BMRB Entry 30265
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Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR30265
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Title: Peptide 38148 modified from fragment 41-60 of Plasmodium falciparum Thrombospondin-Related Sporozoite Protein (TRSP)
Deposition date: 2017-03-03 Original release date: 2018-07-30
Authors: Bermudez, A.; Patarroyo, M.
Citation: Bermudez, A.; Patarroyo, M.. "Peptide 38148 modified from fragment 41-60 of Plasmodium falciparum Thrombospondin-Related Sporozoite Protein (TRSP)" .
Assembly members:
entity_1, polymer, 20 residues, 2431.622 Da.
Natural source: Common Name: Plasmodium falciparum Taxonomy ID: 36329 Superkingdom: Eukaryota Kingdom: not available Genus/species: Plasmodium falciparum
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: SDTRYNKSFINNKHLNEHAH
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 126 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity_1 | 1 |
Entities:
Entity 1, entity_1 20 residues - 2431.622 Da.
| 1 | SER | ASP | THR | ARG | TYR | ASN | LYS | SER | PHE | ILE | |
| 2 | ASN | ASN | LYS | HIS | LEU | ASN | GLU | HIS | ALA | HIS |
Samples:
sample_1: entity_1 16.6 ± 0.1 mg/mL
sample_conditions_1: pH: 3.7; pressure: 1 .; temperature: 295 K
sample_conditions_2: pH: 3.7; pressure: 1 .; temperature: 285 K
sample_conditions_3: pH: 3.7; pressure: 1 .; temperature: 305 K
sample_conditions_4: pH: 3.7; pressure: 1 .; temperature: 315 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY; 2D 1H-1H TOCSY; 2D 1H-1H NOESY | sample_1 | anisotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | anisotropic | sample_conditions_2 |
| 2D 1H-1H TOCSY | sample_1 | anisotropic | sample_conditions_3 |
| 2D 1H-1H TOCSY | sample_1 | anisotropic | sample_conditions_4 |
Software:
InsightII, Accelrys Software Inc. - geometry optimization, refinement
NMR spectrometers:
- Bruker DRX 600 MHz