BMRB Entry 15662

Assembly:

Entities:

Entity 1, amelogenin 191 residues - Formula weight is not available

Samples:

sample_1: amelogenin, [U-99% 13C; U-99% 15N], 2 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

sample_2: amelogenin, 50% [U-15N]-Leu, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_3: amelogenin, 50% [U-15N]-Val, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_4: amelogenin, 50% [U-15N]-His, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_5: amelogenin, 50% [U-15N]-Arg, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_6: amelogenin, 50% [U-15N]-Lys, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_7: amelogenin, 50% [U-15N]-Met, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_8: amelogenin, 50% [U-15N]-Phe, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_9: amelogenin, 50% [U-15N]-Tyr, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

Sample_10: amelogenin, 50% [U-15N]-Glu/Gln, 0.2-1 ± 0.2 mM; acetic acid, [U-2H], 2 ± 0.1 %

sample_conditions_1: ionic strength: 0 M; pH: 3; pressure: 1 atm; temperature: 298 K

Experiments:

Software:

FELIX v2007, Accelrys Software Inc. - chemical shift assignment, data analysis

NMR spectrometers:

• Varian INOVA 900 MHz
• Varian INOVA 600 MHz
• Varian INOVA 800 MHz
• Varian INOVA 750 MHz