BMRB Entry 51742
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR51742
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Title: [D-Cys5,D-Lys16]-STp(5-17), native form PubMed: 36770798
Deposition date: 2022-12-15 Original release date: 2023-03-07
Authors: Shimamoto, Shigeru; Hidaka, Yuji
Citation: Goto, Masaya; Yoshino, Shinya; Hiroshima, Kyona; Kawakami, Toru; Murota, Kaeko; Shimamoto, Shigeru; Hidaka, Yuji. "The Molecular Basis of Heat-Stable Enterotoxin for Vaccine Development and Cancer Cell Detection" Molecules 28, 1128-1128 (2023).
Assembly members:
entity_1, polymer, 13 residues, Formula weight is not available
Natural source: Common Name: E. coli Taxonomy ID: 562 Superkingdom: Bacteria Kingdom: not available Genus/species: Escherichia coli
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: XCELCCNPACAXC
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 63 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | [D-Cys5,D-Lys16]-STp(5-17), native form | 1 |
Entities:
Entity 1, [D-Cys5,D-Lys16]-STp(5-17), native form 13 residues - Formula weight is not available
| 1 | DCY | CYS | GLU | LEU | CYS | CYS | ASN | PRO | ALA | CYS | ||||
| 2 | ALA | DLY | CYS |
Samples:
sample_1: [D-Cys5,D-Lys16]-STp(5-17) 3 mM; sodium phosphate buffer 25 mM
sample_conditions_1: ionic strength: 25 mM; pH: 6.5; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
NMRPipe - chemical shift assignment
NMR spectrometers:
- JEOL JNM-ECA800 800 MHz