BMRB Entry 26033
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR26033
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Title: Structural insight for dynamics of r(CGG) motif RNA found in Fragile X syndrome/ Fragile X tremor ataxia at 25 degree C
Deposition date: 2016-04-12 Original release date: 2017-05-10
Authors: Mishra, Subodh; Kumar, Amit
Citation: Mishra, Subodh; Kumar, Amit. "Structural insights reveal the dynamics of the repeating r(CGG) motif found in Fragile X Syndrome and Fragile-X associated tremor/ataxia syndrome (FXTAS)" .
Assembly members:
RNA_(5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3'), polymer, 9 residues, 2901.816 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
RNA_(5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3'): CCGCGGCGG
- assigned_chemical_shifts
Data type | Count |
1H chemical shifts | 42 |
Additional metadata:
Assembly:
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | RNA (5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3')_1 | 1 |
2 | RNA (5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3')_2 | 1 |
Entities:
Entity 1, RNA (5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3')_1 9 residues - 2901.816 Da.
1 | C | C | G | C | G | G | C | G | G |
Samples:
CGG_25C: RNA (5'-R(P*CP*CP*GP*CP*GP*GP*CP*GP*G)-3') 1.5 mM; H2O 90%; D2O, [U-2H], 10%
sample_conditions_1: pH: 7; pressure: 1 atm; temperature: 298 K
Experiments:
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H NOESY | CGG_25C | isotropic | sample_conditions_1 |
Software:
SPARKY, Goddard - chemical shift assignment
TOPSPIN, Bruker Biospin - chemical shift calculation
DISCOVER, Accelrys Software Inc. - geometry optimization
NMR spectrometers:
- Bruker Avance 400 MHz