BMRB Entry 5731
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5731
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Title: 1H Chemical Shift Assignments for SCR3 peptide (18-34)
Deposition date: 2003-03-12 Original release date: 2004-09-14
Authors: Pertinhez, Thelma; Sherwood, Amanda; Fraceto, Leonardo; Bouchard, Mario; Pitkeathly, Maureen; Smith, Lorna
Citation: Pertinhez, Thelma; Sherwood, Amanda; Fraceto, Leonardo; Bouchard, Mario; Pitkeathly, Maureen; Smith, Lorna. "Alpha and beta Conformational preferences in Fibril Forming Peptides Characterised using NMR and CD Techniques" Spectroscopy (Amsterdam, Neth.) 18, 1-11 (2004).
Assembly members:
SCR3 peptide (18-34), polymer, 17 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
SCR3 peptide (18-34): STNRENFHYGSVVTYRS
- assigned_chemical_shifts
- coupling_constants
| Data type | Count |
| 1H chemical shifts | 334 |
| coupling constants | 29 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | SCR3(18-34), monomer | 1 |
Entities:
Entity 1, SCR3(18-34), monomer 17 residues - Formula weight is not available
| 1 | SER | THR | ASN | ARG | GLU | ASN | PHE | HIS | TYR | GLY | ||||
| 2 | SER | VAL | VAL | THR | TYR | ARG | SER |
Samples:
sample_1: SCR3 peptide (18-34) 2 mM
sample_2: SCR3 peptide (18-34) 2 mM; Trifluorethanol 30%
sample_3: SCR3 peptide (18-34) 2 mM; Trifluorethanol 80%
condition_1: pH: 4; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| TOCSY | not available | not available | condition_1 |
| ROESY | not available | not available | condition_1 |
| DQFCOSY | not available | not available | condition_1 |
Software:
FELIX v2000 and 2.3 -
NMR spectrometers:
- Home built . 500 MHz
- Home built . 600 MHz
- Varian INOVA 500 MHz