BMRB Entry 16407
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR16407
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Title: Role of Trp-Trp interactions in Trpzip beta-hairpin formation, structure and stability PubMed: 19788311
Deposition date: 2009-07-14 Original release date: 2009-08-25
Authors: Wu, Ling; McElheny, Dan; Huang, Rong; Keiderling, Timothy
Citation: Wu, Ling; McElheny, Dan; Huang, Rong; Keiderling, Timothy. "Role of tryptophan-tryptophan interactions in Trpzip beta-hairpin formation, structure, and stability." Biochemistry 48, 10362-10371 (2009).
Assembly members:
W2W11, polymer, 12 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
W2W11: SWTVENGKVTWK
- assigned_chemical_shifts
Data type | Count |
1H chemical shifts | 86 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | monomer | 1 |
Entities:
Entity 1, monomer 12 residues - Formula weight is not available
1 | SER | TRP | THR | VAL | GLU | ASN | GLY | LYS | VAL | THR | ||||
2 | TRP | LYS |
Samples:
sample_1: W2W11 4 ± 0.1 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 0.02 M; pH: 5.8; pressure: 1 atm; temperature: 281 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
NMRView v5.2.2_01, Case, Darden, Cheatham, III, Simmerling, Wang, Duke, Luo, ... and Kollm, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax, Guntert, Mumenthaler and Wuthrich, Johnson, One Moon Scientific - chemical shift assignment, data analysis, peak picking, refinement, structure solution
NMR spectrometers:
- Bruker Avance 800 MHz