BMRB Entry 4266
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4266
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Title: The Solution Structure of a Superpotent B-chain-shortened Single-replacement Insulin Analogue
Deposition date: 1998-11-08 Original release date: 2002-08-12
Authors: Kurapkat, Guenther; Siedentop, Michael; Gattner, Hans-Georg; Hagelstein, Michael; Brandenburg, Dietrich; Grotzinger, Joachim; Wollmer, Axel
Citation: Kurapkat, Guenther; Siedentop, Michael; Gattner, Hans-Georg; Hagelstein, Michael; Brandenburg, Dietrich; Grotzinger, Joachim; Wollmer, Axel. "The Solution Structure of a Superpotent B-chain-shortend Single-replacement Insulin Analogue" Protein Sci. 8, 499-508 (1999).
Assembly members:
[D-AlaB26]destetra(B27-B30)insulin-B26-amide, polymer, 47 residues, Formula weight is not available
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemically synthesized
Entity Sequences (FASTA):
[D-AlaB26]destetra(B27-B30)insulin-B26-amide: GIVEQCCTSICSLYQLENYC
NFVNQHLCGSHLVEALYLVC
GERGFFA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 293 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | [D-AlaB26]DTI-amide_A-chain | 1 |
| 2 | [D-AlaB26]DTI-amide_B-chain | 1 |
Entities:
Entity 1, [D-AlaB26]DTI-amide_A-chain 47 residues - Formula weight is not available
| 1 | GLY | ILE | VAL | GLU | GLN | CYS | CYS | THR | SER | ILE | ||||
| 2 | CYS | SER | LEU | TYR | GLN | LEU | GLU | ASN | TYR | CYS | ||||
| 3 | ASN | PHE | VAL | ASN | GLN | HIS | LEU | CYS | GLY | SER | ||||
| 4 | HIS | LEU | VAL | GLU | ALA | LEU | TYR | LEU | VAL | CYS | ||||
| 5 | GLY | GLU | ARG | GLY | PHE | PHE | ALA |
Samples:
sample_one: [D-AlaB26]destetra(B27-B30)insulin-B26-amide 4 mM
sample_conditions_one: pH*: 1.9 na; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|
Software:
No software information available
NMR spectrometers:
- unknown unknown 0 MHz