BMRB Entry 21082
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21082
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Title: HAL-2/27
Deposition date: 2018-09-19 Original release date: 2020-05-12
Authors: Socha, Ondrej
Citation: Kocendova, Jitka; Vankova, Eva; Volejnikova, Andrea; Nesuta, Ondrej; Hajek, Miroslav; Hadravova, Romana; Humpolickova, Jana; Budesinsky, Milos; Socha, Ondrej; Cerovsky, Vaclav. "HAL-2/27" .
Assembly members:
HAL-2/27, polymer, 13 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
HAL-2/27: GKWMKLLKKILKX
- assigned_chemical_shifts
Data type | Count |
13C chemical shifts | 72 |
15N chemical shifts | 12 |
1H chemical shifts | 117 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | polypeptide | 1 |
Entities:
Entity 1, polypeptide 13 residues - Formula weight is not available
1 | GLY | LYS | TRP | MET | LYS | LEU | LEU | LYS | LYS | ILE | ||||
2 | LEU | LYS | NH2 |
Samples:
sample_1: TFE 30 v/v; H2O 95%; D2O, [U-2H], 5%
sample_conditions_1: pH: 4.4; temperature: 298 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H COSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-15N HSQC | sample_1 | isotropic | sample_conditions_1 |
2D 1H-13C HSQC | sample_1 | isotropic | sample_conditions_1 |
Software:
CcpNmr_Analysis v2.4, CCPN - chemical shift assignment, peak picking
X-PLOR_NIH v2.44, Schwieters, Kuszewski, Tjandra and Clore - refinement, structure solution
TOPSPIN, Bruker Biospin - collection, processing
TALOS, Cornilescu, Delaglio and Bax - data analysis
NMR spectrometers:
- Bruker Avance 600 MHz
Download HSQC peak lists in one of the following formats:
CSV: Backbone
or all simulated shifts
SPARKY: Backbone
or all simulated shifts