12 12 THR N N 15 . . 1 1 12 12 THR H H 1 . 92.736 . . . . . . . . . . . . . . . . 6497 7 12 1JNH . 1 1 13 13 ILE N N 15 . . 1 1 13 13 ILE H H 1 . 93.295 . . . . . . . . . . . . . . . . 6497 7 13 1JNH . 1 1 14 14 THR N N 15 . . 1 1 14 14 THR H H 1 . 92.982 . . . . . . . . . . . . . . . . 6497 7 14 1JNH . 1 1 15 15 LEU N N 15 . . 1 1 15 15 LEU H H 1 . 94.381 . . . . . . . . . . . . . . . . 6497 7 15 1JNH . 1 1 16 16 GLU N N 15 . . 1 1 16 16 GLU H H 1 . 92.463 . . . . . . . . . . . . . . . . 6497 7 16 1JNH . 1 1 17 17 VAL N N 15 . . 1 1 17 17 VAL H H 1 . 93.786 . . . . . . . . . . . . . . . . 6497 7 17 1JNH . 1 1 18 18 GLU N N 15 . . 1 1 18 18 GLU H H 1 . 92.812 . . . . . . . . . . . . . . . . 6497 7 18 1JNH . 1 1 20 20 SER N N 15 . . 1 1 20 20 SER H H 1 . 92.482 . . . . . . . . . . . . . . . . 6497 7 19 1JNH . 1 1 21 21 ASP N N 15 . . 1 1 21 21 ASP H H 1 . 95.081 . . . . . . . . . . . . . . . . 6497 7 20 1JNH . 1 1 22 22 THR N N 15 . . 1 1 22 22 THR H H 1 . 93.745 . . . . . . . . . . . . . . . . 6497 7 21 1JNH . 1 1 23 23 ILE N N 15 . . 1 1 23 23 ILE H H 1 . 94.164 . . . . . . . . . . . . . . . . 6497 7 22 1JNH . 1 1 25 25 ASN N N 15 . . 1 1 25 25 ASN H H 1 . 94.868 . . . . . . . . . . . . . . . . 6497 7 23 1JNH . 1 1 26 26 VAL N N 15 . . 1 1 26 26 VAL H H 1 . 93.874 . . . . . . . . . . . . . . . . 6497 7 24 1JNH . 1 1 27 27 LYS N N 15 . . 1 1 27 27 LYS H H 1 . 94.388 . . . . . . . . . . . . . . . . 6497 7 25 1JNH . 1 1 28 28 ALA N N 15 . . 1 1 28 28 ALA H H 1 . 95.001 . . . . . . . . . . . . . . . . 6497 7 26 1JNH . 1 1 29 29 LYS N N 15 . . 1 1 29 29 LYS H H 1 . 94.614 . . . . . . . . . . . . . . . . 6497 7 27 1JNH . 1 1 30 30 ILE N N 15 . . 1 1 30 30 ILE H H 1 . 93.963 . . . . . . . . . . . . . . . . 6497 7 28 1JNH . 1 1 32 32 ASP N N 15 . . 1 1 32 32 ASP H H 1 . 94.594 . . . . . . . . . . . . . . . . 6497 7 29 1JNH . 1 1 33 33 LYS N N 15 . . 1 1 33 33 LYS H H 1 . 93.478 . . . . . . . . . . . . . . . . 6497 7 30 1JNH . 1 1 34 34 GLU N N 15 . . 1 1 34 34 GLU H H 1 . 91.063 . . . . . . . . . . . . . . . . 6497 7 31 1JNH . 1 1 35 35 GLY N N 15 . . 1 1 35 35 GLY H H 1 . 93.933 . . . . . . . . . . . . . . . . 6497 7 32 1JNH . 1 1 36 36 ILE N N 15 . . 1 1 36 36 ILE H H 1 . 91.336 . . . . . . . . . . . . . . . . 6497 7 33 1JNH . 1 1 39 39 ASP N N 15 . . 1 1 39 39 ASP H H 1 . 94.144 . . . . . . . . . . . . . . . . 6497 7 34 1JNH . 1 1 40 40 GLN N N 15 . . 1 1 40 40 GLN H H 1 . 92.870 . . . . . . . . . . . . . . . . 6497 7 35 1JNH . 1 1 41 41 GLN N N 15 . . 1 1 41 41 GLN H H 1 . 94.196 . . . . . . . . . . . . . . . . 6497 7 36 1JNH . 1 1 42 42 ARG N N 15 . . 1 1 42 42 ARG H H 1 . 93.860 . . . . . . . . . . . . . . . . 6497 7 37 1JNH . 1 1 43 43 LEU N N 15 . . 1 1 43 43 LEU H H 1 . 93.785 . . . . . . . . . . . . . . . . 6497 7 38 1JNH . 1 1 44 44 ILE N N 15 . . 1 1 44 44 ILE H H 1 . 92.479 . . . . . . . . . . . . . . . . 6497 7 39 1JNH . 1 1 45 45 PHE N N 15 . . 1 1 45 45 PHE H H 1 . 93.885 . . . . . . . . . . . . . . . . 6497 7 40 1JNH . 