BMRB Entry 52313
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR52313
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Title: Vcom1 PubMed: 38747744
Deposition date: 2024-02-07 Original release date: 2024-07-22
Authors: Khatibi, Negin; Huang, Yen-Hua; Wang, Conan; Durek, Thomas; Gilding, Edward; Craik, David
Citation: Khatibi, Negin; Huang, Yen-Hua; Wang, Conan; Durek, Thomas; Gilding, Edward; Craik, David. "Isolation and Characterization of Insecticidal Cyclotides from Viola communis" J. Nat. Prod. ., .-. (2024).
Assembly members:
entity_1, polymer, 30 residues, Formula weight is not available
Natural source: Common Name: Violaceae Taxonomy ID: 24921 Superkingdom: Eukaryota Kingdom: Viridiplantae Genus/species: not available not available
Experimental source: Production method: purified from the natural source
Entity Sequences (FASTA):
entity_1: AAVPCGESCVWIPCFSSVIG
CSCKNKVCYN
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 64 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Vcom1 monomer | 1 |
Entities:
Entity 1, Vcom1 monomer 30 residues - Formula weight is not available
| 1 | ALA | ALA | VAL | PRO | CYS | GLY | GLU | SER | CYS | VAL | |
| 2 | TRP | ILE | PRO | CYS | PHE | SER | SER | VAL | ILE | GLY | |
| 3 | CYS | SER | CYS | LYS | ASN | LYS | VAL | CYS | TYR | ASN |
Samples:
sample_1: Vcom1 0.7 mg
sample_conditions_1: ionic strength: 0 M; pH: 3.8; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
TOPSPIN - collection
NMR spectrometers:
- Bruker ARX 600 600 MHz