BMRB Entry 52122
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR52122
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Title: d(5mCpG)3 PubMed: 38131335
Deposition date: 2023-09-11 Original release date: 2023-12-27
Authors: Nichols, Parker; Krall, Jeffrey; Henen, Morkos; Welty, Robb; MacFadden, Andrea; Vicens, Quentin; Vogeli, Beat
Citation: Nichols, Parker; Krall, Jeffrey; Henen, Morkos; Welty, Robb; MacFadden, Andrea; Vicens, Quentin; Vogeli, Beat. "Z-Form Adoption of Nucleic Acid is a Multi-Step Process Which Proceeds through a Melted Intermediate" J. Am. Chem. Soc. 146, 677-694 (2024).
Assembly members:
entity_1, polymer, 6 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: XGXGXG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 38 |
| 1H chemical shifts | 54 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | d(5mCpG)3 | 1 |
Entities:
Entity 1, d(5mCpG)3 6 residues - Formula weight is not available
| 1 | MCY | DG | MCY | DG | MCY | DG |
Samples:
sample_1: d(5mCpG)3 3.1 mM; potassium phosphate 20 mM; NaCl 25 mM; EDTA 0.5 mM
sample_conditions_1: ionic strength: 0.243 M; pH: 6.4; pressure: 1 atm; temperature: 298.15 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-13C HSQC | sample_1 | isotropic | sample_conditions_1 |
Software:
CcpNMR - chemical shift assignment
NMRPipe - processing
TOPSPIN - collection
NMR spectrometers:
- Bruker AVANCE NEO 600 MHz