1 1 46 46 ALA N N 15 . . 1 1 46 46 ALA H H 1 . 94.354 . . . . . . . . . . . . . . . . 6497 7 41 1JNH . 1 1 47 47 GLY N N 15 . . 1 1 47 47 GLY H H 1 . 93.180 . . . . . . . . . . . . . . . . 6497 7 42 1JNH . 1 1 48 48 LYS N N 15 . . 1 1 48 48 LYS H H 1 . 93.576 . . . . . . . . . . . . . . . . 6497 7 43 1JNH . 1 1 49 49 GLN N N 15 . . 1 1 49 49 GLN H H 1 . 93.374 . . . . . . . . . . . . . . . . 6497 7 44 1JNH . 1 1 50 50 LEU N N 15 . . 1 1 50 50 LEU H H 1 . 94.667 . . . . . . . . . . . . . . . . 6497 7 45 1JNH . 1 1 51 51 GLU N N 15 . . 1 1 51 51 GLU H H 1 . 93.287 . . . . . . . . . . . . . . . . 6497 7 46 1JNH . 1 1 52 52 ASP N N 15 . . 1 1 52 52 ASP H H 1 . 93.300 . . . . . . . . . . . . . . . . 6497 7 47 1JNH . 1 1 54 54 ARG N N 15 . . 1 1 54 54 ARG H H 1 . 93.734 . . . . . . . . . . . . . . . . 6497 7 48 1JNH . 1 1 55 55 THR N N 15 . . 1 1 55 55 THR H H 1 . 92.777 . . . . . . . . . . . . . . . . 6497 7 49 1JNH . 1 1 56 56 LEU N N 15 . . 1 1 56 56 LEU H H 1 . 95.084 . . . . . . . . . . . . . . . . 6497 7 50 1JNH . 1 1 57 57 SER N N 15 . . 1 1 57 57 SER H H 1 . 94.209 . . . . . . . . . . . . . . . . 6497 7 51 1JNH . 1 1 58 58 ASP N N 15 . . 1 1 58 58 ASP H H 1 . 95.384 . . . . . . . . . . . . . . . . 6497 7 52 1JNH . 1 1 59 59 TYR N N 15 . . 1 1 59 59 TYR H H 1 . 93.296 . . . . . . . . . . . . . . . . 6497 7 53 1JNH . 1 1 60 60 ASN N N 15 . . 1 1 60 60 ASN H H 1 . 94.263 . . . . . . . . . . . . . . . . 6497 7 54 1JNH . 1 1 61 61 ILE N N 15 . . 1 1 61 61 ILE H H 1 . 93.367 . . . . . . . . . . . . . . . . 6497 7 55 1JNH . 1 1 62 62 GLN N N 15 . . 1 1 62 62 GLN H H 1 . 93.590 . . . . . . . . . . . . . . . . 6497 7 56 1JNH . 1 1 63 63 LYS N N 15 . . 1 1 63 63 LYS H H 1 . 93.856 . . . . . . . . . . . . . . . . 6497 7 57 1JNH . 1 1 64 64 GLU N N 15 . . 1 1 64 64 GLU H H 1 . 93.518 . . . . . . . . . . . . . . . . 6497 7 58 1JNH . 1 1 65 65 SER N N 15 . . 1 1 65 65 SER H H 1 . 94.677 . . . . . . . . . . . . . . . . 6497 7 59 1JNH . 1 1 66 66 THR N N 15 . . 1 1 66 66 THR H H 1 . 92.064 . . . . . . . . . . . . . . . . 6497 7 60 1JNH . 1 1 67 67 LEU N N 15 . . 1 1 67 67 LEU H H 1 . 93.963 . . . . . . . . . . . . . . . . 6497 7 61 1JNH . 1 1 68 68 HIS N N 15 . . 1 1 68 68 HIS H H 1 . 93.744 . . . . . . . . . . . . . . . . 6497 7 62 1JNH . 1 1 69 69 LEU N N 15 . . 1 1 69 69 LEU H H 1 . 93.309 . . . . . . . . . . . . . . . . 6497 7 63 1JNH . 1 1 70 70 VAL N N 15 . . 1 1 70 70 VAL H H 1 . 93.788 . . . . . . . . . . . . . . . . 6497 7 64 1JNH . 1 1 71 71 LEU N N 15 . . 1 1 71 71 LEU H H 1 . 93.729 . . . . . . . . . . . . . . . . 6497 7 65 1JNH . 1 1 73 73 LEU N N 15 . . 1 1 73 73 LEU H H 1 . 93.531 . . . . . . . . . . . . . . . . 6497 7 66 1JNH . 1 1 74 74 ARG N N 15 . . 1 1 74 74 ARG H H 1 . 93.349 . . . . . . . . . . . . . . . . 6497 7 67 1JNH . 1 1 75 75 GLY N N 15 . . 1 1 75 75 GLY H H 1 . 93.998 . . . . . . . . . . . . . . . . 6497 7 68 1JNH . 1 1 76 76 GLY N N 15 . . 1 1 76 76 GLY H H 1 . 93.437 . . . . . . . . . . . . . . . . 