BMRB Entry 4975
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4975
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Title: Assignment of selectively 13C-labeled cellopentaose synthesized using an engineered glycosynthase
Deposition date: 2001-03-20 Original release date: 2001-10-08
Authors: Brun, Emmanuel; Brummer, Harry; Mackenzie, Lloyd; Withers, Stephen; McIntosh, Lawrence
Citation: Brun, Emmanuel; Brumer, Harry; Mackenzie, Lloyd; Withers, Stephen; McIntosh, Lawrence. "Letter to the Editor: Assignment of selectively 13C-labeled cellopentaose synthesized using an engineered glycosynthase" J. Biomol. NMR 21, 67-68 (2001).
Assembly members:
cellopentaose, polymer, 5 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: enzymatic semisynthesis
Entity Sequences (FASTA):
cellopentaose: XXXXX
- assigned_chemical_shifts
- coupling_constants
| Data type | Count |
| 13C chemical shifts | 6 |
| 1H chemical shifts | 7 |
| coupling constants | 8 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | cellopentaose | 1 |
Entities:
Entity 1, cellopentaose 5 residues - Formula weight is not available
| 1 | GLC | GLC | GLC | GLC | GLC |
Samples:
sample_1: cellopentaose, [U-95% 13C]-Glc2, 3.3 mM
condition_1: pH: .; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H-13C HSQC | sample_1 | not available | condition_1 |
| 1H-13C HCCH-COSY | sample_1 | not available | condition_1 |
Software:
FELIX v2.3 - processing
NMR spectrometers:
- Varian Unity 500 MHz