6497 7 stop_ save_ ######################### # Other kinds of data # ######################### save_DFS _Other_data_type_list.Sf_category other_data_types _Other_data_type_list.Sf_framecode DFS _Other_data_type_list.Entry_ID 6497 _Other_data_type_list.ID 1 _Other_data_type_list.Name 'Dynamic Frequency Shift' _Other_data_type_list.Definition 'Magnetic field dependent variation' _Other_data_type_list.Sample_condition_list_ID 1 _Other_data_type_list.Sample_condition_list_label $conditions_1 _Other_data_type_list.Chem_shift_reference_ID . _Other_data_type_list.Chem_shift_reference_label . _Other_data_type_list.Details . _Other_data_type_list.Text_data_format text _Other_data_type_list.Text_data ; Residue deltaDFS(360) deltaDFS(500) deltaDFS (600) Q2 -0.2279 -0.3016 -0.3375 I3 -0.2209 -0.2999 -0.3398 F4 -0.2291 -0.3090 -0.3491 V5 -0.2075 -0.2816 -0.3191 K6 -0.2206 -0.2971 -0.3355 T7 -0.2194 -0.2959 -0.3344 L8 -0.1932 -0.2621 -0.2970 T9 -0.1893 -0.2543 -0.2866 GlO -0.1840 -0.2497 -0.2830 Kll -0.1892 -0.2519 -0.2827 T12 -0.1881 -0.2557 -0.2899 I13 -0.2167 -0.2919 -0.3296 T14 -0.2099 -0.2839 -0.3212 L15 -0.2102 -0.2834 -0.3201 El6 -0.2053 -0.2741 -0.3081 V17 -0.2267 -0.3048 -0.3436 El8 -0.2294 -0.3042 -0.3407 S20 -0.2198 -0.2946 -0.3317 D21 -0.2335 -0.3135 -0.3533 T22 -0.2136 -0.2897 -0.3281 123 -0.2291 -0.3038 -0.3402 N25 -0.2190 -0.2953 -0.3334 V26 -0.2192 -0.2956 -0.3338 K27 -0.2314 -0.3132 -0.3543 A28 -0.2321 -0.3119 -0.3516 K29 -0.2243 -0.3037 -0.3437 I30 -0.2243 -0.3033 -0.3431 Q31 -0.2057 -0.2767 -0.3121 D32 -0.2261 -0.3058 -0.3460 K33 -0.2173 -0.2935 -0.3317 E34 -0.2142 -0.2901 -0.3284 G35 -0.2329 -0.3080 -0.3444 136 -0.2123 -0.2813 -0.3149 D39 -0.2126 -0.2887 -0.3273 Q40 -0.2238 -0.3006 -0.3389 Q41 -0.2120 -0.2881 -0.3267 R42 -0.2123 -0.2863 -0.3234 L43 -0.2068 -0.2808 -0.3182 I44 -0.2128 -0.2873 -0.3248 F45 -0.2229 -0.3006 -0.3395 A46 -0.2132 -0.2880 -0.3257 G47 -0.2044 -0.2778 -0.3150 K48 -0.2210 -0.2957 -0.3328 Q49 -0.1895 -0.2566 -0.2904 LSO -0.2146 -0.2890 -0.3263 E51 -0.2155 -0.2856 -0.3198 D52 -0.2134 -0.2828 -0.3166 R54 -0.2321 -0.3074 -0.3441 T55 -0.2175 -0.2950 -0.3343 L56 -0.2289 -0.3091 -0.3495 S57 -0.2188 -0.2966 -0.3359 D58 -0.2251 -0.3047 -0.3448 Y59 -0.2197 -0.2969 -0.3357 N60 -0.2198 -0.2987 -0.3387 I61 -0.2178 -0.2942 -0.3326 Q62 -0.1815 -0.2439 -0.2750 K63 -0.2176 -0.2898 -0.3252 E64 -0.2212 -0.2995 -0.3390 S65 -0.2252 -0.3025 -0.3410 T66 -0.2123 -0.2874 -0.3251 L67 -0.2130 -0.2880 -0.3259 H68 -0.2194 -0.2972 -0.3365 L69 -0.2145 -0.2900 -0.3280 V70 -0.2340 -0.3148 -0.3552 L71 -0.1992 -0.2702 -0.3061 L73 -0.1414 -0.1919 -0.2174 R74 -0.1078 -0.1464 -0.1659 G75 -0.0663 -0.0895 -0.1019 G76 -0.0382 -0.0519 -0.0588 ; loop_ _Other_data_experiment.Experiment_ID _Other_data_experiment.Experiment_name _Other_data_experiment.Sample_ID _Other_data_experiment.Sample_label _Other_data_experiment.Sample_state _Other_data_experiment.Entry_ID _Other_data_experiment.Other_data_type_list_ID 2 '1JNH-modulated 2D HSQC' 1 $sample_1 isotropic 6497 1 stop_ save_